CN102260959A - Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof - Google Patents
Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof Download PDFInfo
- Publication number
- CN102260959A CN102260959A CN201110172621A CN201110172621A CN102260959A CN 102260959 A CN102260959 A CN 102260959A CN 201110172621 A CN201110172621 A CN 201110172621A CN 201110172621 A CN201110172621 A CN 201110172621A CN 102260959 A CN102260959 A CN 102260959A
- Authority
- CN
- China
- Prior art keywords
- fiber
- doughnut
- cavity
- floccus
- flake
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Nonwoven Fabrics (AREA)
Abstract
The invention discloses a rapid high-rebound high-heat-preservation floccus flake and a preparation method thereof. The elastic heat-preservation floccus flake is prepared by processing raw materials of superfine polyster fiber, hollow fiber with triangular or special-shape holes therein, composite elastic fiber, viscose fiber, polyster fiber with common properties and hollow fiber with a round inner part. The floccus flake is prepared by blending novel high-performance fiber, special fiber, functional fiber and the conventional fiber in different ratios. The obtained floccus flake has the characteristics of quick and high rebound resilience and high heat preservation. The floccus flake meets requirements on lightness of a sleeping bag, compression and rebound, heat preservation, comfortability and the like. The product overcomes the defects of the heat-preserving floccus flake in the conventional sleeping bag, and increases heat preservation ratio and compression resilience ratio.
Description
Technical field
The present invention relates to high insulation flocculus of a kind of quick high resilience and preparation method thereof.
Background technology
At present both at home and abroad the insulation flocculus that uses of sleeping bag mainly contains gum sprayed cotton (containing the elastic force flocculus), hot melting wool, imitative silk flosssilk wadding, melts and sprays cotton, and performance, characteristics are different.
Gum sprayed cotton is the most frequently used common flocculus, advantage be fluffy, resilience good, thickness is arranged, shortcoming is coarse, water-fast the washing not of feel, warming rate is not high.The elastic force flocculus has just increased a small amount of viscose fibre in the gum sprayed cotton production technology, warming and the resilience effect is the same substantially with gum sprayed cotton.
Hot melting wool claims no collodion again, is to utilize viscose fibre as bonding process, and the surface is spraying binder not, is characterized in that air spots is sliding, and floating hair easily gets out the material in face, and warming rate is not high.
Imitative silk flosssilk wadding, the fiber number of fiber than common gum sprayed cotton carry out hot-rolling and plate behind the more surperficial spraying binder, advantage is a surface smoothing, and feel is smooth, water-fast washing, and shortcoming is that compression resilience is relatively poor, and elasticity is bad, and warming rate is high than gum sprayed cotton.
Melt and spray cotton, composition is a polypropylene fibre, through melt-blown process production, with 100g/m
2Be main below the specification.Be characterized in that warming rate of use initial stage is higher, along with using warming rate obviously to descend repeatedly, and easily harden that compression resilience is relatively poor.
Ultra-fine polyester fiber: generally be meant the fiber of fibre number below 0.8dtex, it is a kind of business-like novel synthetic fiber kind that is grown up by Japan phase early 1970s.Claim down-like cotton again, but be the fine fibre of present non-woven production line combing that be characterized in that fiber is superfine, match can effectively be filled up the fibre web space like eider down after the mixing, increase fiber specific surface area, improves the warming rate of flocculus.
Preserve Lay suede fiber, it is a kind of novel high hollow polyester fibre, fiber lumen is sharp triangle, has the same hollow structure of polar bear fur structure, hollow rate is up to 20%, characteristics are flat greatly and not, broken greatly and not, make have light weight behind the flocculus, fluffy, elasticity is lasting, soft, heat-insulating property is excellent.
Composite elastic fiber: be generally bi-component and the curling fiber that is heated.The PET/PBT composite elastic fiber, fiber is made of left and right sides different components, entering the variation that bends of the different left and right sides composition of drying room heating back melting point, forms permanent elastomer.PBT/PET composite elastic fiber and goods thereof are soft, and hygroscopicity, ABRASION RESISTANCE and fiber crimp are good, and the tensile elasticity and the elasticity of compression are fabulous, and its elastic recovery rate is better than the hollow polyester fiber.
