CN106758202A - The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt - Google Patents

The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt Download PDF

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Publication number
CN106758202A
CN106758202A CN201611190547.8A CN201611190547A CN106758202A CN 106758202 A CN106758202 A CN 106758202A CN 201611190547 A CN201611190547 A CN 201611190547A CN 106758202 A CN106758202 A CN 106758202A
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China
Prior art keywords
shirt
drying
temperature
pressing
liquid
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Pending
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CN201611190547.8A
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Chinese (zh)
Inventor
曹群
王素琴
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Fuyang Leopard Head Clothing Technology Co Ltd
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Fuyang Leopard Head Clothing Technology Co Ltd
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Priority to CN201611190547.8A priority Critical patent/CN106758202A/en
Publication of CN106758202A publication Critical patent/CN106758202A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
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    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B1/00—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
    • D06B1/02—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating by spraying or projecting
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    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C15/00—Calendering, pressing, ironing, glossing or glazing textile fabrics
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    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C7/00—Heating or cooling textile fabrics
    • D06C7/02—Setting
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    • D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
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    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D06M13/148—Polyalcohols, e.g. glycerol or glucose
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    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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    • D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
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    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
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    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
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    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
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    • D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
    • D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
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    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01—Natural vegetable fibres
    • D10B2201/02—Cotton

Abstract

The invention discloses the shrinkproof hydroscopic fast-drying type noniron finish liquid and method for sorting of a kind of shirt, it is made up of following raw materials according：Octamethylcy-clotetrasiloxane, t etram-ethyltetravinylcyclotetrasiloxane, potassium hydroxide, cetyl trimethylammonium bromide, butyl acrylate, acrylic acid, the methoxy acrylate of acrylic acid 2, potassium peroxydisulfate, appropriate OPEO, propane diols, glycerine, butane tetracid, lemon acid amide, triethanolamine, butenoic acid, sodium hypophosphite, boric acid, the semi-annular jade pendant acid derivative of talan two, etherification modified amino silicones, amido silicon oil, isomerous tridecanol polyoxyethylene ether, appropriate deionized water；The dressing liquid that the present invention is provided has good crease-resistant, non-ironing, quick-drying effect, and keep good, the comfortable and easy to wear advantage of fabric feeling, in addition, the anti-crease finishing liquid safety and environmental protection, will not release formaldehyde, be harmful to human health, through the shirt ready-made clothes Machine Washable after treatment, normally dry it is non-ironing, it is ultimate attainment crease-resistant indeformable, be worthy to be popularized.

