CN102515532A - Preparation method of light-peach-colored crystal bead blanks - Google Patents
Preparation method of light-peach-colored crystal bead blanks Download PDFInfo
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- CN102515532A CN102515532A CN2011104030464A CN201110403046A CN102515532A CN 102515532 A CN102515532 A CN 102515532A CN 2011104030464 A CN2011104030464 A CN 2011104030464A CN 201110403046 A CN201110403046 A CN 201110403046A CN 102515532 A CN102515532 A CN 102515532A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
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Abstract
The invention discloses a preparation method of light-peach-colored crystal bead blanks. Aiming at defects of poor coloring reproducibility, poor product stability, low production efficiency, and unsuitability for continuous tank furnace production of prior art for preparing light-peach-colored crystal bead blanks, the invention provides a light-peach-colored crystal bead blank preparation method with good coloring reproducibility, stable product quality, high production efficiency, and suitability for continuous tank furnace production. According to the light-peach-colored crystal bead blank preparation method, the light-peach-colored crystal bead blanks are prepared from raw materials of, by weight: 50-70 parts of quartz sand, 5-15 parts of soda ash, 7-16 parts of potassium carbonate, 2-9 parts of potassium nitrate, 2-5 parts of boric acid, no more than 45-65 parts of lead silicate, no more than 3 parts of antimony trioxide, no more than 8 parts of cerium oxide, no more than 5 parts of barium carbonate, no more than 10 parts of titanium pigment, no more than 3 parts of zinc oxide, and no more than 15 parts of erbium oxide.
Description
Technical field
The present invention relates to the artificial crystal production field, particularly a kind of preparation method of shallow honey peach look crystal pearl embryo.
Background technology
Shallow honey peach look crystal pearl embryo is the work in-process that are used for preparing shallow honey peach look quartzy product; Be to adopt erbium ion painted in the shallow honey peach look of the existing preparation crystal pearl embryo technology; Erbium ion is provided by erbium oxide, adopt product ubiquity that the shallow honey peach look of existing preparation crystal pearl embryo explained hereafter goes out color reproduction poor, unstable product quality; Production efficiency is low, is not suitable for the weak point of the production operation of continuous tank furnace.In addition, in the shallow honey peach look of existing preparation crystal pearl embryo technology, in the composition of raw materials of shallow honey peach look crystal pearl embryo, the red lead component is arranged, red lead is volatile, can cause environmental pollution.
Summary of the invention
It is poor to the objective of the invention is to existing above-mentioned the color reproduction of the shallow honey peach look of existing preparation crystal pearl embryo technology; Unstable product quality, production efficiency is low, is not suitable for the weak point of the production operation of continuous tank furnace; Provide a kind of color reproduction good; Constant product quality, production efficiency is high, can be fit to the preparation method of shallow honey peach look crystal pearl embryo of the production operation of continuous tank furnace.
The technical scheme that the present invention adopted is accomplished through following mode: a kind of preparation method of shallow honey peach look crystal pearl embryo, the weight proportion of this shallow honey peach look crystal pearl embryo raw material is: 50～70 parts of silica sands, 5～15 parts of soda ash, 7～16 parts in salt of wormwood, 2～9 parts in saltpetre, 2～5 parts of boric acid, lead silicate≤45-65 part, Antimony Trioxide: 99.5Min≤3 part, cerium oxide≤8 part, barium carbonate≤5 part, white titanium pigment≤10 part, zinc oxide≤3 part, Erbium trioxide≤15 part.
In the preparation method of above-mentioned shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, keep oxidizing atmosphere and glass quartz liquation liquid level stabilizing when founding;
(4) the glass quartz liquation is molded into shallow honey peach water after the homogenizing cooling and bores the pearl embryo.
In the preparation method of above-mentioned shallow honey peach look crystal pearl embryo, in the preparation process (3) of shallow honey peach look crystal pearl embryo, temperature is controlled at 1300 ℃～1500 ℃ when founding.
In the preparation method of above-mentioned shallow honey peach look crystal pearl embryo, in the preparation process (4) of shallow honey peach look crystal pearl embryo, cooling temperature is controlled at 550 ℃～1030 ℃, and is preferred: 750 ℃～900 ℃.
