CN101912161B - Mint tobacco filter stick and preparation method thereof - Google Patents
Mint tobacco filter stick and preparation method thereof Download PDFInfo
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- CN101912161B CN101912161B CN2010102536439A CN201010253643A CN101912161B CN 101912161 B CN101912161 B CN 101912161B CN 2010102536439 A CN2010102536439 A CN 2010102536439A CN 201010253643 A CN201010253643 A CN 201010253643A CN 101912161 B CN101912161 B CN 101912161B
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Abstract
The invention discloses a filter material of a cigarette filter stick and a composite filter stick made of the same. The filter material comprises a fiber base material and a plasticizer, wherein a Chinese herbal medicinal mixture of 3 to 4 weight parts of mint and 2 to 3 weight parts of blackberrykiky rhizome and 4 weight parts of tobacco leaf powder particles are added into the fiber base material; the granularity of the mixed particles is 40 to 80 meshes; and the additive amount is that each millimeter of filter stick contains 1.0 to 1.5mg of Chinese herbal medicinal mixed particles. The mint and blackberrykiky rhizome mixed particles are used as the adsorbing material of the functional composite filter stick, and factors such as the additive proportion and additive amount of the mint and the blackberrykiky rhizome, the granularity of the particles, the additive amount of the plasticizer and the like are determined. A cigarette finished product consists of the composite filter stick, cut tobacco and cigarette paper rolls and can effectively reduce harmful substances in smoke, cannot influence the flavor of cigarettes, and has the effects of moistening throat, hydrating, reducing the stimulation of the smoke to the throat and the like.
Description
Technical field
The invention belongs to the production of cigarettes field, be specifically related to a kind of filter bar for cigarette and preparation method thereof.
Background technology
Cigarette produces harmful substances such as CO, tar in aspiration procedure, the smoking time one is long, and that smoker throat just has is dry, itch, cough even sore symptom.The raising of Along with people's health perception is had higher requirement to the security of cigarette.Cigarette filter rod to promoting the cigarette smoking quality, filters the harmful substance in the flue gas as the filtering material of cigarette smoke, improves cigarette security aspect and all has important function.In recent years, countries in the world were also increasing to the research of new type functional filter stick.
Domestic applications patent " a kind of new cigarette filter stick is with filtering material and preparation method ", application number: 200710066121.6, a kind of expanded cabo particle that adopts is disclosed as filter stick for cigarettes of filtering material and preparation method thereof.Number of patent application 200910172250.2 discloses a kind of new material that can effectively adsorb sour gas, and this material is introduced different basic groups through porous material is carried out chemical modification.This material is made an addition to cigarette filter rod, can reduce hydrogen cyanide burst size in the cigarette mainstream flue gas.Number of patent application 200720155556.3 discloses the filter stick that has Pu'er tea, adopts harmful substance that the cigarette of this filter stick can reduce volatility and half volatile in the main flume most effectively like nitrite, BaP, tar etc.Number of patent application: 03260500.5 discloses a kind of vinegar fibre adds nanometer noble metal catalyst binary compound filter candle, and this filter stick can effectively reduce the content of carbon monoxide in the cigarette smoke.
At present; Most of both at home and abroad research all is that porous prilled material is added in the filter stick; When cigarette smoking, the main flume filter stick of flowing through, the porous material in the filter stick produces suction-operated to flue gas; Harmful substance is adsorbed on the porous particle, thereby has reduced the content of harmful substance in main flume.But in the harmful substance of porous material in the absorption flue gas, also the fragrance component in the flue gas has been adsorbed, thereby the suction quality of reduction cigarette.In addition, the particle majority that adds in the filter stick is to adopt chemical method to handle to obtain, and the security of himself remains further research, and material price cost such as noble metal is higher.Therefore, when the requirement because of reducing tar and reducing harm reduces the harmful components in the flue gas, how to keep the perfume quantity of cigarette, improve the suction quality of cigarette, become the difficult problem that scientific and technical personnel are badly in need of solving.
Summary of the invention
The purpose of this invention is to provide a kind of peppermint cigarette that contains the Chinese herbal medicine particle and use composite filter, the perfume quantity when aspirating to increase promotes the suction dry, alleviates the excitant of flue gas to smoker throat.
Another object of the present invention provides the preparation method of above-mentioned composite filter.
The present invention realizes above-mentioned purpose through following scheme.
