CN103153961A - 氟虫腈制备方法 - Google Patents
氟虫腈制备方法 Download PDFInfo
- Publication number
- CN103153961A CN103153961A CN2011800344333A CN201180034433A CN103153961A CN 103153961 A CN103153961 A CN 103153961A CN 2011800344333 A CN2011800344333 A CN 2011800344333A CN 201180034433 A CN201180034433 A CN 201180034433A CN 103153961 A CN103153961 A CN 103153961A
- Authority
- CN
- China
- Prior art keywords
- acid
- formula
- minutes
- reaction mixture
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 0 *C(C(NN*)=C1*=C)=**1c(c(N)cc([N+]*)c1)c1N Chemical compound *C(C(NN*)=C1*=C)=**1c(c(N)cc([N+]*)c1)c1N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/14—Ectoparasiticides, e.g. scabicides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Animal Behavior & Ethology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Public Health (AREA)
- Agronomy & Crop Science (AREA)
- Medicinal Chemistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Claims (9)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US36336610P | 2010-07-12 | 2010-07-12 | |
US61/363366 | 2010-07-12 | ||
PCT/IL2011/000546 WO2012007938A1 (en) | 2010-07-12 | 2011-07-10 | Fipronil production process |
Publications (1)
Publication Number | Publication Date |
---|---|
CN103153961A true CN103153961A (zh) | 2013-06-12 |
Family
ID=44645163
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2011800344333A Pending CN103153961A (zh) | 2010-07-12 | 2011-07-10 | 氟虫腈制备方法 |
Country Status (13)
Country | Link |
---|---|
US (10) | US20130197238A1 (zh) |
EP (1) | EP2593436A1 (zh) |
JP (1) | JP2013532187A (zh) |
KR (1) | KR20130124473A (zh) |
CN (1) | CN103153961A (zh) |
AU (1) | AU2011277946B2 (zh) |
BR (1) | BR112013000758A8 (zh) |
CA (1) | CA2805227A1 (zh) |
CO (1) | CO6660510A2 (zh) |
MX (1) | MX2013000374A (zh) |
NZ (1) | NZ605535A (zh) |
WO (1) | WO2012007938A1 (zh) |
ZA (1) | ZA201300195B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103360316A (zh) * | 2013-04-22 | 2013-10-23 | 浙江海正化工股份有限公司 | 一种氟虫腈的制备方法 |
CN106458875A (zh) * | 2014-06-26 | 2017-02-22 | 住友化学株式会社 | 苯酚化合物的制造方法 |
CN111004180A (zh) * | 2019-09-11 | 2020-04-14 | 浙江埃森化学有限公司 | 一种制备氟虫腈的方法 |
CN115003656A (zh) * | 2020-01-31 | 2022-09-02 | 拜耳公司 | [(1,4,5-三取代1h-吡唑-3-基)硫烷基]乙酸衍生物和其盐及其作为活性除草成分的用途 |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1968578A4 (en) | 2005-12-14 | 2011-02-23 | Makhteshim Chem Works Ltd | POLYMORPHIC AND AMORPHOUS FORMS OF 5-AMINO-L- [2,6-DICHLORO-4- (TRIFLUOROMETHYL) PHENYL] -4- [(TRIFLUOROMETHYL) SULFINYL] -IH-PYRAZOLE-3-CARBONITRIL |
IT1400666B1 (it) | 2010-07-07 | 2013-06-28 | Finchimica Srl | Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli. |
CN102690232A (zh) * | 2012-05-30 | 2012-09-26 | 河南中医学院 | 一种氟虫腈中间体的合成方法 |
EP3412658A1 (en) * | 2017-06-09 | 2018-12-12 | Solvay Sa | Processes for the manufacture of sulfur-substitued pyrazole derivatives |
CN111386256A (zh) | 2017-11-15 | 2020-07-07 | 阿达玛马克西姆有限公司 | 5-氨基-1-(2,6-二氯-4-三氟甲基-苯基)-4-乙基硫烷基-1h-吡唑-3-甲腈及相关化合物的合成 |
CN108318604A (zh) * | 2017-12-19 | 2018-07-24 | 上海市农产品质量安全检测中心 | 一种牛奶中氟虫腈及其代谢物的检测方法 |
KR102083906B1 (ko) | 2018-09-21 | 2020-03-03 | (주)스페이스링크 | 피프로닐 대사산물의 효과적인 제거 물질 생성장치 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007122440A1 (en) * | 2006-04-25 | 2007-11-01 | Gharda Chemicals Limited | Process for the preparation of fipronil, an insecticide, and related pyrazoles |
CN101250158A (zh) * | 2008-04-02 | 2008-08-27 | 湖南化工研究院 | 一种氟虫腈的制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8713768D0 (en) | 1987-06-12 | 1987-07-15 | May & Baker Ltd | Compositions of matter |
DK1222173T3 (da) | 1999-10-22 | 2004-09-20 | Bayer Cropscience Sa | Fremgangsmåde til fremstilling af 4-trifluormethylsulphinylpyrazolderivat |
PL2443093T3 (pl) * | 2009-03-16 | 2014-04-30 | Basf Agro B V Arnhem Nl Zuerich Branch | Sposób wytwarzania pochodnych pirazolu |