The preparation method of the shallow honey peach look of the present invention crystal pearl embryo compares with the shallow honey peach look of existing preparation crystal pearl embryo technology, has following characteristics:
1, adopts shallow honey peach look crystal pearl embryo composition of raw materials of the present invention, make the redox equilibrium of erbium ion in the process of founding keep stable, thereby obtain to have the shallow honey peach look of well reproduced property.
2, the preparation method of the shallow honey peach look of the present invention crystal pearl embryo has reduced plumbous content in the crystal pearl embryo, adopts the Na-K-B-Si-Pb system to reach the optical property requirement of high refractive index.
3, in shallow honey peach look crystal pearl embryo composition of raw materials of the present invention, replace red lead with lead silicate, lead silicate is more stable, and is not volatile, has environment protection significance.
4, the present invention can carry out the continuous working kiln production operation, has improved efficient and production capacity.
Embodiment
Through embodiment the present invention is made further below and specifying.
Embodiment 1
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 50 parts of silica sands, 8 parts of soda ash, 7 parts in salt of wormwood, 2 parts in saltpetre, 2 parts of boric acid, 45 parts in lead silicate, 1 part of Antimony Trioxide: 99.5Min, 6 parts, 1 part of cerium oxide, 2 parts of barium carbonates, 10 parts of white titanium pigments, 1 part in zinc oxide, 10 parts of Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 550 ℃～1030 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 2
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 70 parts of silica sands, 15 parts of soda ash, 16 parts in salt of wormwood, 9 parts in saltpetre, 5 parts of boric acid, 55 parts in lead silicate, 3 parts of Antimony Trioxide: 99.5Mins, 8 parts of cerium oxide, 5 parts of barium carbonates, 5 parts of white titanium pigments, 3 parts in zinc oxide, 7 parts of Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 550 ℃～1030 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 3
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 60 parts of silica sands, 10 parts of soda ash, 14 parts in salt of wormwood, 6 parts in saltpetre, 4 parts of boric acid, 63 parts in lead silicate, 2 parts of Antimony Trioxide: 99.5Mins, 1 part of cerium oxide, 2 parts of barium carbonates, 9 parts of white titanium pigments, 1 part in zinc oxide, 13 parts of Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 4
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 55 parts of silica sands, 7 parts of soda ash, 15 parts in salt of wormwood, 9 parts in saltpetre, 4 parts of boric acid, 3 parts of Antimony Trioxide: 99.5Mins, 2 parts of cerium oxide, 5 parts of barium carbonates, 9 parts of white titanium pigments, 3 parts in zinc oxide, 2 parts of Erbium trioxides, 55 parts in lead silicate;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 5
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 2 parts of 65 parts of silica sands, 13 parts of soda ash, 4 parts in salt of wormwood, 2 parts in saltpetre, 3 parts of boric acid, lead silicate≤48 part, cerium oxide≤8 part, white titanium pigment≤5 part, zinc oxide≤3 part, Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 6
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 57 parts of silica sands, 9 parts of soda ash, 6 parts in salt of wormwood, 8 parts in saltpetre, 4 parts of boric acid, 58 parts in lead silicate, 2 parts of Antimony Trioxide: 99.5Mins, 0.5 part of barium carbonate, 3 parts of white titanium pigments, 4 parts of Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 7
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 68 parts of silica sands, 12 parts of soda ash, 16 parts in salt of wormwood, 4 parts in saltpetre, 5 parts of boric acid, 55 parts in lead silicate, 3 parts of Antimony Trioxide: 99.5Mins, 3 parts of cerium oxide, 10 parts of white titanium pigments, 5 parts of barium carbonates, 3 parts in zinc oxide, Erbium trioxide≤9 part;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach water and bore the pearl embryo.
Embodiment 8
A kind of preparation method of shallow honey peach look crystal pearl embryo, the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes; Wherein, the composition of raw materials (weight ratio) of shallow honey peach look crystal pearl embryo is: 62 parts of silica sands, 9 parts of soda ash, 10 parts in salt of wormwood, 5 parts in saltpetre, 2 parts of boric acid, 61 parts in lead silicate, 2 parts of Antimony Trioxide: 99.5Mins, 1 part of cerium oxide, 4 parts of barium carbonates, 4 parts of white titanium pigments, 2 parts in zinc oxide, 6 parts of Erbium trioxides;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, when founding, temperature is controlled at 1300 ℃～1500 ℃, keeps oxidizing atmosphere and glass quartz liquation liquid level stabilizing;
(4) with the glass quartz liquation when homogenizing is cooled to 750 ℃～900 ℃, be molded into shallow honey peach look crystal pearl embryo.
