CN103755486B - A kind of Compound traditional Chinese medicine liquid foliar fertilizer and preparation method thereof - Google Patents
A kind of Compound traditional Chinese medicine liquid foliar fertilizer and preparation method thereof Download PDFInfo
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Abstract
A kind of Compound traditional Chinese medicine liquid foliar fertilizer and preparation method thereof, utilize the tuber of pinellia of herbal medicine, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., euphorbia fischeriana, Artemisia scoparia, three kinds or more formula in month root of langdu and acid solvent agent boric acid tri butyl ester thereof, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, vialidon, three kinds or more in zinc sulfate is filled a prescription 100 DEG C of hot water mixing solutionss, by soaking, grind slurrying, filter, the compound Chinese herb foliar nutrient that clarification process is produced.The present invention is a kind of botanical pesticide fertilizer, has the toxic effect composition of organic insecticidal sterilization and the composite fluid preparation of acidotrophy element fertilizer.
Description
Technical field
The invention belongs to technical field of fertilizers, relate to and a kind ofly prevent and treat plant pest and the Compound traditional Chinese medicine liquid foliar fertilizer of tool nutrition and manufacture craft.
Background technology
For many years, along with the raising of farm output, the application quantity of chemical fertilizer, agricultural chemicals strengthens, and its residual quantity on farm crop, also in increasing, causes environmental pollution and people and animals are acute or the potential hazard of chronic poisoning is difficult problem agriculture production being badly in need of will solve or will solve for a long time.In recent years, along with continuing to optimize of the structure of agricultural production, green agricultural product area constantly increases, agriculture production technology improves constantly, agricultural product quality standard constantly promotes, greatly developing green safety agricultural-food is targets that our National agricultural is produced, reduce the consumption of chemical fertilizer and chemical pesticide, the height poison of restriction chemical fertilizer and chemical pesticide, the kind of high residue and using method and use range are applied in the standardized production of development green agricultural product, open up the main task that environment-friendly and green agrochemical fertilizer product is related industries technician.The effect that foliar nutrient only has its supplementary plant nutrition is generally applied in current agriculture production; namely use even if also just namely join with sterilant or sterilant compound; and chemical composition residual quantity is high has potential threat to people and animals are healthy; the Remixed agent of some medicine fertilizer simultaneously, production process equipment is loaded down with trivial details, has both needed the equipment producing fertilizer as tablets press dryer etc.; also will the equipment of production Liquid traditional Chinese medicine; this will consume mass energy, and its facility investment is also large, is that medium-sized and small enterprises can not bear.
In addition, how reaching Traditional Chinese medicine fertilizer unification is also the difficult problem that professional person will solve and pay close attention to always.Herbal medicine is the rarity of China's traditional Chinese medical science, its natural resources is extensive, utilize herbal control plant pest to develop simultaneously with the fertilizer application of supplementary plant nutrition simultaneously, can reach and gather materials on the spot, ecological safety, the object of environmental protection is the important content of current national development environment friendly agricultural, green fertilizer.Utilize have local resources extensive, easily to get and preventing disease pest control strengthens the hypertoxicity of plant immunization effective herbal medicine and in high-temperature hot water acidic solution, easily extracts the active high characteristic of virulence, Compound traditional Chinese medicine liquid foliar fertilizer is made as solvent agent with the acidotrophy preparation of industry, medicine, agriculturally widespread use, thus there is raw material easily obtain, utilize waste material weeds poisonous in productive life, the best Chinese herbal medicine formula of research trial, belong to botanical pesticide fertilizer, refuse reclamation, production technique are easy, fertilizer drug effect is high, the innovation of environmental protection.
Summary of the invention
The object of the invention is for developing agricultural green agricultural product, open up botanical pesticide fertilizer, enforcement environment protective plant protecting, environment friendly agricultural fertilizer provide one to have efficient ecological safety and environmental protection, and production technique is simple, does not need Traditional Chinese medicine fertilizer new variety and the making method of complex apparatus.The object of this invention is to provide and a kind ofly prevent and treat plant pest and the Compound traditional Chinese medicine liquid foliar fertilizer of tool nutrition and manufacture craft.
For achieving the above object, the technical solution used in the present invention is:
A kind of Compound traditional Chinese medicine liquid foliar fertilizer, is characterized in that comprising following raw material is made:
Herbal medicine: the tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., the three kinds or more in euphorbia fischeriana, Artemisia scoparia, the moon root of langdu; Described herbal medicine is the tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., the dry root medicine materical crude slice of the three kinds or more in euphorbia fischeriana, Artemisia scoparia, the moon root of langdu or dry herb; Weight proportion between herbal raw material is 1:0.8 ~ 1.2;