Viscose fibre is low-melting-point composite fiber again, is commonly called as core-skin fibre, and the fusing point on fiber top layer and vitrification point are lower than the conventional polyester fiber, be mixed into net enter drying room after the low-melting-point composite fiber fusion, the bonding fibre web.Its effect is that the flocculus pulling force is strengthened, and has water-wash resistance.
Conventional fibre is ordinary polyester fiber (being the polyster fibre of common performance) or common hollow polyester fiber (being that cavity is circular doughnut).
Summary of the invention
The purpose of this invention is to provide a kind of elasticity insulation flocculus and preparation method thereof.
Elasticity insulation flocculus of the present invention obtains according to being prepared as follows method.
The unit mass of elasticity insulation flocculus of the present invention is 149g/m
2, clo value is 2.38, compressive recovery rate is 97%.
The method for preparing the elasticity insulation flocculus provided by the present invention, comprise the steps: that polyster fibre and the rounded doughnut of cavity with ultra-fine polyester fiber, cavity doughnut triangular in shape, composite elastic fiber, viscose fibre, common performance are raw material, processing obtains the elasticity insulation flocculus.
In the said method, the ratio of quality and the number of copies of the doughnut that the polyster fibre of described ultra-fine polyester fiber, cavity doughnut triangular in shape, composite elastic fiber, viscose fibre, common performance and cavity are rounded is: 15~25: 15~25: 5~15: 7~10: 10~25: 15~25, or 15~25: 15~25: 5~15: 7~10: 15~25: 15~25, or 15~25: 15~25: 5~15: 7~10: 10~15: 15~25.
In above-mentioned arbitrary described method, described composite elastic fiber is the PET/PBT composite elastic fiber; The fusing point of described viscose fibre is 150 ℃; Described cavity doughnut triangular in shape is that cavity is sharp leg-of-mutton doughnut.
In above-mentioned arbitrary described method,
The fineness of described ultra-fine polyester fiber is 0.78dtex, and length is 32mm to 51mm;
The fineness of the doughnut that described cavity is triangular in shape is 1.56dtex to 1.67dtex, and length is 38mm to 51mm;
The fineness of described composite elastic fiber is 2.22dtex, and length is 38mm to 51mm;
The fineness of described viscose fibre is 4.0dtex, and length is 38mm to 51mm;
The fineness of the polyster fibre of described common performance is 1.33dtex to 1.8dtex, and length is 38mm to 51mm;
The fineness of the doughnut that described cavity is rounded is 3.33dtex~6.64dtex, and length is 54mm to 64mm.
In above-mentioned arbitrary described method, described processing steps is as follows: mixing, shredding, combing, lapping, spray glue, oven dry, cooling.
In above-mentioned arbitrary described method, described oven dry is carried out under 110 ℃~120 ℃, 130 ℃~145 ℃, 155 ℃~170 ℃ temperature successively.
In the said method, ultra-fine polyester fiber can effectively be filled up the fibre web space, increases fiber specific surface area, improves the warming rate of flocculus.
Inside is the doughnut in triangle or different hole, makes the flocculus resistance to compression.
Composite elastic fiber, be generally bi-component and the curling fiber that is heated, make the flocculus high resilience.
Viscose fibre bonds together the various components in the flocculus.
Ordinary polyester fiber and inside are circular doughnut, and the fiber for very conventional plays skeleton, closely knit and elastic force effect in flocculus.
Sleeping bag or the tent made by elasticity insulation flocculus of the present invention also belong to protection scope of the present invention.
The flocculus of the present invention preparation adopts the different proportionings of novel high-performance fiber, special fibre, functional fiber and conventional fibre and is mixed and made into.The flocculus that obtains has quick high resilience and the good characteristics of warmth retention property.Adapt to sleeping bag in light weight, compress, resilience is quick, requirement such as warming, comfortable.This product should overcome the shortcoming and defect that existing sleeping bag has been used insulation flocculus, improves warming rate, the compression rebound rate of flocculus.