Description

The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt
Technical field
It is non-ironing the present invention relates to ready-made clothes functional treatment technical field, more particularly to a kind of shrinkproof hydroscopic fast-drying type of shirt Dressing liquid and its method for sorting.
Background technology
Cotton ready-made clothes is so that its is comfortable and easy to wear, natural environmental-protective the features such as it is very popular, but due to wearing and washing During exist and easily wrinkle, be difficult the performance deficiency arranged, the life for giving people brings inconvenience.Therefore wear and relax Suitable, flat crease-resistant ready-made clothes application prospect that is very tangible, non-ironing, conveniently arranging is very wide.And current most popular N- The crease-shedding finishing agent of methylol class, it may appear that formaldehyde, pH value be exceeded and residuals cause the problem of skin urtication, causes wide Big consumer is panic to the psychology of crease-resistant ready-made clothes security performance, simultaneously because the crease-resistant treatment of tradition changes to original fabric performance Become, cause to lose the original water suction of cotton ready-made clothes, lead wet comfort property, therefore produce meet market public demand into Clothing is of great significance.
By patent retrieval, the contrast patent of Patent No. 201010300167.1, it discloses a kind of cotton shirt No-iron treatment method, step is successively Resin Absorbent → preliminary drying → pressing → bake → cool down；Resin Absorbent step is will be main The working solution of component modification bishydroxymethyl dihydroxy ethylene urea or modified alkyl dihydroxy ethylene urea is applied on shirt, raw Output has the cotton shirt of wash and wear, although resin by modification, but due to the invertibity of modifying process, in life Produce, accumulating and wear during use easily generation formaldehyde indirectly, can not completely by work by last cooling link Residuals are removed totally in liquid, there is unstable formaldehyde, pH value content, dress safety excitatory and environmentally friendly hidden danger.
A kind of contrast patent 2 of Patent No. 201410639422.3, the formaldehydeless antibacterial it discloses shirt is non-ironing whole Reason liquid and method for sorting, its use ready-made clothes prewashing-drying-dressing liquid process-determine wet drying-pressing-bake-static balancing-into The technological process of clothing after backwashing-drying is processed shirt, front and rear in this invention to dry production link twice, and use is 40-60 DEG C of low temperature drying temperature, while be " 6-12h " the time required to static balancing production link, with duration, production efficiency It is low, it is unfavorable for industrialization, streamlined, mass, large-scale production, economic and social benefit is low；It is multiple in ready-made clothes prewashing and ready-made clothes Wash in washing link twice, there is a problem of water resources consumption greatly and environment protection emission, be unfavorable for energy-saving and emission-reduction.Repeatedly wash simultaneously Wash and easily occur clothes when shirt washing quantity is more and mutually wind, knot and cause the serious fold of clothes, outward appearance poor Problem, influences crease-resistant rank and product quality, and utilization rate of equipment and installations is low during negligible amounts, and scale and benefit are poor.For prior art The problem and defect of presence, the present invention provide a kind of environmentally friendly noniron finish liquid and its ready-made clothes method for sorting so that produce Ready-made clothes reaches the performance of non-ironing, shrinkproof, moisture absorption, quick-drying, and safe and healthy, ring on the basis of original wrinkle resistance is kept Protect, easily realize industrialization, streamlined, mass and scale, reach huge economic benefit and social benefit.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of shrinkproof hydroscopic fast-drying type of shirt is non-ironing Dressing liquid and its method for sorting.
The present invention is achieved by the following technical solutions：
A kind of shrinkproof hydroscopic fast-drying type noniron finish liquid of shirt, is made up of the raw material of following weight portion：Prestox ring four Siloxanes 9-10, t etram-ethyltetravinylcyclotetrasiloxane 1-1.5, potassium hydroxide 0.01-0.02, cetyl trimethyl bromination Ammonium 0.32-0.35, butyl acrylate 15-18, acrylic acid 1.5-2, acrylic acid 2- methoxy acrylates 0.5-0.7, potassium peroxydisulfate 0.02-0.03, appropriate OPEO, propane diols 0.5-0.7, glycerine 0.8-0.9, butane tetracid 24-26, citric acid Amine 16-18, triethanolamine 2.5-2.7, butenoic acid 1.1-1.6, sodium hypophosphite 0.8-1, boric acid 0.25-0.3, the semi-annular jade pendant of talan two Acid derivative 2-2.5, etherification modified amino silicones 1.8-2, amido silicon oil 0.6-0.8, isomerous tridecanol polyoxyethylene ether 0.22-0.24, appropriate deionized water.
A kind of shrinkproof hydroscopic fast-drying type noniron finish liquid of shirt, is made up of following specific steps：