Acidotrophy fertilizer as solvent agent: comprise boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, the three kinds or more saturated hot-water solution in ammonium sulfate, zinc sulfate; Utilize boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, the potassium primary phosphate of acidotrophy fertilizer, the mixed solution of the saturated hot-water solution of ammonium sulfate, zinc sulfate, as solvent agent, grinds the technique acquisition Chinese medicine of soya-bean milk and the fertile slurries body of herbal mixture of fertilizer by tradition;
The described acidic fertilizier as solvent agent is boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, the concentration of the saturated hot-water mixed solution of the three kinds or more in ammonium sulfate, zinc sulfate is 70% ~ 80%, and the weight ratio of herbal medicine and solvent agent fertilizer is 1:2 ~ 11.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: described composition of raw materials is calculated by weight to:
Herbal medicine gross weight 50 ㎏, fills a prescription as the tuber of pinellia dry root medicine materical crude slice 10 ㎏; The root of langdu dry root medicine materical crude slice 10 ㎏; Rumex patientia Linn. dry root medicine materical crude slice 10 ㎏; Taraxacum dry root medicine materical crude slice 10 ㎏; Herba daturae 10 ㎏;
Solvent agent gross weight 100 ㎏, formula is 100 DEG C of hot water 60 ㎏; Sterilization crystallizing sulfanilamide 0.1 ㎏; Niflumic acid 0.05 ㎏; Potassium primary phosphate 35 ㎏; Selenous acid 0.1 ㎏; Zinc sulfate 4.75 ㎏;
Composition of raw materials product herbal medicine is 1:8 with the gross weight ratio of solvent agent; Herbal medicine amounts to 50 ㎏, wherein: the tuber of pinellia dry root medicine materical crude slice 10 ㎏; The root of langdu dry root medicine materical crude slice 10 ㎏; Rumex patientia Linn. dry root medicine materical crude slice 10 ㎏; Taraxacum dry root medicine materical crude slice 10 ㎏; Herba daturae 10 ㎏, than solvent agent 100 DEG C of hot water mixing solutions 400 ㎏; The formulation by weight ratio of mediator is 100 DEG C of hot water 239 ㎏; Sterilization crystallizing sulfanilamide 0.4 ㎏; Niflumic acid 0.2 ㎏; Potassium primary phosphate 140 ㎏; Selenous acid 0.4 ㎏; Zinc sulfate 20 ㎏; First medium-height grass pharmaceutical media agent 100 ㎏ is soaked, first time defibrination solvent agent 200 ㎏; Second time defibrination solvent agent 100 ㎏.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: described raw material herbal medicine and solvent agent prescription are counted by product weight:
Herbal medicine is 1:9 with the gross weight ratio of solvent agent; Herbal medicine amounts to 50 ㎏, wherein: Herba Artemisiae annuae dry herb 10 ㎏, wolf tail grass dry herb 12 ㎏, the root of langdu dry root medicine materical crude slice 8 ㎏, taraxacum dry herb 10 ㎏, thorn apple dry herb 10 ㎏; Than solvent agent hot water mixing solutions 450 ㎏, its solvent agent weight ratio is filled a prescription: be 100 DEG C of hot water 270 ㎏; Boric acid tri butyl ester 0.45 ㎏; Sulindac 0.225 ㎏; Potassium primary phosphate 157.5 ㎏; Sodium Selenite 0.45 ㎏; Zinc sulfate 21.375 ㎏; Soak with solvent agent 150 ㎏; First time defibrination solvent agent 200 ㎏; Second time defibrination solvent agent 100 ㎏.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: described raw material herbal medicine and solvent agent prescription are 1:10 by gross weight ratio; Herbal medicine amounts to 50 ㎏; Calamus dry herb 9 ㎏, Herba Ixeritis chinensis dry herb 8 ㎏, Herba Artemisiae Scopariae dry herb 11 ㎏, setose thistle dry herb 11 ㎏, Herba Artemisiae annuae dry herb 11 ㎏ in formula; Than solvent agent hot water mixing solutions 500 ㎏, solvent agent weight ratio is 100 DEG C of hot water 300 ㎏; Methyl salicylate 0.5 ㎏; Niflumic acid 0.25 ㎏; Potassium primary phosphate 175 ㎏; Sodium Selenite 0.5 ㎏; Zinc sulfate 22.75 ㎏; Soak with solvent agent 200 ㎏; First time defibrination solvent agent 200 ㎏; Second time defibrination solvent agent 100 ㎏.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: raw material herbal medicine and solvent agent prescription product gross weight are than being 1:11; Herbal medicine amounts to 50 ㎏, and formula is crowndaisy chrysanthemum dry herb 10 ㎏, Artemisia scoparia dry herb 11 ㎏, Szechwan Chinaberry Fruit dry fruit 10 ㎏, the root of langdu dry root medicine materical crude slice 10 ㎏, wolf tail grass dry herb 9 ㎏; Than solvent agent hot water mixing solutions 550 ㎏, solvent agent formulation by weight is 100 DEG C of hot water 330 ㎏; Methyl salicylate 0.55 ㎏; Ethyl acetate 0.275 ㎏; Potassium primary phosphate 192.5 ㎏; Boric acid tri butyl ester 0.55 ㎏; Zinc sulfate 26.125 ㎏; Soak with solvent agent 200 ㎏; First time defibrination solvent agent 300 ㎏; Second time defibrination solvent agent 50 ㎏.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: described raw material herbal medicine and solvent agent prescription are 1:10 by gross weight ratio; Wherein: Herba Potentillae Chinensis dry herb 12 ㎏, Herba Ixeritis chinensis dry herb 8 ㎏, Herba Artemisiae Scopariae dry herb 11 ㎏, setose thistle dry herb 10 ㎏, Herba Artemisiae annuae dry herb 9 ㎏; Than solvent agent hot water mixing solutions 500 ㎏; Soak with solvent agent 200 ㎏; First time defibrination solvent agent 200 ㎏; Second time defibrination solvent agent 100 ㎏; Solvent agent formulation by weight is 100 DEG C of hot water 300 ㎏; Methyl salicylate 0.5 ㎏; Niflumic acid 0.25 ㎏; Potassium primary phosphate 175 ㎏; Sodium Selenite 1.5 ㎏; Zinc sulfate 22.75 ㎏.
According to described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: described raw material herbal medicine and solvent agent prescription are 1:10 by product gross weight ratio; The dry herb of Herba Potentillae Chinensis, the dry herb of Herba Ixeritis chinensis, the dry herb of Herba Artemisiae Scopariae, the dry herb of setose thistle, each 10 ㎏ of the dry herb of Herba Artemisiae annuae, amount to 50 ㎏ than solvent agent hot water mixing solutions 500 ㎏; Solvent agent formulation by weight is 100 DEG C of hot water 300 ㎏; Methyl salicylate 1.5 ㎏; Niflumic acid 0.25 ㎏; Potassium primary phosphate 155 ㎏; Sodium Selenite 0.5 ㎏; Zinc sulfate 42.75 ㎏; Soak with solvent agent 200 ㎏; First time defibrination solvent agent 200 ㎏; Second time defibrination solvent agent 100 ㎏.
