CN104195830B - A kind of woolen anti-gigging-pilling agent and preparation method thereof - Google Patents
A kind of woolen anti-gigging-pilling agent and preparation method thereof Download PDFInfo
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- CN104195830B CN104195830B CN201410426102.XA CN201410426102A CN104195830B CN 104195830 B CN104195830 B CN 104195830B CN 201410426102 A CN201410426102 A CN 201410426102A CN 104195830 B CN104195830 B CN 104195830B
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Abstract
The invention provides a kind of woolen anti-gigging-pilling agent, described woolen anti-gigging-pilling agent is made up of each material of following mass fraction: ethyl acrylate: 15-20 part, polyoxyethylene octylphenyl alcohol: 15-20 part, zinc nitrate: 10-15 part, stearic acid: 5-8 part, sodium sulphate: 5-8 part, n-butanol: 2-4 part, potassium tartrate: 2-4 part, shitosan: 1-3 part, sodium dihydrogen phosphate: 2-4 part, ethanol 70-80 part, water: 320-360 part.The present invention also provides the preparation method of above-mentioned anti-gigging-pilling agent.Woolen fabric anti-fluffing and anti-pilling grade is improved more than 2 grades by woolen anti-gigging-pilling agent of the present invention, and keeps hydrophily substantially constant.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, be specifically related to a kind of woolen anti-gigging-pilling agent and preparation method thereof.
Background technology
Woolen fabric is being taken in process, due to fabric itself and the rubbing action being subject to multiple external force and the external world, before generation significantly damages, and easily generation pilling phenomenon.The pilling of fabric face, natural fabric and science fabric generally all can occur, comparatively obviously with outstanding when especially Mao Diyu hair nitrile BLENDED FABRIC makes coat.Fabric pilling impact clothing is attractive in appearance, reduces wearability.Along with growth in the living standard, the requirement of people to appearance of fabrics and wearability is also more and more higher, therefore, carries out anti-pilling finishing to fabric, improves wearing comfort and the quality of fabric, is day by day subject to the attention of domestic and international dyeing and finishing worker.
Summary of the invention
The invention provides a kind of woolen anti-gigging-pilling agent, it has good ANTIPILLING effect; For this reason, the present invention also provides its preparation method.
The woolen anti-gigging-pilling agent of one provided by the invention, described woolen anti-gigging-pilling agent is made up of each material of following mass fraction: ethyl acrylate: 15-20 part, polyoxyethylene octylphenyl alcohol: 15-20 part, zinc nitrate: 10-15 part, stearic acid: 5-8 part, sodium sulphate: 5-8 part, n-butanol: 2-4 part, potassium tartrate: 2-4 part, shitosan: 1-3 part, sodium dihydrogen phosphate: 2-4 part, ethanol 70-80 part, water: 320-360 part.
Preferably, described woolen anti-gigging-pilling agent is made up of each material of following mass fraction: ethyl acrylate: 18 parts, polyoxyethylene octylphenyl alcohol: 18 parts, zinc nitrate: 12 parts, stearic acid: 6 parts, sodium sulphate: 6 parts, n-butanol: 3 parts, potassium tartrate: 3 parts, shitosan: 2 parts, sodium dihydrogen phosphate: 3 parts, ethanol 75 parts, water: 340 parts.
Preferably, described chitosan molecule amount is 50,000, and deacetylation is 90%.
The present invention also provides the preparation method of above-mentioned woolen anti-gigging-pilling agent, and step is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 65-75 DEG C, stir 40-50min;
(2) add all the other components of proportional quantity, stir 20-30min;
(3) be cooled to normal temperature and get final product.
Woolen fabric anti-fluffing and anti-pilling grade is improved more than 2 grades by woolen anti-gigging-pilling agent of the present invention, and keeps hydrophily substantially constant.
Detailed description of the invention
Following embodiment is convenient to understand the present invention better, but does not limit the present invention.Experimental technique in following embodiment, if no special instructions, is conventional method.
embodiment 1
The formula of a kind of woolen anti-gigging-pilling agent of the present invention is as follows:
Ethyl acrylate: 18g, polyoxyethylene octylphenyl alcohol: 18g, zinc nitrate: 12g, stearic acid: 6g, sodium sulphate: 6g, n-butanol: 3g, potassium tartrate: 3g, shitosan: 2g, sodium dihydrogen phosphate: 3g, ethanol 75g, water: 340g.
The preparation method of a kind of woolen anti-gigging-pilling agent of the present invention is:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 70 DEG C, stir 45min;
(2) add all the other components of proportional quantity, stir 25min;
(3) be cooled to normal temperature and get final product.
embodiment 2
The formula of a kind of woolen anti-gigging-pilling agent of the present invention is as follows:
Ethyl acrylate: 15g, polyoxyethylene octylphenyl alcohol: 15g, zinc nitrate: 10g, stearic acid: 8g, sodium sulphate: 8g, n-butanol: 2g, potassium tartrate: 2g, shitosan: 1g, sodium dihydrogen phosphate: 2g, ethanol 70g, water: 320g.
The preparation method of a kind of woolen anti-gigging-pilling agent of the present invention is:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 65 DEG C, stir 40min;
(2) add all the other components of proportional quantity, stir 30min;
(3) be cooled to normal temperature and get final product.
embodiment 3
The formula of a kind of woolen anti-gigging-pilling agent of the present invention is as follows:
Ethyl acrylate: 20g, polyoxyethylene octylphenyl alcohol: 20g, zinc nitrate: 15g, stearic acid: 5g, sodium sulphate: 5g, n-butanol: 4g, potassium tartrate: 4g, shitosan: 3g, sodium dihydrogen phosphate: 4g, ethanol 80g, water: 360g.