（1）By cetyl trimethylammonium bromide and OPEO according to mass ratio 1:2-3 mixes, and is added to deionization To being completely dissolved, wherein the mass fraction of cetyl trimethylammonium bromide is 3.2-3.5% to ultrasonic disperse, at room temperature in water It is passed through nitrogen to be stirred with the rotating speed of 1400-1600r/min, is then slowly added into octamethylcy-clotetrasiloxane, the ethene of tetramethyl four Basic ring tetrasiloxane and potassium hydroxide, rise high-temperature and obtain pre-emulsion to 80 DEG C of continuous high speed stirring 1-2h, then add Butyl acrylate, acrylic acid and acrylic acid 2- methoxy acrylates, when rising high-temperature to 80-90 DEG C, were added dropwise with the speed of 3d/s Potassium sulfate solution, successive reaction 5-8h after completion of dropwise addition is 7-8 with NaOH regulation system pH value, is filtered standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will Standby solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved （1）The product of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to mass ratio according to total raw material and deionized water：1.5 mix Conjunction stirs, and adds step（2）The product mixing and stirring of preparation obtains dressing liquid.
A kind of noniron finish method of shirt ready-made clothes, is made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved, and use liquefied ammonia using compact spinning technique + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high quality fabric high；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, by hot melt adhesive tape or lining cloth sewing at suture, then by pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid treatment：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol, The dressing liquid for descending slowly and lightly is collected by the circulatory system simultaneously and is recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate control is in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80- 105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55- 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
It is an advantage of the invention that：Shitosan as the unique positively charged native biopolymer polysaccharide of nature, due to Degradable, the good biocompatibility of Nantural non-toxic, antibiotic property are used as excellent dyeing accelerant, shrink-resistant agent, antiseptic Etc. textile process industry is widely used in, substantial amounts of hydroxyl and amino group are contained in the surface of shitosan, and bioactivity is high, are conducive to The Shrinkproof crease-resistant effect of finishing agent is improved, water insoluble due to shitosan, the present invention is using dimethylformamide as reaction Medium, N- maleylations is carried out to shitosan and is modified, and improves water-soluble, and acrylic acid ester emulsion has good film-forming property, and cohesive force is strong Advantage, be widely used, but easily become sticky at high temperature, the shortcoming that low temperature becomes fragile, fastness to wet rubbing is poor in being applied to fabric, And feel is hardened, polysiloxanes has the advantages that excellent high-low temperature resistant, compliance, smoothness, herein in compound emulsifying agent Effect is lower to utilize octamethylcy-clotetrasiloxane and t etram-ethyltetravinylcyclotetrasiloxane for monomer prepares the poly- silica of vinyl Alkane emulsion, has the advantages that good high temperature resistant, machinery, freeze thaw stability, and utilize the mode of emulsion polymerization to propylene Acid esters is emulsion modified, improves quick-drying, heat-resisting quantity, the smoothness of fabric, recycles modified shitosan colloidal sol and is modified Acrylic acid ester emulsion be compounded to form hybrid collosol, and polybasic carboxylic acid compound, in the presence of composite catalyst, what is be made is whole The enough hydroxyl reactions with cellulose of reason liquid energy, cellulosic molecule is coupled together, and forms the three-dimensional network of ester crosslinking, imparting fabric Wrinkle resistance, easy-care properties, quick-drying, the feel that improve fabric is, the strength for enhancing fabric, washability and water proofing property.
In addition the shirt ready-made clothes method for sorting that the present invention is provided avoids in convection oven drying mode to go out between different garment pieces Existing cold wave problem of non-uniform, the clothes that reduction tradition drying drying is brought winds, piles up the fold of generation and cause shirt The poor problem of outward appearance, can rapidly be cooled down to the fiber molecule that huge energy is obtained in shirt, make the crease-resistant of its acquisition Performance is solidified rapidly, reaches excellent non-ironing rank, is arranged in the wasting of resources and environmental protection for avoiding traditional water-washing method from producing While putting problem, the shirt feel after treatment is very soft, nature comfortable and easy to wear, after testing by this patent produce into Clothing, before washing water imbibition be less than or equal to 8s, washing 50 times after water imbibition within 25s, while its content of formaldehyde reaches and does not examine The basic security performance indications such as the level for going out, pH value, peculiar smell and decomposable asymmetric choice net carcinogenic aromatic amine dyestuff are up to state standards requirement, do To environmental protection, safety, noresidue, and flat appearance degree, rivel outward appearance, seam outward appearance are higher by 0.5-1 grades of national standard.Simultaneously Industrialization, streamlined, mass, the production of scale are realized, preferably economic and social benefit is reached.
The dressing liquid that the present invention is provided has good crease-resistant, non-ironing, a quick-drying effect, and keeps that fabric feeling is good, wears Comfortable advantage, additionally, the anti-crease finishing liquid safety and environmental protection, will not release formaldehyde, be harmful to human health, after treatment Shirt ready-made clothes Machine Washable, normally dry it is non-ironing, it is ultimate attainment crease-resistant indeformable, be worthy to be popularized.
Specific embodiment