DK2493860T3 (da) * | 2009-10-30 | 2014-04-07 | Basf Se | Fremgangsmåde til fremstilling af 4-sulfinylpyrazolderivater |
IT1400666B1 (it) * | 2010-07-07 | 2013-06-28 | Finchimica Srl | Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli. |
-
2011
- 2011-07-10 CN CN2011800344333A patent/CN103153961A/zh active Pending
- 2011-07-10 MX MX2013000374A patent/MX2013000374A/es not_active Application Discontinuation
- 2011-07-10 CA CA2805227A patent/CA2805227A1/en not_active Abandoned
- 2011-07-10 KR KR1020137001662A patent/KR20130124473A/ko not_active Application Discontinuation
- 2011-07-10 EP EP11752348.0A patent/EP2593436A1/en not_active Withdrawn
- 2011-07-10 WO PCT/IL2011/000546 patent/WO2012007938A1/en active Application Filing
- 2011-07-10 BR BR112013000758A patent/BR112013000758A8/pt not_active Application Discontinuation
- 2011-07-10 US US13/809,327 patent/US20130197238A1/en not_active Abandoned
- 2011-07-10 JP JP2013519212A patent/JP2013532187A/ja not_active Ceased
- 2011-07-10 NZ NZ60553511A patent/NZ605535A/en not_active IP Right Cessation
- 2011-07-10 AU AU2011277946A patent/AU2011277946B2/en not_active Ceased
-
2012
- 2012-12-27 CO CO12234698A patent/CO6660510A2/es unknown
-
2013
- 2013-01-08 ZA ZA2013/00195A patent/ZA201300195B/en unknown
- 2013-06-25 US US13/926,389 patent/US20130289283A1/en not_active Abandoned
-
2014
- 2014-02-06 US US14/174,406 patent/US20140155620A1/en not_active Abandoned
- 2014-09-12 US US14/485,508 patent/US20150099892A1/en not_active Abandoned
-
2016
- 2016-06-29 US US15/196,633 patent/US20160304467A1/en not_active Abandoned
-
2017
- 2017-01-17 US US15/408,124 patent/US20170121290A1/en not_active Abandoned
- 2017-07-25 US US15/659,440 patent/US20170320832A1/en not_active Abandoned
-
2018
- 2018-02-02 US US15/887,231 patent/US20180155294A1/en not_active Abandoned
- 2018-05-29 US US15/991,776 patent/US20180282286A1/en not_active Abandoned
-
2019
- 2019-01-25 US US16/257,452 patent/US20190152921A1/en not_active Abandoned
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007122440A1 (en) * | 2006-04-25 | 2007-11-01 | Gharda Chemicals Limited | Process for the preparation of fipronil, an insecticide, and related pyrazoles |
CN101250158A (zh) * | 2008-04-02 | 2008-08-27 | 湖南化工研究院 | 一种氟虫腈的制备方法 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103360316A (zh) * | 2013-04-22 | 2013-10-23 | 浙江海正化工股份有限公司 | 一种氟虫腈的制备方法 |
CN106458875A (zh) * | 2014-06-26 | 2017-02-22 | 住友化学株式会社 | 苯酚化合物的制造方法 |
CN111004180A (zh) * | 2019-09-11 | 2020-04-14 | 浙江埃森化学有限公司 | 一种制备氟虫腈的方法 |
CN115003656A (zh) * | 2020-01-31 | 2022-09-02 | 拜耳公司 | [(1,4,5-三取代1h-吡唑-3-基)硫烷基]乙酸衍生物和其盐及其作为活性除草成分的用途 |
Also Published As
Publication number | Publication date |
---|---|
US20140155620A1 (en) | 2014-06-05 |
BR112013000758A2 (pt) | 2016-05-24 |
US20130289283A1 (en) | 2013-10-31 |
AU2011277946A1 (en) | 2013-02-07 |
NZ605535A (en) | 2015-03-27 |
EP2593436A1 (en) | 2013-05-22 |
US20170121290A1 (en) | 2017-05-04 |
JP2013532187A (ja) | 2013-08-15 |
ZA201300195B (en) | 2013-09-25 |
WO2012007938A1 (en) | 2012-01-19 |
US20180155294A1 (en) | 2018-06-07 |
BR112013000758A8 (pt) | 2018-02-14 |
KR20130124473A (ko) | 2013-11-14 |
US20190152921A1 (en) | 2019-05-23 |
US20180282286A1 (en) | 2018-10-04 |
US20130197238A1 (en) | 2013-08-01 |
MX2013000374A (es) | 2013-03-05 |
US20160304467A1 (en) | 2016-10-20 |
AU2011277946B2 (en) | 2015-06-11 |
US20170320832A1 (en) | 2017-11-09 |
CO6660510A2 (es) | 2013-04-30 |
WO2012007938A8 (en) | 2012-12-13 |
CA2805227A1 (en) | 2012-01-19 |
US20150099892A1 (en) | 2015-04-09 |
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CB02 | Change of applicant information |
Address after: Holland Curacao Applicant after: Adama Searl Hughes Co.,Ltd. Kuraso branch Address before: Holland Curacao Applicant before: Selhus Property Company Elvita Plant Protection Branch |
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