The specific embodiment
Employed experimental technique is conventional method if no special instructions among the following embodiment.
Used material, reagent etc. if no special instructions, all can obtain from commercial channels among the following embodiment.
The preparation of embodiment 1, elasticity insulation flocculus
One, raw material (preferably)
0.78dtex * 32mm specification ultra-fine polyester fiber, 15 parts by mass;
1.67dtex * 38mm specification is preserved Lay suede fiber, 25 parts by mass;
2.22dtex * 51mm specification PET/PBT composite elastic fiber, 5 parts by mass;
4.0dtex * 51mm specification low-melting-point composite fiber (fusing point is 150 ℃), 7 parts by mass;
1.33dtex * 38mm specification ordinary polyester fiber, 16 parts by mass;
6.64dtex the common hollow polyester fiber of * 64mm specification, 16 parts by mass.
Two, technology
Adopt nonwoven manufacturing technique, step is: mix, first shredding, smart shredding, combing, lapping, spray glue, oven dry, cooling, cutting edge, coiling, cutting form flocculus finished product volume.
Wherein, oven dry is adopted gradual, three layers of drying room, and near-bottom temperature is controlled at 115 ℃, and the middle level temperature is controlled at 140 ℃, and the upper strata temperature is controlled at 165 ℃.
Three, properties of product detect
Every is detected index and all uses same instrument to test under the same conditions.
The detection method of compressive recovery rate: FZ/T 64003-1993 gum sprayed cotton flocculus;
Clo value (CLO) detection method: the mensuration of GB/T 11048-1989 insulating property of textile;
3 repetitions are established in experiment, and the result is as shown in table 1.
Table 1, flocculus effect
The preparation of embodiment 2, elasticity insulation flocculus
One, raw material (minimum)
0.78dtex * 40mm specification ultra-fine polyester fiber 20 parts by mass;
1.56dtex * 40mm specification is preserved Lay suede fiber 15 parts by mass;
2.22dtex * 38mm specification PET/PBT composite elastic fiber 10 parts by mass;
4.0dtex * 38mm specification low-melting-point composite fiber (fusing point is 150 ℃) 8 parts by mass;
1.8dtex * 51mm specification ordinary polyester fiber 10 parts by mass;
Common hollow polyester fiber 15 parts by mass of fineness 5.33dtex * 54mm specification.
Two, technology
Method is with consistent described in the embodiment 1, and different is in the baking step, and near-bottom temperature is controlled at 110 ℃, and the middle level temperature is controlled at 130 ℃, and the upper strata temperature is controlled at 155 ℃.
Three, flocculus effect: do not have significant difference with embodiment 1 gained flocculus effect.
The preparation of embodiment 3, elasticity insulation flocculus
One, raw material (maximum)
0.78dtex * 51mm specification ultra-fine polyester fiber 25 parts by mass;
1.60dtex * 51mm specification is preserved Lay suede fiber 20 parts by mass;
2.22dtex * 40mm specification PET/PBT composite elastic fiber 15 parts by mass;
4.0dtex * 40mm specification low-melting-point composite fiber (fusing point is 150 ℃) 10 parts by mass;
1.50dtex * 40mm specification ordinary polyester fiber 25 parts by mass;
6.64dtex common hollow polyester fiber 25 parts by mass of * 60mm specification.
Two, technology
Method is with consistent described in the embodiment 1, and different is in the baking step, and near-bottom temperature is controlled at 120 ℃, and the middle level temperature is controlled at 145 ℃, and the upper strata temperature is controlled at 170 ℃.
Three, flocculus effect: do not have significant difference with embodiment 1 gained flocculus effect.
Claims (9)
1. method for preparing the elasticity insulation flocculus, comprise the steps: that polyster fibre and the rounded doughnut of cavity with ultra-fine polyester fiber, cavity doughnut triangular in shape, composite elastic fiber, viscose fibre, common performance are raw material, processing obtains the elasticity insulation flocculus.