Make a method for described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that comprising the following steps:
(1) soak: by the herbal medicine tuber of pinellia, Herba Potentillae Chinensis, setose thistle, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., euphorbia fischeriana, Artemisia scoparia, the dry root medicine materical crude slice of the three kinds or more in month root of langdu or dry herb, use boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, the concentration of the hot water saturated solution of the solvent agent of zinc sulfate three kinds or more be 70% ~ 80% mixing solutions soak 24 hours for subsequent use, the weight ratio of the dry root medicine materical crude slice of compound Chinese herb and nutritious fertilizer is 1:2 ~ 2.5,
(2) slurrying is ground totally 2 times: the ratio defibrination equaling 1:4 ~ 6 according to the formula Chinese herbal of soaking than solvent agent, slurrying is ground with mill beans slag-removing device, the formula Chinese herbal of soaking equaled 1:4 than solvent agent and ground the dregs of a decoction squeezed out first time, equal 1:2 ~ 3 according to the dregs of a decoction than solvent agent again to mix thoroughly, continue to squeeze and once starch, defibrination particle diameter is 1 ~ 100 micron;
(3) filter.First filter cloth 100 ~ 200 order pressing plate coarse filtration is made with non-woven fabrics by grinding the compound Chinese herb fertilizer solution slurry squeezed; And then use liquid medicine filter circular impact screen, sieve the thinnest to 0.028mm, filter most I to 5 micron, fill the screen cloth of 1 ~ 5 layer of different meshes, sorting or filtration are carried out to the material of 2 ~ 6 grades simultaneously.Filtering accuracy: 5 ~ 100 microns; Make the compound medicines solution body containing herbal medicine and fertilizer and herbal mixture fertilizer liquid.
(4) centrifugal clarification: adopt high speed tubular-bowl centrifuge to carry out centrifugal clarification, extract some albumen in medical fertilizer liquid body, pectin, polysaccharide, saponin and some insoluble fluid impurity and fine particle etc., whizzer separating factor 15000, being separated smallest particles is 0.5 micron, collects clarified liq and medical fertilizer liquid body finished product.
According to the making method of described Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: proportioning raw materials is calculated as by product weight:
Herbal raw material gross weight 50 ㎏, wherein: the tuber of pinellia dry root medicine materical crude slice 10 ㎏; The root of langdu dry root medicine materical crude slice 10 ㎏; Rumex patientia Linn. dry root medicine materical crude slice 11 ㎏; Taraxacum dry root medicine materical crude slice 11 ㎏; Herba daturae 8 ㎏;
Solvent agent gross weight 100 ㎏: solvent agent is 100 DEG C of hot water 60 ㎏; Sterilization crystallizing sulfanilamide 0.1 ㎏; Niflumic acid 0.05 ㎏; Potassium primary phosphate 35 ㎏; Selenous acid 0.1 ㎏; Zinc sulfate 4.75 ㎏;
Herbal raw material is 1:8 with the gross weight ratio of solvent agent;
Herbal raw material gross weight 50 ㎏, wherein: the tuber of pinellia dry root medicine materical crude slice 10 ㎏; The root of langdu dry root medicine materical crude slice 10 ㎏; Rumex patientia Linn. dry root medicine materical crude slice 11 ㎏; Taraxacum dry root medicine materical crude slice 11 ㎏; Herba daturae 8 ㎏; Than solvent agent 100 DEG C of hydrothermal solution mixed solution 400 ㎏, the formulation by weight ratio of solvent agent is 100 DEG C of hot water 239 ㎏, sterilization crystallizing sulfanilamide 0.4 ㎏, niflumic acid 0.2 ㎏, potassium primary phosphate 130 ㎏, selenous acid 0.4 ㎏, zinc sulfate 30 ㎏; First medium-height grass pharmaceutical media agent 100 ㎏ is soaked, first time defibrination solvent agent 200 ㎏, second time defibrination solvent agent 100 ㎏;
Concrete technology making step is as follows:
(1) soak; Herbal medicine and solvent agent weight ratio: herbal medicine gross weight 50 ㎏, wherein: the tuber of pinellia dry root medicine materical crude slice 10 ㎏; The root of langdu dry root medicine materical crude slice 10 ㎏; Rumex patientia Linn. dry root medicine materical crude slice 11 ㎏; Taraxacum dry root medicine materical crude slice 11 ㎏; Herba daturae 8 ㎏; Than solvent agent hot water mixing solutions consumption 100 ㎏, soak 24 hours;
(2) grind liquid slurry altogether secondary: herbal medicine and solvent agent weight ratio: the impregnated formula Chinese herbal tuber of pinellia of use solvent agent, the root of langdu, Rumex patientia Linn., taraxacum, Herba daturae totally 150 ㎏ than solvent agent formulation by weight than 200 ㎏, again grind hot water mixing solutions 100 ㎏ that the coarse filtration dregs of a decoction that liquid slurry first time grinds slurries add above solvent agent again, grind secondary slurries, namely the slurrying liquid mixing of twice obtains raw product herbal medicine fertilizer solution slurry;
(3) filter: comprise two-step process: one is coarse filtration mistake, filter grinding the liquid slurry plate-and-frame filter press squeezed, filter cloth 100 ~ 200 order pressing plate coarse filtration made by lint-free non-woven fabrics, and the material of some macrobeads, thickness is removed; Two is adopt circular impact screen, sieves the thinnest to 500 orders or 0.028mm, filters most I to 5 micron, fill the screen cloth of 1 ~ 5 layer of different meshes, carry out sorting or filtration simultaneously to the material of 2 ~ 6 grades.Filtering accuracy: 5 ~ 100 microns;
(4) clarify: filtrate after filtration adopts high speed tubular type centrifuge, rotating speed 16000r/h, diameter 105mm, power 3kw, centrifugal go out relative density of medicine liquid 1.07, make the fertile clarified liq head product of herbal medicine.