The shrinkproof hydroscopic fast-drying type noniron finish liquid of a kind of shirt, by following weight portion（Kilogram）Raw material be made： Octamethylcy-clotetrasiloxane 9, t etram-ethyltetravinylcyclotetrasiloxane 1, potassium hydroxide 0.01, cetyl trimethylammonium bromide 0.32nd, butyl acrylate 15, acrylic acid 1.5, the methoxy acrylate 0.5 of acrylic acid 2, potassium peroxydisulfate 0.02, octyl phenol polyoxyethylene Appropriate ether, propane diols 0.5, glycerine 0.8, butane tetracid 24, lemon acid amide 16, triethanolamine 2.5, butenoic acid 1.1, sodium hypophosphite 0.8th, boric acid 0.25, the semi-annular jade pendant acid derivative 2 of talan two, etherification modified amino silicones 1.8, amido silicon oil 0.6, isomery ten Triol APEO 0.22, appropriate deionized water.
A kind of shrinkproof hydroscopic fast-drying type noniron finish liquid of shirt, is made up of following specific steps：
（1）By cetyl trimethylammonium bromide and OPEO according to mass ratio 1:2 mixing, are added to deionized water To being completely dissolved, wherein the mass fraction of cetyl trimethylammonium bromide is 3.2% to middle ultrasonic disperse, and nitrogen is passed through at room temperature Gas is stirred with the rotating speed of 1400r/min, is then slowly added into octamethylcy-clotetrasiloxane, t etram-ethyltetravinylcyclotetrasiloxane And potassium hydroxide, rise high-temperature and obtain pre-emulsion to 80 DEG C of continuous high speed stirring 1h, then add butyl acrylate, propylene Acid and the methoxy acrylate of acrylic acid 2, when rising high-temperature to 80 DEG C, potassium persulfate solution, completion of dropwise addition are added dropwise with the speed of 3d/s Successive reaction 5h, is 7 with NaOH regulation system pH value afterwards, is filtered standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7h at 100 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will be standby Solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved（1）Prepare Product, regulation system pH value is to 7 standby after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to mass ratio according to total raw material and deionized water：1.5 mix Conjunction stirs, and adds step（2）The product mixing and stirring of preparation obtains dressing liquid.
Case study on implementation 1：By taking 80 diclinic line shirt production as an example:
（1）Fabric is preferred：Select by 80 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 16 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 105 DEG C, preliminary drying time 90s, it is 45% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 160 DEG C, and pressing pressure is 13kg/cm2, during pressing Between 30s；
（7）Bake sizing：Baking temperature is 185 DEG C, bakes the time for 50s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 30min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 105 DEG C, the Drying and cooling time is 30min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 1 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 2：By taking 80 double flat line shirt production as an example：
（1）Fabric is preferred：Select by 80 double flat pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 17 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 100 DEG C, preliminary drying time 80s, it is 42% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 155 DEG C, and pressing pressure is 10kg/cm2, during pressing Between 26s；
（7）Bake sizing：Baking temperature is 180 DEG C, bakes the time for 30s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 25min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 75%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 100 DEG C, the Drying and cooling time is 25min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 2 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 3：By taking 100 diclinic line shirt production as an example：
（1）Fabric is preferred：Select by 100 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 19 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 95 DEG C, preliminary drying time 95s, it is 35% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 150 DEG C, and pressing pressure is 5kg/cm2, the pressing time 22s；
（7）Bake sizing：Baking temperature is 170 DEG C, bakes the time for 90s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 15min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 65%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 95 DEG C, The Drying and cooling time is 20min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 3 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 4：By taking 120 diclinic line shirt production as an example：
（1）Fabric is preferred：Select by 120 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 21 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80 DEG C, preliminary drying time 110s, it is 20% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 140 DEG C, and pressing pressure is 3kg/cm2, the pressing time 12s；
（7）Bake sizing：Baking temperature is 165 DEG C, bakes the time for 120s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 10min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 55%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90 DEG C, The Drying and cooling time is 15min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 4 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
The case study on implementation properties of product test index of table 1 and national standard contrast table
Test event National standard Case study on implementation 1 Case study on implementation 2 Case study on implementation 3 Case study on implementation 4
Flat appearance degree 3.5 4 4 4 4
Seam outward appearance 3 4 4 4 4
Rivel outward appearance 3 4 4 4 4
Content of formaldehyde ≤75 Do not detect Do not detect Do not detect Do not detect
Water imbibition before washing - 8 7 6 6
Water imbibition after 50 washings - 24 22 18 15