Claims (5)
1. the preparation method of a shallow honey peach look crystal pearl embryo is characterized in that the weight proportion of this shallow honey peach look crystal pearl embryo raw material is: 50～70 parts of silica sands, 5～15 parts of soda ash, 7～16 parts in salt of wormwood, 2～9 parts in saltpetre, 2～5 parts of boric acid, lead silicate≤45-65 part, Antimony Trioxide: 99.5Min≤3 part, cerium oxide≤8 part, barium carbonate≤5 part, white titanium pigment≤10 part, zinc oxide≤3 part, Erbium trioxide≤15 part.
2. the preparation method of shallow honey peach look crystal pearl embryo according to claim 1 is characterized in that the preparation method of shallow honey peach look crystal pearl embryo may further comprise the steps:
(1) after being weighed up by weight ratio, the raw material of shallow honey peach look crystal pearl embryo mixes;
The shallow honey peach look crystal pearl embryo raw material that (2) will mix carries out granulation through tablets press;
(3) will process granular shallow honey peach look crystal pearl embryo raw material and put into the glass quartz tank furnace and found, keep oxidizing atmosphere and glass quartz liquation liquid level stabilizing when founding;
(4) the glass quartz liquation is molded into shallow honey peach water after the homogenizing cooling and bores the pearl embryo.
3. the preparation method of shallow honey peach look crystal pearl embryo according to claim 2 is characterized in that in the preparation process (3) of shallow honey peach look crystal pearl embryo, temperature is controlled at 1300 ℃～1500 ℃ when founding.
4. the preparation method of shallow honey peach look crystal pearl embryo according to claim 2 is characterized in that in the preparation process (4) of shallow honey peach look crystal pearl embryo, cooling temperature is controlled at 550 ℃～1030 ℃.
5. the preparation method of shallow honey peach look crystal pearl embryo according to claim 4 is characterized in that in the preparation process (4) of shallow honey peach look crystal pearl embryo, cooling temperature is controlled at 750 ℃～900 ℃.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103466945A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Formula of colored glaze |
| CN103466947A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Preparation technique of colored glaze with favorable clarification effect and high quality |
| CN103466944A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Colored glaze with favorable clarification effect and high product quality |
| CN103466946A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Preparation method of colored glaze |
| CN104445938A (en) * | 2014-10-31 | 2015-03-25 | 太仓市科教新城琉璃艺术策划中心 | Production process of colored glaze |
| CN104556696A (en) * | 2015-01-06 | 2015-04-29 | 浙江伟兴水晶有限公司 | Pink crystal bead embryo and preparation method thereof |
| CN109761502A (en) * | 2019-03-27 | 2019-05-17 | 广东蓝碟羽水晶饰品有限公司 | A kind of manufacturing method of rare earth tinted clear grey crystal pearl base |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103466945A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Formula of colored glaze |
| CN103466947A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Preparation technique of colored glaze with favorable clarification effect and high quality |
| CN103466944A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Colored glaze with favorable clarification effect and high product quality |
| CN103466946A (en) * | 2013-09-06 | 2013-12-25 | 太仓市科教新城琉璃艺术策划中心 | Preparation method of colored glaze |
| CN104445938A (en) * | 2014-10-31 | 2015-03-25 | 太仓市科教新城琉璃艺术策划中心 | Production process of colored glaze |
| CN104556696A (en) * | 2015-01-06 | 2015-04-29 | 浙江伟兴水晶有限公司 | Pink crystal bead embryo and preparation method thereof |
| CN104556696B (en) * | 2015-01-06 | 2016-03-23 | 浙江伟兴水晶有限公司 | A kind of rosy quartz pearl embryo and preparation method thereof |
| CN109761502A (en) * | 2019-03-27 | 2019-05-17 | 广东蓝碟羽水晶饰品有限公司 | A kind of manufacturing method of rare earth tinted clear grey crystal pearl base |
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Effective date of registration: 20220211 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Kangji street, Jindong District, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |