CN102674425B - 一种常温法纳米级碳酸钙生产工艺 - Google Patents
一种常温法纳米级碳酸钙生产工艺 Download PDFInfo
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- CN102674425B CN102674425B CN 201210158716 CN201210158716A CN102674425B CN 102674425 B CN102674425 B CN 102674425B CN 201210158716 CN201210158716 CN 201210158716 CN 201210158716 A CN201210158716 A CN 201210158716A CN 102674425 B CN102674425 B CN 102674425B
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- calcium carbonate
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- carbonization
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 98
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 74
- 238000000034 method Methods 0.000 title claims abstract description 47
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 239000013078 crystal Substances 0.000 claims abstract description 28
- 238000001035 drying Methods 0.000 claims abstract description 26
- 238000010000 carbonizing Methods 0.000 claims abstract description 11
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 29
- 238000003763 carbonization Methods 0.000 claims description 27
- 230000015572 biosynthetic process Effects 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 15
- 239000000292 calcium oxide Substances 0.000 claims description 15
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 15
- 238000007670 refining Methods 0.000 claims description 15
- 239000001569 carbon dioxide Substances 0.000 claims description 14
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 14
- 238000000746 purification Methods 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 13
- 239000003112 inhibitor Substances 0.000 claims description 11
- 239000012065 filter cake Substances 0.000 claims description 10
- 235000013336 milk Nutrition 0.000 claims description 10
- 239000008267 milk Substances 0.000 claims description 10
- 210000004080 milk Anatomy 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 10
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 8
- 230000018044 dehydration Effects 0.000 claims description 8
- 238000006297 dehydration reaction Methods 0.000 claims description 8
- 230000005587 bubbling Effects 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 5
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 claims description 5
- 238000004381 surface treatment Methods 0.000 claims description 5
- 239000000725 suspension Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 4
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 4
- 238000005265 energy consumption Methods 0.000 abstract description 4
- 239000002245 particle Substances 0.000 abstract description 3
- 239000004033 plastic Substances 0.000 abstract description 3
- 229920003023 plastic Polymers 0.000 abstract description 3
- 239000012847 fine chemical Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 238000003889 chemical engineering Methods 0.000 abstract 1
- 239000003973 paint Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 5
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 description 3
- 238000005255 carburizing Methods 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000007710 freezing Methods 0.000 description 3
- 230000008014 freezing Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 235000019983 sodium metaphosphate Nutrition 0.000 description 3
- 239000001488 sodium phosphate Substances 0.000 description 3
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical group [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 3
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 3
- 235000019801 trisodium phosphate Nutrition 0.000 description 3
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 3
- 229960001763 zinc sulfate Drugs 0.000 description 3
- 229910000368 zinc sulfate Inorganic materials 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 150000003016 phosphoric acids Chemical class 0.000 description 2
- 239000004584 polyacrylic acid Substances 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 238000004513 sizing Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
Description
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CN 201210158716 CN102674425B (zh) | 2012-05-19 | 2012-05-19 | 一种常温法纳米级碳酸钙生产工艺 |
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CN102674425A CN102674425A (zh) | 2012-09-19 |
CN102674425B true CN102674425B (zh) | 2013-12-18 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9902652B2 (en) | 2014-04-23 | 2018-02-27 | Calera Corporation | Methods and systems for utilizing carbide lime or slag |