Tool of the present invention has the following advantages:
1, the present invention is a kind of botanical pesticide fertilizer, has the toxic effect composition of organic insecticidal sterilization and the composite fluid preparation of acidotrophy element fertilizer.Its technique utilizes the pesticide-germicide effective constituent of herbal medicine in hot acid solution, easily divide the principle parsed, then through the hot acid aqueous solution soaking of solvent agent, the liquid preparation of production of milling, filter, be separated, clarify.The toxic effect composition that the present invention to utilize in the dry heel piece of poisonous Chinese herbal medicine formula or herb contained sterilization to control worm soaks with acid solvent agent prescription mixed hot water solution process, mill, filter, separating clarifying produces Liquid traditional Chinese medicine foliar nutrient product.The single trophicity that it changes conventional foliage fertilizer is the multifunctionality of disease-resistant sterilization and disinsection, and solving existing foliage fertilizer product technology only has the trophic function of fertilizer without the shortcoming of desinsection disease cure function, achieves the environmental protection object of botanical pesticide fertilizer.The present invention makes, and " fertilizer " combines with " herbal medicine "; Crop alimentary combines with the ecological, environmental protective of preventing disease pest control, increases the security of plant and farm environment, makes fertilising and prevention and elimination of disease and pests in one, saves man-hour, saves labour, and reaching applies fertilizer cures the disease the multiple-effect function of disease-resistant resistance to sick desinsection.Add security and the feature of environmental protection of agrochemical fertilizer use simultaneously, improve long-lasting and the high efficiency of fertilizer and agricultural chemicals.This product herbal medicine material is the injurious weed on deserted mountain, can turn waste into wealth.
This products production manufacture craft simply only needs four step programs, equipment is simple, improve the both effectiveness of productive labor and energy saving, improve the security of plant, thoroughly eliminate the residual hazard of agrochemical fertilizer, realizing innovation and the creation of botanical pesticide fertilizer, for product innovation created by development environment friendly agricultural fertilizer, providing technical support for producing green agricultural product, for agricultural produce, the excellent creation good basis of agricultural product quality.
2, the physicochemical property of this Chinese medicinal liquor fertilizer are in acid.Be the physico-chemical property utilizing the virulence composition of its Chinese medicine easily to dissolve in hot water acidic solution, its toxic effect composition is extracted, be dispersed in the Traditional Chinese medicine fertilizer of the liquid form made in the medium of suitable acid compound water.Have the medium of Chinese medicine antibacterial desinsection and acute toxicity, the nutritive ingredient that its plant needs is high effective constituent > 70% such as () phosphorus, potassium, zinc, and stable chemical nature is odorless, tasteless, without residual hazard, soluble in water, does not lump.
3, the medicine in Liquid traditional Chinese medicine fertilizer disperses in media as well with molecularity or graininess, thus the liquid medicine forming homogeneous phase is fertile.Herbal medicine toxic effect particle dispersion in liquid medicine fertilizer even, liquid phase stability good and toxic side effect is little.The dispersity of medicine is large, absorbs fast, compares can play drug effect more rapidly with corresponding solid dosage, improve the bioavailability of medicine;
4, production technique is simple, and do not need complex apparatus, processing charges is only 1/10th of general liquid fertilizer and Chinese medicine preparation, greatly can reduce production cost, can also save a large amount of fuel energy.
5, there is effect plant sterilization being controlled to worm and supplementary plant nutrition.Utilize the effect having on plant leaf surface and supplement the nutrients and prevent and treat plant pest, can for the foliar spray of plant, soil foliage top dressing or seed soaking, fill with root, rushing of day-light greenhouse fruits and vegetables is executed and drip irrigation etc.
6, belong to the free from chloride Traditional Chinese medicine fertilizer of ecological organic safety, use range is extensive.
This product expression goes out significant effect of increasing production and improves crop quality, the various resistance of enhancing crop, for farm crop base fertilizer and middle and later periods foliage application, be applicable to various crop such as various grain, cash crop and melon and fruit, vegetables etc., for some fear-chlorion crops, it shows better effect.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described:
A kind of Compound traditional Chinese medicine liquid foliar fertilizer of the present invention, its composition comprises:
Herbal medicine: the tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., the three kinds or more in euphorbia fischeriana, Artemisia scoparia, the moon root of langdu; Acidotrophy fertilizer comprises boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, the three kinds or more saturated hot-water solution in ammonium sulfate, zinc sulfate.Its special feature is: the boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, the potassium primary phosphate that utilize acidotrophy fertilizer, the mixed solution of the saturated hot-water solution of ammonium sulfate, zinc sulfate, as solvent agent, grinds the technique acquisition Chinese medicine of soya-bean milk and the fertile slurries body of herbal mixture of fertilizer by tradition.
Herbal medicine described in above-mentioned Compound traditional Chinese medicine liquid foliar fertilizer is the tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., the dry root medicine materical crude slice of the three kinds or more in euphorbia fischeriana, Artemisia scoparia, the moon root of langdu or dry herb; Weight proportion between herbal raw material is 1:0.8 ~ 1.2;
Acidic fertilizier as solvent agent is boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, the concentration of the saturated hot-water mixed solution of the three kinds or more in ammonium sulfate, zinc sulfate is 70% ~ 80%, and the weight ratio of herbal medicine and solvent agent fertilizer is 1:2 ~ 11.
Making method of the present invention is as follows:
A kind of making method of Compound traditional Chinese medicine liquid foliar fertilizer, it is characterized in that: its formula composition comprises the herbal medicine tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., euphorbia fischeriana, Artemisia scoparia, three kinds or more in month root of langdu, respectively with 100 DEG C of hot water dissolving's boric acid tri butyl esters, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, the concentration of the saturated mixed solution of hot water of the three kinds or more in zinc sulfate is 70% ~ 80%, as the solvent agent of extracting Chinese medicine toxic effect composition, the weight ratio of herbal medicine and solvent agent fertilizer is 1:2 ~ 11.