The preparation method of a kind of woolen anti-gigging-pilling agent of the present invention is:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 75 DEG C, stir 50min;
(2) add all the other components of proportional quantity, stir 20min;
(3) be cooled to normal temperature and get final product.
embodiment 4
The formula of a kind of woolen anti-gigging-pilling agent of the present invention is as follows:
Ethyl acrylate: 15g, polyoxyethylene octylphenyl alcohol: 20g, zinc nitrate: 15g, stearic acid: 6g, sodium sulphate: 5g, n-butanol: 4g, potassium tartrate: 2g, shitosan: 3g, sodium dihydrogen phosphate: 4g, ethanol 70g, water: 350g.
The preparation method of a kind of woolen anti-gigging-pilling agent of the present invention is:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 72 DEG C, stir 50min;
(2) add all the other components of proportional quantity, stir 25min;
(3) be cooled to normal temperature and get final product.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a woolen anti-gigging-pilling agent, it is characterized in that: described woolen anti-gigging-pilling agent is made up of each material of following mass fraction: ethyl acrylate: 15-20 part, polyoxyethylene octylphenyl alcohol: 15-20 part, zinc nitrate: 10-15 part, stearic acid: 5-8 part, sodium sulphate: 5-8 part, n-butanol: 2-4 part, potassium tartrate: 2-4 part, shitosan: 1-3 part, sodium dihydrogen phosphate: 2-4 part, ethanol 70-80 part, water: 320-360 part.
2. woolen anti-gigging-pilling agent according to claim 1, it is characterized in that: described woolen anti-gigging-pilling agent is made up of each material of following mass fraction: ethyl acrylate: 18 parts, polyoxyethylene octylphenyl alcohol: 18 parts, zinc nitrate: 12 parts, stearic acid: 6 parts, sodium sulphate: 6 parts, n-butanol: 3 parts, potassium tartrate: 3 parts, shitosan: 2 parts, sodium dihydrogen phosphate: 3 parts, ethanol 75 parts, water: 340 parts.
3. woolen anti-gigging-pilling agent according to claim 1 and 2, is characterized in that: described chitosan molecule amount is 50,000, and deacetylation is 90%.
4. the preparation method of the woolen anti-gigging-pilling agent described in claim 1 or 2, is characterized in that: step is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 65-75 DEG C, stir 40-50min;
(2) add all the other components of proportional quantity, stir 20-30min;
(3) be cooled to normal temperature and get final product.
5. the preparation method of woolen anti-gigging-pilling agent according to claim 3, is characterized in that: step is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, zinc nitrate, n-butanol and ethanol are mixed, be heated to 65-75 DEG C, stir 40-50min;
(2) add all the other components of proportional quantity, stir 20-30min;
(3) be cooled to normal temperature and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410426102.XA CN104195830B (en) | 2014-08-27 | 2014-08-27 | A kind of woolen anti-gigging-pilling agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410426102.XA CN104195830B (en) | 2014-08-27 | 2014-08-27 | A kind of woolen anti-gigging-pilling agent and preparation method thereof |
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| CN104195830A CN104195830A (en) | 2014-12-10 |
| CN104195830B true CN104195830B (en) | 2016-04-13 |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105603760A (en) * | 2016-03-14 | 2016-05-25 | 太仓棨淂服装有限公司 | Anti-pilling finishing agent for knitted fabric and application |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2740759A (en) * | 1951-11-13 | 1956-04-03 | Ciba Ltd | Preparation for treating textile fibers and yarns |
| CN102899904A (en) * | 2012-09-05 | 2013-01-30 | 吴江涵辉纺织有限公司 | Cashmere sweater anti-pilling treatment agent |
| CN102978935A (en) * | 2012-12-04 | 2013-03-20 | 海泰纺织（苏州）有限公司 | Knitwear fleece material fluffing treating agent and method for preparing same |
| CN103243565A (en) * | 2013-05-23 | 2013-08-14 | 南通大学 | Finishing agent endowing modal knitted fabrics with antibacterial property and pilling resistance and finishing method of finishing agent |
| CN103710986A (en) * | 2013-12-02 | 2014-04-09 | 常熟市新蕾针织有限公司 | Preparation method of knitwear suede-like material pile treatment agent |
-
2014
- 2014-08-27 CN CN201410426102.XA patent/CN104195830B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2740759A (en) * | 1951-11-13 | 1956-04-03 | Ciba Ltd | Preparation for treating textile fibers and yarns |
| CN102899904A (en) * | 2012-09-05 | 2013-01-30 | 吴江涵辉纺织有限公司 | Cashmere sweater anti-pilling treatment agent |
| CN102978935A (en) * | 2012-12-04 | 2013-03-20 | 海泰纺织（苏州）有限公司 | Knitwear fleece material fluffing treating agent and method for preparing same |
| CN103243565A (en) * | 2013-05-23 | 2013-08-14 | 南通大学 | Finishing agent endowing modal knitted fabrics with antibacterial property and pilling resistance and finishing method of finishing agent |
| CN103710986A (en) * | 2013-12-02 | 2014-04-09 | 常熟市新蕾针织有限公司 | Preparation method of knitwear suede-like material pile treatment agent |
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| CN104195830A (en) | 2014-12-10 |
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Inventor after: Cai Daogui Inventor before: Zhou Min |
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| TR01 | Transfer of patent right |
Effective date of registration: 20160907 Address after: Guangyi Street dragon jade South Industrial Zone, Chenghai District of Guangdong city in Shantou province 515000 Patentee after: Chenghai Shantou victory wool weaving Co., Ltd. Address before: 214000 Jiangsu Province, Wuxi city Xishan District Yang Jian Zhen Li an Cun Xi Hu Lu Bei Patentee before: WUXI QISHENG KNITTING GLOVES FACTORY |