CN102286665A - 一种复杂含砷及有价金属渣尘物料的综合回收方法 - Google Patents
一种复杂含砷及有价金属渣尘物料的综合回收方法 Download PDFInfo
- Publication number
- CN102286665A CN102286665A CN201110260188XA CN201110260188A CN102286665A CN 102286665 A CN102286665 A CN 102286665A CN 201110260188X A CN201110260188X A CN 201110260188XA CN 201110260188 A CN201110260188 A CN 201110260188A CN 102286665 A CN102286665 A CN 102286665A
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- China
- Prior art keywords
- arsenic
- slag
- rotary kiln
- stove
- furnace
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052785 arsenic Inorganic materials 0.000 title claims abstract description 91
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 239000002893 slag Substances 0.000 title claims abstract description 76
- 239000002184 metal Substances 0.000 title claims abstract description 29
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000000463 material Substances 0.000 title claims abstract description 12
- 239000000428 dust Substances 0.000 title abstract description 8
- 238000011084 recovery Methods 0.000 title abstract description 5
- 239000003513 alkali Substances 0.000 claims abstract description 27
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 19
- 239000000956 alloy Substances 0.000 claims abstract description 19
- 238000007670 refining Methods 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 16
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 15
- 230000003647 oxidation Effects 0.000 claims abstract description 12
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 12
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 12
- 239000011701 zinc Substances 0.000 claims abstract description 12
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000001704 evaporation Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 229910052787 antimony Inorganic materials 0.000 claims abstract description 6
- RMBBSOLAGVEUSI-UHFFFAOYSA-H Calcium arsenate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-][As]([O-])([O-])=O.[O-][As]([O-])([O-])=O RMBBSOLAGVEUSI-UHFFFAOYSA-H 0.000 claims abstract description 5
- 239000004568 cement Substances 0.000 claims abstract description 5
- 230000008018 melting Effects 0.000 claims abstract 2
- 238000002844 melting Methods 0.000 claims abstract 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 30
- 239000003500 flue dust Substances 0.000 claims description 25
- 239000003818 cinder Substances 0.000 claims description 9
- 239000011575 calcium Substances 0.000 claims description 8
- 238000003723 Smelting Methods 0.000 claims description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000002817 coal dust Substances 0.000 claims description 6
- 230000008020 evaporation Effects 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000004744 fabric Substances 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- TVQLLNFANZSCGY-UHFFFAOYSA-N disodium;dioxido(oxo)tin Chemical compound [Na+].[Na+].[O-][Sn]([O-])=O TVQLLNFANZSCGY-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- 235000017550 sodium carbonate Nutrition 0.000 claims description 3
- 229940079864 sodium stannate Drugs 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- 229910000519 Ferrosilicon Inorganic materials 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 238000007664 blowing Methods 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 abstract description 4
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 abstract description 4
- 229910052797 bismuth Inorganic materials 0.000 abstract description 3
- 229910052709 silver Inorganic materials 0.000 abstract description 3
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 abstract description 2
- 238000007796 conventional method Methods 0.000 abstract description 2
- 239000004332 silver Substances 0.000 abstract description 2
- 239000000779 smoke Substances 0.000 abstract description 2
- GOLCXWYRSKYTSP-UHFFFAOYSA-N Arsenious Acid Chemical compound O1[As]2O[As]1O2 GOLCXWYRSKYTSP-UHFFFAOYSA-N 0.000 abstract 4
- 230000001376 precipitating effect Effects 0.000 abstract 2
- 229940103357 calcium arsenate Drugs 0.000 abstract 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 abstract 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 abstract 1
- 235000011116 calcium hydroxide Nutrition 0.000 abstract 1
- 239000000920 calcium hydroxide Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- RHZUVFJBSILHOK-UHFFFAOYSA-N anthracen-1-ylmethanolate Chemical compound C1=CC=C2C=C3C(C[O-])=CC=CC3=CC2=C1 RHZUVFJBSILHOK-UHFFFAOYSA-N 0.000 description 2
- 239000003830 anthracite Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- JRIGVWDKYXCHMG-UHFFFAOYSA-N (5-arsoroso-2-hydroxyphenyl)azanium;chloride Chemical compound Cl.NC1=CC([As]=O)=CC=C1O JRIGVWDKYXCHMG-UHFFFAOYSA-N 0.000 description 1
- 229910001316 Ag alloy Inorganic materials 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000722270 Regulus Species 0.000 description 1
- ASDVIRMTSAONFT-UHFFFAOYSA-N [As].[Pb]=O Chemical compound [As].[Pb]=O ASDVIRMTSAONFT-UHFFFAOYSA-N 0.000 description 1
- ACWONLHCGMCSPD-UHFFFAOYSA-N [Bi].[Ag].[Sn].[Pb].[Sb].[As] Chemical compound [Bi].[Ag].[Sn].[Pb].[Sb].[As] ACWONLHCGMCSPD-UHFFFAOYSA-N 0.000 description 1