The manufacturing process steps of its production method is:
1, the raw material of herbal medicine and fertilizer prepares.
By quality standard and the agricultural commodity fertilizer standard of the dry root medicine materical crude slice of herbal medicine of " Chinese Pharmacopoeia ", get ready and prepare enough the qualified herbal medicine tuber of pinellia, setose thistle, Herba Potentillae Chinensis, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., euphorbia fischeriana, Artemisia scoparia, the moon root of langdu etc.; Acid solvent agent nutritious fertilizer is boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, zinc sulfate etc.
2, soak.By the herbal medicine tuber of pinellia, Herba Potentillae Chinensis, setose thistle, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., euphorbia fischeriana, Artemisia scoparia, the dry root medicine materical crude slice of the three kinds or more in month root of langdu or dry herb, use boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, the concentration of the hot water saturated solution of the solvent agent of zinc sulfate three kinds or more be 70% ~ 80% mixing solutions soak 24 hours for subsequent use.During immersion, the weight ratio of the dry root medicine materical crude slice of compound Chinese herb and nutritious fertilizer is 1:2 ~ 2.5.
3, filter pulp is ground.Equal the ratio defibrination of 1:4 ~ 6 than the mixed hot water solvent agent of 70% ~ 80% concentration according to the formula Chinese herbal of soaking, slurrying is ground with mill beans slag-removing device, first time grinds the dregs of a decoction squeezed out, equal 1:2 ~ 3 according to the dregs of a decoction than the mixed hot water solvent agent of 70% ~ 80% concentration again to mix thoroughly, continue to squeeze and once starch, defibrination particle diameter is 1 ~ 100 micron.
4, filter.First filter cloth 100-200 order pressing plate coarse filtration is made with non-woven fabrics by grinding the compound Chinese herb fertilizer slurries squeezed; And then with liquid medicine filter, " capable DL " serial circular impact screen, sieves the thinnest to 0.028mm, filters most I to 5 micron, fills the screen cloth of 1 ~ 5 layer of different meshes (fineness), carry out sorting or filtration to the material of 2 ~ 6 grades simultaneously.Filtering accuracy: 5 ~ 100 microns.Make the compound medicines solution body containing herbal medicine and fertilizer and herbal mixture fertilizer liquid.
5, centrifugal clarification.GQ105R type high speed tubular-bowl centrifuge is adopted to carry out centrifugal clarification, extract some albumen in medical fertilizer liquid body, pectin, polysaccharide, saponin and some insoluble fluid impurity and fine particle etc., whizzer separating factor 15000, being separated smallest particles is 0.5 micron, collects clarified liq and the elementary finished product of herbal mixture solution body.
6, the elementary finished product of herbal mixture solution body, loads large tank and enters head product storehouse.
7, finished product and quality examination.
The herbal medicine adopting this manufacture craft to produce and the compound liquid of fertilizer and herbal mixture fertilizer just finished product, detects with acidometer (PHS-2 type), the pH value of this Traditional Chinese medicine fertilizer compound fluid and density, this liquid is in acid, pH value is 5.04, and pH value range is 4.6 ~ 5.6, and density is 1.07, utilize gas chromatography determination, its compound fluid is also containing the tuber of pinellia, Herba Potentillae Chinensis, setose thistle, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, the flavonoid that the herbal medicine such as the root of langdu have, coumarins, diterpenes, triterpenes, organic and the Inorganic chemical composition of the antibacterial insecticidal actions such as lignanoids and cinnamic acid alcohol glycoside, determining general flavone content is 1.77%, total acidic component content is 1.57%, polysaccharide content is 25.6%, contents of monosaccharides is 1.35%, (comprise glucose, fructose and sucrose and polysaccharide) and containing much starch and fiber, measure in this herbal mixture solution body also containing KH
2pO
4(in acid anhydride base) 27% ~ 40% or ZnSO
2the content of 9 kinds of metallic elements such as 0.5%, Ca, Mg, Pb, Cu, Zn, Cd, Fe, Mn totally 5%.
8, pouring liquid and packaging.High-precision liquid pouring package machine is adopted to carry out finished product production.The whole processes such as this mechanical bag, filling, involution, printing lot number, cut-out, counting complete automatically, Microprocessor S3C44B0X, and accurate positioning is reliable, and liquid product takes the plastic bottle packing of compound film bag packaging or 20 ~ 50 milliliters.
Below this Chinese medicinal liquor fertilizer and making method are described in detail:
Principle of work of the present invention is: adopt the toxic effect composition in acid solvent pickling process extraction herbal medicine.Utilize acidic fertilizier as the solvent agent of extracting herbal medicine toxic active ingredient, according to the dissolving properties of toxic effect composition in the acid solvent of high temperature in herbal medicine, select the characteristic large to toxic active ingredient solubleness, and effective constituent is dissolved out in the tissue of medicinal material.When high-temperature acidic solvent be added in the dry root medicine materical crude slice (herb) of herbal medicine due to the diffusion of solvent, osmosis dissolve effective constituent, make high temperature volatile and be dissolved in acid or organic acid combine component separating out.Not chemical transformation in chemical composition.Moisture contained by Liquid traditional Chinese medicine fertilizer is also the solvent being separated or dissolving herbal medicine toxic active ingredient simultaneously.