Claims (3)

1. the shrinkproof hydroscopic fast-drying type noniron finish liquid of a kind of shirt, it is characterised in that system is prepared by the raw material of following weight portion Into：Octamethylcy-clotetrasiloxane 9-10, t etram-ethyltetravinylcyclotetrasiloxane 1-1.5, potassium hydroxide 0.01-0.02,16 Alkyl trimethyl ammonium bromide 0.32-0.35, butyl acrylate 15-18, acrylic acid 1.5-2, acrylic acid 2- methoxy acrylates 0.5- 0.7th, potassium peroxydisulfate 0.02-0.03, appropriate OPEO, propane diols 0.5-0.7, glycerine 0.8-0.9, butane tetracid 24-26, lemon acid amide 16-18, triethanolamine 2.5-2.7, butenoic acid 1.1-1.6, sodium hypophosphite 0.8-1, boric acid 0.25-0.3, The semi-annular jade pendant acid derivative 2-2.5 of talan two, etherification modified amino silicones 1.8-2, amido silicon oil 0.6-0.8, isomery 13 Alcohol APEO 0.22-0.24, appropriate deionized water.
2. the shrinkproof hydroscopic fast-drying type noniron finish liquid of a kind of shirt according to claim 1, it is characterised in that by following tool Body step is made：
（1）By cetyl trimethylammonium bromide and OPEO according to mass ratio 1:2-3 mixes, and is added to deionization To being completely dissolved, wherein the mass fraction of cetyl trimethylammonium bromide is 3.2-3.5% to ultrasonic disperse, at room temperature in water It is passed through nitrogen to be stirred with the rotating speed of 1400-1600r/min, is then slowly added into octamethylcy-clotetrasiloxane, the ethene of tetramethyl four Basic ring tetrasiloxane and potassium hydroxide, rise high-temperature and obtain pre-emulsion to 80 DEG C of continuous high speed stirring 1-2h, then add Butyl acrylate, acrylic acid and acrylic acid 2- methoxy acrylates, when rising high-temperature to 80-90 DEG C, were added dropwise with the speed of 3d/s Potassium sulfate solution, successive reaction 5-8h after completion of dropwise addition is 7-8 with NaOH regulation system pH value, is filtered standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will Standby solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved （1）The product of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to mass ratio according to total raw material and deionized water：1.5 mix Conjunction stirs, and adds step（2）The product mixing and stirring of preparation obtains dressing liquid.
3. a kind of noniron finish method of shirt ready-made clothes, it is characterised in that be made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved, and use liquefied ammonia using compact spinning technique + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high quality fabric high；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, by hot melt adhesive tape or lining cloth sewing at suture, then by pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid treatment：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol, The dressing liquid for descending slowly and lightly is collected by the circulatory system simultaneously and is recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate control is in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80- 105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55- 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
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CN106592223A (en) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 Water-proofing, oil-proofing and antifouling type easy-care finishing liquid of shirt and finishing method of water-proofing, oil-proofing and antifouling type easy-care finishing liquid
CN106592224A (en) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 Wear-resisting ironing-free finishing liquid of shirt and finishing method of wear-resisting ironing-free finishing liquid
CN106592225A (en) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 Aromatherapy skin-protection type non-ironing finishing liquid for shirts and finishing method thereof
CN106758200A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt
CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt

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CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt
CN106758200A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt
CN108867068A (en) * 2018-06-04 2018-11-23 安徽恒益纺织科技有限公司 A kind of no-iron treatment method of clothes pure cotton product
CN108867067A (en) * 2018-06-04 2018-11-23 安徽恒益纺织科技有限公司 A kind of no-iron treatment method for chemical fiber plus material
CN108914574A (en) * 2018-07-25 2018-11-30 苏州市天翱特种织绣有限公司 A kind of preparation method of anti-wrinkle shrink-proof Silk shell fabric
CN108914574B (en) * 2018-07-25 2020-11-06 上海兆妩品牌管理有限公司 Preparation method of anti-wrinkle shrink-proof silk-woven fabric
CN109183407A (en) * 2018-08-14 2019-01-11 福建福田纺织印染科技有限公司 The preparation method of hydroscopic fast-drying shell fabric
CN111809304A (en) * 2020-07-20 2020-10-23 浙江真爱毯业科技有限公司 Bei Si Li La Chuer woollen blanket
CN111809304B (en) * 2020-07-20 2022-07-19 浙江真爱毯业科技有限公司 Bessel raschel blanket

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