- DTIBEWODSYURBV-UHFFFAOYSA-N [Sb]=O.[Cl] Chemical compound [Sb]=O.[Cl] DTIBEWODSYURBV-UHFFFAOYSA-N 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000006256 anode slurry Substances 0.000 description 1
- 229910000413 arsenic oxide Inorganic materials 0.000 description 1
- 229960002594 arsenic trioxide Drugs 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- KTTMEOWBIWLMSE-UHFFFAOYSA-N diarsenic trioxide Chemical compound O1[As](O2)O[As]3O[As]1O[As]2O3 KTTMEOWBIWLMSE-UHFFFAOYSA-N 0.000 description 1
- -1 filters Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 229910052973 jamesonite Inorganic materials 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229950008475 oxophenarsine Drugs 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/04—Working-up slag
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B5/00—Treatment of metallurgical slag ; Artificial stone from molten metallurgical slag
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B7/00—Hydraulic cements
- C04B7/14—Cements containing slag
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B30/00—Obtaining antimony, arsenic or bismuth
- C22B30/04—Obtaining arsenic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/10—Production of cement, e.g. improving or optimising the production methods; Cement grinding
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Ceramic Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
Description
Claims (1)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110260188XA CN102286665B (zh) | 2011-09-05 | 2011-09-05 | 一种复杂含砷及有价金属渣尘物料的综合回收方法 |
PCT/CN2012/080278 WO2013034049A1 (zh) | 2011-09-05 | 2012-08-17 | 一种复杂含砷及有价金属渣尘物料的综合回收方法 |
AU2012306934A AU2012306934B2 (en) | 2011-09-05 | 2012-08-17 | Comprehensive recovery method for complex material containing arsenic and valuable metal slags |
EP12829796.7A EP2682487B1 (en) | 2011-09-05 | 2012-08-17 | Comprehensive recovery method for complex material containing arsenic and valuable metal slags |
CL2013001671A CL2013001671A1 (es) | 2011-09-05 | 2013-06-11 | Método para la recuperación total desde un material complejo de escorias que contienen arsénico y metales valiosos mediante las etapas de volatilizar arsénico; purificar polvos;fundición reductora de las escorias producidas; reducir la escoria del horno de soplado; refinación y tratamiento de la escoria básica. |
ZA2013/05117A ZA201305117B (en) | 2011-09-05 | 2013-07-08 | Comprehensive recovery method for complex material containing aresenic and valuable metal slags |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110260188XA CN102286665B (zh) | 2011-09-05 | 2011-09-05 | 一种复杂含砷及有价金属渣尘物料的综合回收方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102286665A true CN102286665A (zh) | 2011-12-21 |
CN102286665B CN102286665B (zh) | 2012-10-31 |
Family
ID=45333419
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201110260188XA Active CN102286665B (zh) | 2011-09-05 | 2011-09-05 | 一种复杂含砷及有价金属渣尘物料的综合回收方法 |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP2682487B1 (zh) |
CN (1) | CN102286665B (zh) |
AU (1) | AU2012306934B2 (zh) |
CL (1) | CL2013001671A1 (zh) |
WO (1) | WO2013034049A1 (zh) |
ZA (1) | ZA201305117B (zh) |
Cited By (19)
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WO2013034049A1 (zh) * | 2011-09-05 | 2013-03-14 | 耒阳市焱鑫有色金属有限公司 | 一种复杂含砷及有价金属渣尘物料的综合回收方法 |
CN103060570A (zh) * | 2013-01-15 | 2013-04-24 | 昆明理工大学 | 一种污泥有价成分的提取方法 |
CN103602834A (zh) * | 2013-11-07 | 2014-02-26 | 昆明理工大学 | 一种选择性氧化-还原法回收砷锑烟尘中砷、锑的方法 |
CN104294053A (zh) * | 2014-11-01 | 2015-01-21 | 中南大学 | 一种从含砷烟尘还原挥发分离砷的方法 |
CN104451171A (zh) * | 2014-12-18 | 2015-03-25 | 中南大学 | 一种含砷烟尘流态化脱砷的方法 |
CN105506295A (zh) * | 2015-12-31 | 2016-04-20 | 耒阳市焱鑫有色金属有限公司 | 一种联合脱砷提纯砷的方法 |
CN106148728A (zh) * | 2016-07-05 | 2016-11-23 | 湖南博环保科技有限公司 | 一种利用回转窑装置同时处置多种含锌危险废物的方法 |
CN106756059A (zh) * | 2016-12-21 | 2017-05-31 | 中南大学 | 一种从含砷烟尘回收有价金属及沉淀转化法合成固砷矿物的方法 |
CN106756058A (zh) * | 2016-12-21 | 2017-05-31 | 中南大学 | 一种从含砷烟尘中脱砷及其固化的方法 |
CN106834715A (zh) * | 2016-12-21 | 2017-06-13 | 中南大学 | 一种含砷物料的综合利用方法 |
CN106834716A (zh) * | 2016-12-21 | 2017-06-13 | 中南大学 | 一种含砷烟尘脱砷及有价元素综合回收利用的方法 |
CN107739837A (zh) * | 2017-11-01 | 2018-02-27 | 紫金铜业有限公司 | 一种铜冶炼高砷烟灰高效脱砷的方法 |
CN108517415A (zh) * | 2018-05-16 | 2018-09-11 | 中南大学 | 一种砷碱渣中砷与碱的高效分离方法 |
CN108547012A (zh) * | 2018-03-22 | 2018-09-18 | 河南宏泰新材料科技有限公司 | 含砷废料的处理工艺、制备无机纤维的方法以及回收砷的方法 |
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CN109748526A (zh) * | 2019-02-14 | 2019-05-14 | 长沙中硅水泥技术开发有限公司 | 一种水泥窑资源化协同处置砷碱渣工艺***与方法 |
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CN101899574A (zh) * | 2010-08-04 | 2010-12-01 | 锡矿山闪星锑业有限责任公司 | 一种火法炼锑中综合回收砷碱渣和二氧化硫烟气的方法 |
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Also Published As
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WO2013034049A1 (zh) | 2013-03-14 |
CL2013001671A1 (es) | 2013-09-13 |
EP2682487B1 (en) | 2016-07-13 |
EP2682487A4 (en) | 2015-03-18 |
ZA201305117B (en) | 2014-09-25 |
CN102286665B (zh) | 2012-10-31 |
AU2012306934A1 (en) | 2013-08-01 |
AU2012306934B2 (en) | 2015-05-21 |
EP2682487A1 (en) | 2014-01-08 |
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