Fabrication processing:
Select materials and adopt the herbal medicine tuber of pinellia, Rumex patientia Linn., thorn apple, Szechwan Chinaberry Fruit, Herba Artemisiae annuae, wolf tail grass, Chang Pu, Herba Bidentis Bipinnatae, Herba Ixeritis chinensis, taraxacum, Herba Artemisiae Scopariae, Stellera chamaejasme L., the three kinds or more dry root medicine materical crude slice in euphorbia fischeriana, Artemisia scoparia, setose thistle, the moon root of langdu etc. or dry herb, acid solvent agent is boric acid tri butyl ester, selenous acid, Sodium Selenite, wintergreen oil, sterilization crystallizing sulfanilamide, niflumic acid, ethyl acetate, sulindac, potassium primary phosphate, ammonium sulfate, the saturated mixing solutions concentration of three kinds or more hot water of zinc sulfate is 70% ~ 80%, soak formula Chinese herbal 24 hours → grind slurrying continuous quadratic → filtration (2 ~ 100 microns) → separating clarifying (0.5-10 micron) → carry out efficiency light spectrometer and chemical physical property detection → pouring liquid and finished product packing → product warehousing → market development to head product quality to sell
Below in conjunction with example, technological process is described in detail.
embodiment 1
Raw material herbal medicine and solvent agent prescription are calculated as by product weight:
Herbal medicine gross weight 50 ㎏, fills a prescription as the dry root medicine materical crude slice of the tuber of pinellia dry root medicine materical crude slice 10 ㎏+root of langdu dry root medicine materical crude slice 10 ㎏+Rumex patientia Linn. dry root medicine materical crude slice 10 ㎏+taraxacum 10 ㎏+Herba daturae 10 ㎏;
Solvent agent gross weight 100 ㎏, formula is 100 DEG C of hot water 60 ㎏+sterilization crystallizing sulfanilamide 0.1 ㎏+niflumic acid 0.05 ㎏+potassium primary phosphate 35 ㎏+selenous acid 0.1 ㎏+zinc sulfate 4.75 ㎏.
Herbal medicine is 1:8 with the gross weight ratio of solvent agent;
Herbal medicine amounts to 50 ㎏ (wherein the dry root medicine materical crude slice of the tuber of pinellia dry root medicine materical crude slice 10 ㎏+root of langdu dry root medicine materical crude slice 10 ㎏+Rumex patientia Linn. dry root medicine materical crude slice 10 ㎏+taraxacum 10 ㎏+Herba daturae 10 ㎏) than solvent agent 100 DEG C of hydrothermal solution mixed solution 400 ㎏ (the formulation by weight ratio of solvent agent is 100 DEG C of hot water 239 ㎏+sterilization crystallizing sulfanilamide 0.4 ㎏+niflumic acid 0.2 ㎏+potassium primary phosphate 140 ㎏+selenous acid 0.4 ㎏+zinc sulfate 20 ㎏), first soaks medium-height grass pharmaceutical media agent 100 ㎏+first time defibrination solvent agent 200 ㎏+second time defibrination solvent agent 100 ㎏);
Concrete technology making step is as follows:
(1) soak.Herbal medicine and solvent agent weight ratio: Chinese herbal medicine formula is that the tuber of pinellia dry root medicine materical crude slice+root of langdu dry root medicine materical crude slice+Rumex patientia Linn. dry root medicine materical crude slice+taraxacum dry root medicine materical crude slice+Herba daturae (each 10 ㎏) amounts to 50 ㎏ than solvent agent hot water mixing solutions consumption 100 ㎏, solvent agent formulation by weight ratio be 100 DEG C of hot water 60 ㎏+sterilization crystallizing sulfanilamide 0.1 ㎏+niflumic acid 0.05 ㎏+potassium primary phosphate 35 ㎏+selenous acid 0.1 ㎏+zinc sulfate 4.75 ㎏ soak 24 little time.
(2) defibrination, comprises twice.Herbal medicine and solvent agent weight ratio: the impregnated formula Chinese herbal tuber of pinellia+root of langdu+Rumex patientia Linn.+taraxacum+Herba daturae of use solvent agent totally 150 ㎏, than solvent agent weight 200 ㎏ that fills a prescription, is 100 DEG C of hot water 120 ㎏+sterilization crystallizing sulfanilamide 0.2 ㎏+niflumic acid 0.1 ㎏+potassium primary phosphate 70 ㎏+selenous acid 0.2 ㎏+zinc sulfate 9.5 ㎏ and grinds liquid processed slurry.Secondary slurrying is hot water mixing solutions 100 ㎏ (instant mediator formulation by weight is 100 DEG C of hot water 60 ㎏+sterilization crystallizing sulfanilamide 0.1 ㎏+niflumic acid 0.05 ㎏+potassium primary phosphate 35 ㎏+selenous acid 0.1 ㎏+zinc sulfate 4.75 ㎏) the filter dregs of a decoction grinding slurries for the first time being added again above solvent agent, grind secondary slurries, namely the slurrying liquid mixing of twice obtains raw product herbal medicine fertilizer slurries.
(3) filter.Comprise two-step process
One is coarse filtration mistake, and filter grinding the liquid slurry plate-and-frame filter press squeezed, filter cloth 100 ~ 200 order pressing plate coarse filtration made by lint-free non-woven fabrics, and the material of some macrobeads, thickness is removed; Two is adopt " capable DL " serial circular impact screen, sieves the thinnest to 500 orders or 0.028mm, filters most I to 5 micron, fill the screen cloth of 1 ~ 5 layer of different meshes (fineness), carry out sorting or filtration simultaneously to the material of 2 ~ 6 grades.Filtering accuracy: 5 ~ 100 microns.
(4) clarify.Filtrate after filtration adopts GQ105R type high speed tubular type centrifuge (rotating speed 16000r/h, diameter 105mm, power 3kw), centrifugal go out relative density of medicine liquid 1.07, make the fertile clarified liq head product of herbal medicine.
The technical parameter of said herbal medicine liquid foliage fertilizer:
1, appearance color: brown light yellow transparent liquid
2, relative density: the density 1.07kg/L(liter of liquid).
3, pH value: PH4.6 ~ 5.04; Meet 3.5 ~ 8 of GB.
4, solubleness: insolubles content 0.1% in solution; 5% of symbol GB.
5, stability: by herbal mixture solution body under simulation commercially available back condition, put in room temperature, after carrying out the primary stability examination of 24 hours, 48 hours, 72 hours; Proceed to examine once for 1,2,3 month, then every half a year once again; Preserve in 37 ~ 40 DEG C and relative humidity 75%, monthly examine once, continuous three months) stability assessment result, this compound Chinese herb solution body preparation good stability, stablizes and within 3 months, occurs that minute quantity precipitates, but after shake, resolution of precipitate, does not affect drug effect quality, does not belong to rotten.