Families Citing this family (19)
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BR102013016060B1 (pt) * | 2013-06-24 | 2015-06-02 | Ecofill Espec Em Tecnologia De Transf De Resíduos Ltda | Processos seco e úmido de recuperação, beneficiamento e reaproveitamento do resíduo de dregs gerado na indústria de celulose e produtos obtidos através dos mesmos |
CN104418376B (zh) * | 2013-09-03 | 2016-08-17 | 井陉县京华钙业有限公司 | 一种沉淀碳酸钙的生产工艺 |
CN103950964B (zh) * | 2014-04-29 | 2018-02-23 | 东华大学 | 一种通过调节碳化次数制备不同径向比纳米碳酸钙颗粒的方法 |
CN103950965B (zh) * | 2014-04-29 | 2016-07-13 | 东华大学 | 一种运用种晶法制备不同尺寸纳米碳酸钙的方法 |
SI2966129T1 (sl) * | 2014-07-11 | 2019-02-28 | Omya International Ag | Postopek sušenja |
CN104085896B (zh) | 2014-07-18 | 2015-12-09 | 大唐国际发电股份有限公司高铝煤炭资源开发利用研发中心 | 活性硅酸钙的制备方法 |
CN104389025B (zh) * | 2014-10-17 | 2017-03-22 | 东北大学 | 一种增强硫酸钙晶须疏水性的方法 |
CN105060330B (zh) * | 2015-09-14 | 2018-04-06 | 广西大学 | 一种球形碳酸钙晶体的制备方法 |
CN105329928A (zh) * | 2015-12-10 | 2016-02-17 | 湖南化工职业技术学院 | 一种纳米碳酸钙活化方法 |
CN106517285B (zh) * | 2016-11-21 | 2017-11-14 | 广西华纳新材料科技有限公司 | 一种棒状纳米碳酸钙的制备方法 |
CN109592702A (zh) * | 2018-12-29 | 2019-04-09 | 福建贝思科电子材料股份有限公司 | 一种纳米级碳酸盐及其制备方法 |
CN109809457B (zh) * | 2019-03-21 | 2021-07-09 | 广西碳酸钙产业化工程院有限公司 | 规整球形碳酸钙及其制备工艺 |
CN110817921A (zh) * | 2019-10-24 | 2020-02-21 | 湖南金箭新材料科技有限公司 | 一种纳米碳酸钙陈化、均化、表面处理一体化生产工艺 |
AU2021226337A1 (en) | 2020-02-25 | 2022-09-08 | Arelac, Inc. | Methods and systems for treatment of limestone to form vaterite |
CN111717928A (zh) * | 2020-04-24 | 2020-09-29 | 广西科学院 | 一种原位电化学沉淀技术制备纳米碳酸钙的方法 |
CN111453754A (zh) * | 2020-04-28 | 2020-07-28 | 广西夏阳环保科技有限公司 | 一种高纯度、高活性纳米碳酸钙的制备方法 |
MX2022016196A (es) | 2020-06-30 | 2023-04-26 | Arelac Inc | Métodos y sistemas para la formación de vaterita a partir de piedra caliza utilizando horno eléctrico. |
CN113019664A (zh) * | 2021-04-23 | 2021-06-25 | 山东宇信纳米科技有限公司 | 一种超低水分的纳米碳酸钙干燥解聚***及其使用方法 |
CN115353138A (zh) * | 2022-08-10 | 2022-11-18 | 中南大学 | 一种食品级轻质碳酸钙的制备方法 |
Family Cites Families (3)
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JP4245712B2 (ja) * | 1998-12-18 | 2009-04-02 | 奥多摩工業株式会社 | 製紙スラッジを利用した軽質炭酸カルシウムおよびその製法 |
FI120032B (fi) * | 2004-07-13 | 2009-06-15 | Fp Pigments Oy | Menetelmä ja laite kalsiumkarbonaattituotteen valmistamiseksi, tuote ja sen käyttö |
CN101108741A (zh) * | 2006-07-21 | 2008-01-23 | 北京市化工建材厂 | 一种纳米活性碳酸钙的工业制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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US9902652B2 (en) | 2014-04-23 | 2018-02-27 | Calera Corporation | Methods and systems for utilizing carbide lime or slag |
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Address after: 426181 Yongzhou city of Hunan province Qiyang Lijiaping town Horse Street Applicant after: HUNAN JINJIAN NEW MATERIAL TECHNOLOGY Co.,Ltd. Address before: 426181 Yongzhou city of Hunan province Qiyang Lijiaping town Horse Street Applicant before: QIYANG JIAMING CHEMICAL Co.,Ltd. |
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Denomination of invention: A production process of nanometer calcium carbonate at room temperature Effective date of registration: 20201029 Granted publication date: 20131218 Pledgee: Yongzhou branch of China Construction Bank Co.,Ltd. Pledgor: HUNAN JINJIAN NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2020430000023 |
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Date of cancellation: 20210322 Granted publication date: 20131218 Pledgee: Yongzhou branch of China Construction Bank Co.,Ltd. Pledgor: HUNAN JINJIAN NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2020430000023 |
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Denomination of invention: A production process of nanometer calcium carbonate at room temperature Effective date of registration: 20210623 Granted publication date: 20131218 Pledgee: Yongzhou branch of China Construction Bank Co.,Ltd. Pledgor: HUNAN JINJIAN NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021430000020 |
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Denomination of invention: A Production Process of Nanoscale Calcium Carbonate by Room Temperature Method Effective date of registration: 20230830 Granted publication date: 20131218 Pledgee: Yongzhou branch of China Construction Bank Co.,Ltd. Pledgor: HUNAN JINJIAN NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2023430000021 |
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