2. method according to claim 1, it is characterized in that: the ratio of quality and the number of copies of the doughnut that the polyster fibre of described ultra-fine polyester fiber, cavity doughnut triangular in shape, composite elastic fiber, viscose fibre, common performance and cavity are rounded is: 15~25: 15~25: 5~15: 7~10: 10~25: 15~25, or 15~25: 15~25: 5~15: 7~10: 15~25: 15~25, or 15~25: 15~25: 5~15: 7~10: 10~15: 15~25.
3. method according to claim 1 and 2 is characterized in that:
Described composite elastic fiber is the PET/PBT composite elastic fiber; Described cavity doughnut triangular in shape is that cavity is sharp leg-of-mutton doughnut.
4. according to arbitrary described method among the claim 1-3, it is characterized in that:
The fineness of described ultra-fine polyester fiber is 0.78dtex, and length is 32mm to 51mm;
The fineness of the doughnut that described cavity is triangular in shape is 1.56dtex to 1.67dtex, and length is 38mm to 51mm;
The fineness of described composite elastic fiber is 2.22dtex, and length is 38mm to 51mm;
The fineness of described viscose fibre is 4.0dtex, and length is 38mm to 51mm;
The fineness of the polyster fibre of described common performance is 1.33dtex to 1.8dtex, and length is 38mm to 51mm;
The fineness of the doughnut that described cavity is rounded is 3.33dtex~6.64dtex, and length is 54mm to 64mm.
5. according to arbitrary described method among the claim 1-4, it is characterized in that: described processing steps is as follows: mixing, shredding, combing, lapping, spray glue, oven dry, cooling.
6. according to arbitrary described method among the claim 1-5, it is characterized in that: described oven dry is carried out under 110 ℃~120 ℃, 130 ℃~145 ℃, 155 ℃~170 ℃ temperature successively.
7. the elasticity insulation flocculus for preparing by arbitrary described method among the claim 1-6.
8. elasticity insulation flocculus according to claim 7 is characterized in that: the unit mass of described elasticity insulation flocculus is 149g/m
2, clo value is 2.38, compressive recovery rate is 97%.
9. sleeping bag or the tent of making by claim 7 or 8 described elasticity insulation flocculus.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110172621A CN102260959A (en) | 2011-06-24 | 2011-06-24 | Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110172621A CN102260959A (en) | 2011-06-24 | 2011-06-24 | Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN102260959A true CN102260959A (en) | 2011-11-30 |
Family
ID=45007783
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201110172621A Pending CN102260959A (en) | 2011-06-24 | 2011-06-24 | Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102260959A (en) |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104233483A (en) * | 2014-08-28 | 2014-12-24 | 湖州通益环保纤维股份有限公司 | Three-dimensional hollow down-like short fiber |
CN106120153A (en) * | 2016-08-30 | 2016-11-16 | 丹阳市宇晟纺织新材料有限公司 | A kind of energy-efficient method for shaping of high resiliency any surface finish glue-free cotton |
CN106436012A (en) * | 2015-08-13 | 2017-02-22 | 蒋敏容 | Functional floccules and product |
CN107253335A (en) * | 2017-04-28 | 2017-10-17 | 昆山胜昱无纺布有限公司 | A kind of high resilience thermal non-woven fabric |
CN107401007A (en) * | 2017-08-30 | 2017-11-28 | 江苏鑫轮特种纤维科技发展有限公司 | A kind of preparation of novel antibacterial Composite Double functional fibre and its application method |
CN107429454A (en) * | 2015-01-21 | 2017-12-01 | 普莱玛有限公司 | Anti-migration batting with draftability and preparation method thereof and the product including the batting |