6, assay: utilize high performance liquid chromatography and chemical property determination, this Traditional Chinese medicine fertilizer contains main chemical compositions flavonoid, coumarins, lignanoids, diterpenes, sterol and amino acid etc. in root of Stellera chamaejasme, total flavonoid component content 1.77%, total acidic component content 1.57%, furoeoumarin lactone content 0.5%; Also containing the K in potassium dihydrogen phosphate
2o content is more than or equal to 27%, P
2o
5be more than or equal to 40%; Hydrocarbon polymer is more than or equal to 15.5%, middle and trace element 9.5% and organic and inorganic chemical composition 4.16%.
embodiment 2
Raw material herbal medicine and solvent agent prescription are counted by product weight: herbal medicine and solvent agent gross weight are than being 1:9; Formula Chinese herbal gross weight 50 ㎏ (wherein, the dry herb of Herba Artemisiae annuae 10 ㎏+wolf tail grass dry herb 12 ㎏+root of langdu dry root medicine materical crude slice 8 ㎏+taraxacum dry herb 10 ㎏+thorn apple dry herb 10 ㎏) than solvent agent hot water mixing solutions 450 ㎏ (solvent agent weight ratio formula is 100 DEG C of hot water 270 ㎏+boric acid tri butyl ester 0.45 ㎏+sulindac 0.225 ㎏+potassium primary phosphate 157.5 ㎏+Sodium Selenite 0.45 ㎏+zinc sulfate 21.375 ㎏), immersion solvent agent 150 ㎏+first time defibrination solvent agent 200 ㎏+second time defibrination solvent agent 100 ㎏); Other operating process are with embodiment 1.
embodiment 3
Raw material herbal medicine and solvent agent prescription are counted by product weight: herbal medicine and solvent agent gross weight are than being 1:10; Herbal medicine gross weight 50 ㎏ (wherein, crowndaisy chrysanthemum dry herb 11 ㎏, + Artemisia scoparia dry herb 10 ㎏, + Szechwan Chinaberry Fruit (dry fruit) 8 ㎏, + the root of langdu dry root medicine materical crude slice 10 ㎏, + Herba Artemisiae annuae dry herb 11 ㎏), than solvent agent hot water mixing solutions 500 ㎏ (solvent agent prescription weight ratio is 100 DEG C of hot water 300 ㎏+methyl salicylate 0.5 ㎏+niflumic acid 0.25 ㎏+potassium primary phosphate 175 ㎏+Sodium Selenite 0.5 ㎏+zinc sulfate 22.75 ㎏); Immersion solvent agent 200 ㎏+first time defibrination solvent agent 200 ㎏+second time defibrination solvent agent 100 ㎏); Other operations are with embodiment 1.
embodiment 4
Raw material herbal medicine and solvent agent prescription are counted by product weight: herbal medicine and solvent agent gross weight are than being 1:11; Herbal medicine amounts to 50 ㎏ (formula is the dry herb of the dry herb of crowndaisy chrysanthemum 10 ㎏+Artemisia scoparia 11 ㎏+Szechwan Chinaberry Fruit (dry fruit) 10 ㎏+root of langdu dry root medicine materical crude slice 10 ㎏+wolf tail grass dry herb 9 ㎏) than solvent agent hot water mixing solutions 550 ㎏ (solvent agent formulation by weight is 100 DEG C of hot water 330 ㎏+methyl salicylate 0.55 ㎏+ethyl acetate 0.275 ㎏+potassium primary phosphate 192.5 ㎏+boric acid tri butyl ester 0.55 ㎏+zinc sulfate 26.125 ㎏), immersion solvent agent 200 ㎏+first time defibrination solvent agent 300 ㎏+second time defibrination solvent agent 50 ㎏); Other operations are with embodiment 1.
embodiment 5
Raw material herbal medicine and solvent agent prescription are counted by product weight: herbal medicine is 1:10 with solvent agent gross weight ratio: herbal medicine amounts to 50 ㎏ (in formula the dry herb of calamus 9 ㎏+Herba Ixeritis chinensis dry herb 8 ㎏+Herba Artemisiae Scopariae dry herb 11 ㎏+setose thistle dry herb 11 ㎏+Herba Artemisiae annuae dry herb 11 ㎏) than solvent agent hot water mixing solutions 500 ㎏; (comprising immersion solvent agent 200 ㎏+first time defibrination solvent agent 200 ㎏+second time defibrination solvent agent 100 ㎏); Solvent agent formulation by weight is 100 DEG C of hot water 300 ㎏+methyl salicylate 0.5 ㎏+niflumic acid 0.25 ㎏+potassium primary phosphate 175 ㎏+Sodium Selenite 0.5 ㎏+zinc sulfate 22.75 ㎏, and other operations are with embodiment 1.
embodiment 6
Raw material herbal medicine and solvent agent prescription count 1:10 by product weight, herbal medicine and solvent agent gross weight amount to 50 ㎏ (wherein, the dry herb of Herba Potentillae Chinensis 12 ㎏+Herba Ixeritis chinensis dry herb 8 ㎏+Herba Artemisiae Scopariae dry herb 11 ㎏+setose thistle dry herb 10 ㎏+Herba Artemisiae annuae dry herb 9 ㎏), than solvent agent hot water mixing solutions 500 ㎏ (solvent agent formulation by weight is 100 DEG C of hot water 300 ㎏+methyl salicylate 0.5 ㎏+niflumic acid 0.25 ㎏+potassium primary phosphate 175 ㎏+Sodium Selenite 1.5 ㎏+zinc sulfate 22.75 ㎏), immersion solvent agent 200 ㎏+first time defibrination solvent agent 200 ㎏+second time defibrination solvent agent 100 ㎏), other operations are with embodiment 1.