CN107523937A (en) * | 2017-09-01 | 2017-12-29 | 江苏鑫轮特种纤维科技发展有限公司 | The preparation of antibacterial Composite Double functional fibre and its application method |
CN108221174A (en) * | 2018-02-01 | 2018-06-29 | 中国人民解放军62023部队 | A kind of far-infrared warm flame retarding function flocculus and preparation method thereof |
CN109914033A (en) * | 2019-03-07 | 2019-06-21 | 福建省晋江市恒丰喷胶棉织造有限公司 | A kind of glue spraying cotton material and preparation method thereof |
CN111648025A (en) * | 2020-03-23 | 2020-09-11 | 东华大学 | Micro-nano fiber warming flocculus with longitudinal variable density structure and preparation method thereof |
CN112411007A (en) * | 2020-11-19 | 2021-02-26 | 湖州欣缘纺织有限公司 | Fluffy polyester wadding sheet with good warm-keeping effect |
CN114293317A (en) * | 2021-12-30 | 2022-04-08 | 湖南名品实业股份有限公司 | Mixed fiber material and preparation method thereof |
CN114855363A (en) * | 2022-05-30 | 2022-08-05 | 江苏美罗家用纺织品有限公司 | Silk-like cotton made from soybean and processing method thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1644779A (en) * | 2005-01-17 | 2005-07-27 | 东华大学 | Production of silk cotton wadding material |
CN101476212A (en) * | 2009-01-19 | 2009-07-08 | 汕头市奥山服饰有限公司 | Thermal protection flocculus and manufacturing method thereof |
CN101481851A (en) * | 2009-01-19 | 2009-07-15 | 汕头市奥山服饰有限公司 | Thermal protection flocculus and manufacturing method thereof |
CN101718024A (en) * | 2009-12-15 | 2010-06-02 | 汕头市奥山服饰有限公司 | Insulation flocculus and manufacture method thereof |
-
2011
- 2011-06-24 CN CN201110172621A patent/CN102260959A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1644779A (en) * | 2005-01-17 | 2005-07-27 | 东华大学 | Production of silk cotton wadding material |
CN101476212A (en) * | 2009-01-19 | 2009-07-08 | 汕头市奥山服饰有限公司 | Thermal protection flocculus and manufacturing method thereof |
CN101481851A (en) * | 2009-01-19 | 2009-07-15 | 汕头市奥山服饰有限公司 | Thermal protection flocculus and manufacturing method thereof |
CN101718024A (en) * | 2009-12-15 | 2010-06-02 | 汕头市奥山服饰有限公司 | Insulation flocculus and manufacture method thereof |
Non-Patent Citations (2)
Title |
---|
翁和生: "葆莱绒被芯制品的研究与开发", 《上海纺织科技》 * |
高秀丽等: "葆莱绒纤维结构与其织物的相关性能研究", 《上海纺织科技》 * |
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104233483A (en) * | 2014-08-28 | 2014-12-24 | 湖州通益环保纤维股份有限公司 | Three-dimensional hollow down-like short fiber |
US10954615B2 (en) | 2015-01-21 | 2021-03-23 | Primaloft, Inc. | Migration resistant batting with stretch and methods of making and articles comprising the same |
CN107429454A (en) * | 2015-01-21 | 2017-12-01 | 普莱玛有限公司 | Anti-migration batting with draftability and preparation method thereof and the product including the batting |
JP2018509529A (en) * | 2015-01-21 | 2018-04-05 | プリマロフト,インコーポレイテッド | Transition resistant batting having stretchability, method for producing the batting, and article containing the batting |
CN106436012A (en) * | 2015-08-13 | 2017-02-22 | 蒋敏容 | Functional floccules and product |
CN106120153A (en) * | 2016-08-30 | 2016-11-16 | 丹阳市宇晟纺织新材料有限公司 | A kind of energy-efficient method for shaping of high resiliency any surface finish glue-free cotton |
CN107253335A (en) * | 2017-04-28 | 2017-10-17 | 昆山胜昱无纺布有限公司 | A kind of high resilience thermal non-woven fabric |
CN107401007A (en) * | 2017-08-30 | 2017-11-28 | 江苏鑫轮特种纤维科技发展有限公司 | A kind of preparation of novel antibacterial Composite Double functional fibre and its application method |
CN107523937A (en) * | 2017-09-01 | 2017-12-29 | 江苏鑫轮特种纤维科技发展有限公司 | The preparation of antibacterial Composite Double functional fibre and its application method |
CN108221174A (en) * | 2018-02-01 | 2018-06-29 | 中国人民解放军62023部队 | A kind of far-infrared warm flame retarding function flocculus and preparation method thereof |
CN108221174B (en) * | 2018-02-01 | 2019-12-10 | 军事科学院***工程研究院军需工程技术研究所 | Far infrared thermal insulation flame-retardant functional flocculus and preparation method thereof |
CN109914033A (en) * | 2019-03-07 | 2019-06-21 | 福建省晋江市恒丰喷胶棉织造有限公司 | A kind of glue spraying cotton material and preparation method thereof |
CN111648025A (en) * | 2020-03-23 | 2020-09-11 | 东华大学 | Micro-nano fiber warming flocculus with longitudinal variable density structure and preparation method thereof |
CN111648025B (en) * | 2020-03-23 | 2021-10-26 | 东华大学 | Micro-nano fiber warming flocculus with longitudinal variable density structure and preparation method thereof |
CN112411007A (en) * | 2020-11-19 | 2021-02-26 | 湖州欣缘纺织有限公司 | Fluffy polyester wadding sheet with good warm-keeping effect |
CN114293317A (en) * | 2021-12-30 | 2022-04-08 | 湖南名品实业股份有限公司 | Mixed fiber material and preparation method thereof |
CN114855363A (en) * | 2022-05-30 | 2022-08-05 | 江苏美罗家用纺织品有限公司 | Silk-like cotton made from soybean and processing method thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102260959A (en) | Rapid high-rebound high-heat-preservation floccus flake and preparation method thereof | |
CN101476212B (en) | Manufacturing method of thermal protection flocculus | |
CN101481851A (en) | Thermal protection flocculus and manufacturing method thereof | |
CN101718024A (en) | Insulation flocculus and manufacture method thereof | |
CN101109135A (en) | High stretch soft cotton and manufacturing method thereof | |
NO124547B (en) | ||
CN103306050A (en) | Preparation method of tailorable and washable silk floss flocculus | |
CN102689469B (en) | A kind of composite double layer non-weaving cloth and preparation method thereof | |
CN106012287A (en) | Multifunctional waffle cotton thermal batting and preparation method thereof | |
CN109629118A (en) | A kind of cloth for cleaning and its manufacturing method | |
CN104323636B (en) | A kind of multipurpose cotton-wadded quilt and manufacture craft thereof | |
CN105908369A (en) | Double-side shaped glue-free cotton wadding and manufacturing method thereof | |
CN103061034A (en) | Production method of silk-like cotton | |
CN109056190A (en) | A kind of temperature controllable can generating negative ions cushion and bedding core production method | |
CN113235221A (en) | Water-repellent heat-storage warm-keeping flocculus and preparation method thereof | |
CN103182816B (en) | A kind of uniform high-performance leather base cloth | |
CN108914378A (en) | A kind of wadding and preparation method thereof, heat insulating products | |
CN207313862U (en) | A kind of compound loft nonwoven material of multicomponent | |
CN103590195A (en) | Method for making acupuncture cotton with abnormal-shaped surface | |
CN114481437A (en) | Polylactic acid fiber and silk vertical cotton wadding and preparation method thereof | |
CN113279136B (en) | Pearl fiber composite thermal insulating flocculus and preparation method thereof | |
TW201723260A (en) | Vertical cotton and preparation method thereof having applications to filtration, heat insulation, and sound absorption | |
CN104816513B (en) | A kind of film flocking formula high-elastic heat insulation flaky material and its manufacture method | |
CN111002645A (en) | Method for manufacturing high-efficiency warm velvet fiber core material | |
CN109910382A (en) | A kind of lace needle thorn composite material production technology |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C12 | Rejection of a patent application after its publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20111130 |