The solubleness of more than three kinds mixed solutions of the solvent agent three kinds such as the ethyl acetate in the present invention+boric acid tri butyl ester+niflumic acid or potassium primary phosphate+Sodium Selenite+sulindac+boron nitride+wintergreen oil+selenous acid+sterilization crystallizing sulfanilamide+fenamic acid+vialidon+ammonium sulfate+zinc sulfate is 70% ~ 80%, the aqueous solubilities of dissolved mediator is low, easily volatilize dilution Sum decomposition out under adding the high-temperature condition of medium-height grass the effective elements of the medicine more than 60 DEG C, therefore, soaking and be all to mill slurrying with the dissolved in boiled water solvent agent of 100 DEG C in point secondary pulping process simultaneously.
Drug effect, the fertilizer efficiency field test of compound Chinese herb foliage fertilizer control plant pest
On crop yield impact and preventing disease pest control effect summary sheet
Test plot area 10 mu in this table, two are repeated three process, and process 1 is that No. 1, herbal medicine foliage fertilizer (product of example 2) dilutes 500 times, and in disease insect pest early period of origination, foliar spray, sprayed second time again every one week, connect spray 2 times; Process 2 and process 3 are No. 2, compound Chinese herb foliage fertilizer (product of example 3), dilute 800 times, dilute 500 times and disease insect pest early period of origination foliar spray, spray second time every one week again, connect spray 2 times; As can be seen from the comparative test result of different treatment, the impact of fertilizer efficiency on output is basically identical, but drug effect significant difference, the holding effect of diluting 500 times is the longest 61 days, basic prevention and elimination of disease and pests of need not going and buy Chinese medicine before vegetable sprout term, due to high temperature summer and autumn, the time controlling disease is longer, resist seedling stage hot and humid root disease and be easier to the critical porion that occurs, to have kept a full stand of seedings strong sprout for vegetables and the disease-resistant resistance to disease of the middle and late growth stage lays good basis.
Compound Chinese herb foliar nutrient using method:
Seed soaking: this product dilutes 500 times of immersion kinds, pulls out after drying and can sow.
Base manure: 3 ~ 5 kilograms every mu mix fine earth or farm manure mixing use.
Fill with root: dilute 500 ~ 1000 times and evenly water in crop root to crop growth period, rushing of booth fruits and vegetables is executed and drip irrigation.
Compound Chinese herb foliar nutrient leaf surface spraying test effect records table:
Claims (1)
1. a making method for Compound traditional Chinese medicine liquid foliar fertilizer, is characterized in that: proportioning raw materials is calculated as by product weight:
Herbal raw material is 1:8 with the gross weight ratio of solvent agent;
Herbal raw material gross weight 50 ㎏, the wherein tuber of pinellia dry root medicine materical crude slice 10 ㎏, the root of langdu dry root medicine materical crude slice 10 ㎏, Rumex patientia Linn. dry root medicine materical crude slice 11 ㎏, taraxacum dry root medicine materical crude slice 11 ㎏, Herba daturae 8 ㎏;
Solvent agent 400 ㎏, the weight proportion of solvent agent is 100 DEG C of hot water 239 ㎏, sterilization crystallizing sulfanilamide 0.4 ㎏, niflumic acid 0.2 ㎏, potassium primary phosphate 130 ㎏, selenous acid 0.4 ㎏, zinc sulfate 30 ㎏; First medium-height grass pharmaceutical media agent 100 ㎏ is soaked, first time defibrination solvent agent 200 ㎏, second time defibrination solvent agent 100 ㎏;
Concrete technology making step is as follows:
(1) soak: adopt said herbal medicine raw material gross weight 50 ㎏, solvent agent consumption 100 ㎏, soaks 24 hours;
(2) grind liquid slurry secondary altogether: with the solvent agent impregnated herbal medicine tuber of pinellia dry root medicine materical crude slice, the root of langdu dry root medicine materical crude slice, Rumex patientia Linn. dry root medicine materical crude slice, the dry root medicine materical crude slice of taraxacum, Herba daturae totally 150 ㎏, add solvent agent 200 ㎏, grind first time slurries; Again grind coarse filtration dregs of a decoction solubilization mediator 100 ㎏ again that liquid slurry first time grinds slurries, grind secondary slurries, namely the slurrying liquid mixing of twice obtains raw product herbal medicine fertilizer solution slurry;
(3) filter: comprise two-step process, one is coarse filtration mistake, and filter grinding the liquid slurry plate-and-frame filter press squeezed, filter cloth made by lint-free non-woven fabrics, and 100 ~ 200 order pressing plate coarse filtration, remove the material of some macrobeads, thickness; Two is adopt circular impact screen, sieves the thinnest to 500 orders or 0.028mm, filters most I to 5 micron, fill the screen cloth of 1 ~ 5 layer of different meshes, carry out sorting or filtration simultaneously to the material of 2 ~ 6 grades, filtering accuracy 5 ~ 100 microns;
(4) clarify: filtrate after filtration adopts high speed tubular type centrifuge, rotating speed 16000r/h, diameter 105mm, power 3kw, centrifugal go out relative density of medicine liquid 1.07, make Compound traditional Chinese medicine liquid foliar fertilizer.
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| CN105884443A (en) * | 2014-10-31 | 2016-08-24 | 蓝承娟 | Formula fertilizer capable of increasing fruiting rate of corn |
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| CN108077000A (en) * | 2017-12-12 | 2018-05-29 | 江西省抚州市农业科学研究所 | A kind of double seasons pair spray direct-sowing cultivating methods of rice |
| CN108503453A (en) * | 2018-06-24 | 2018-09-07 | 覃海平 | A kind of general foliar fertilizer and preparation method thereof promoting flowering of plant result |
| CN108484299A (en) * | 2018-06-24 | 2018-09-04 | 覃海平 | A kind of general foliar fertilizer and preparation method thereof |
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