A kind of mint tobacco filter stick contains peppermint, the Chinese herbal medicine particle of blackberry lily composition and the mixture of tobacco leaf powder particle, as filtering material in the filter stick.Peppermint, blackberry lily and tobacco leaf powder particle three's mass ratio is in the mixture: 3～4 parts of peppermints, 2～3 parts of blackberry lilys, 4 parts in tobacco leaf powder.The Chinese herbal medicine particle that peppermint, blackberry lily are formed is with behind peppermint and the blackberry lily preliminarily dried, mixes 40～80 mesh sieves after the pulverizing again, moisture regain then under 40～60 ℃, dry to moisture be 6～10%.
Can adopt following this mint tobacco filter stick of step preparation:
(1) take from the peppermint base of leaf of right drying, the blackberry lily rhizome is 40～60 ℃ of oven dry down, dry to moisture be 8%～12%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 40～80 mesh sieves, get peppermint powder particle and Blackberrylily Rhizome particle.
(2) the peppermint cigarette of getting certain trade mark is used pipe tobacco, under 40～60 ℃, dry by the fire to moisture be 8%～10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 40～80 mesh sieves, get the tobacco powder particle.
(3) above-mentioned three kinds of powder particles are mixed, the quality of various particles is: 3～4 parts of peppermints, and 2～3 parts of blackberry lilys, 4 parts in tobacco leaf powder, then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.
(4) processed is carried out to compound particles in moisture regain back, at low temperatures (40～60 ℃) dry to moisture be 6%～10%.
(5) carry out perfuming after the dehydration and handle, the ratio with 0.05% adds menthol to compound particles, mixes, and leaves standstill and stores 48h, promptly gets the peppermint cigarette and uses the composite filter particle.
In this composite filter, the content of hybrid particles is include mixed particle 1～1.5mg in the filter stick of every mm length.These Chinese herbal medicine hybrid particles are dispersed in the tow of filter stick.Its manufacturing process comprises the steps:
(1) compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.
(2) adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up; Then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm; 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.0～1.5mg/mm.
Test is found, Chinese herbal medicine that the present invention is used and tobacco powder particle, and its size just is applicable to and is added in the filter stick, and it comparatively stably is dispersed in the filter stick tow, is difficult for being scattered; Filter stick Chinese herbal medicine and tobacco composition particle have the cigarette flavor of increasing amount simultaneously, reduce the flue gas excitant, promote the effect of cigarette smoking quality, can reduce the harmful substance contents in the flue gas effectively simultaneously.The more important thing is; Different with most of harm reduction filter sticks, the blackberry lily particle makes an addition in the filter stick, reduces the harmful substance contents in the main flume; But the fragrance component in the time of can't adsorbing the cigarette suction; The active ingredient that blackberry lily evaporated can be alleviated the stimulation of flue gas, but can not produce the assorted flavor of peculiar smell, and these characteristics are fit to it very much should be in cigarette filter rod.This hybrid particles is under the situation of the applied amount of 1～1.5mg; The mixture of Chinese herbal medicines powder is present in the filter stick; Can not cause the cigarette odor-absorbing obvious variation; Even promoted the suction fragrance of cigarette, infer that this possibly be that the smell of blackberry lily helps transferring the fragrance component of pipe tobacco, thereby fragrance is further promoted; And the formed cigarette smell coordination of the combination of blackberry lily and peppermint is fit to be applied in the mentholated cigarette.
Compared with prior art, the present invention has following beneficial effect:
1. the invention property ground adds Chinese herbal medicine such as blackberry lily, peppermint and tobacco particle in the filter stick; This filter stick is applied on the peppermint cigarette; When not changing the cigarette smoking style; The perfume quantity of cigarette be can increase, and natural mint flavored, thereby the suction mouthfeel and the suction quality of cigarette effectively improved.
2. though composite filter provided by the present invention has added the mixture of Chinese herbal medicines particle; But can't cause negative effect to the suction style of cigarette product, simultaneously during cigarette smoking, the volatilization of being heated of the active ingredient in peppermint and the blackberry lily; Suck together in smoker's mouth in company with main flume; Can alleviate the excitant of flue gas to a certain extent, have and wet one's whistle, preserve moisture, alleviate the effects such as excitant of flue gas throat to smoker throat.
3. composite filter provided by the present invention cigarette mainstream flue gas is had certain dam, filtering function, can reduce the harmful substance contents in the main flume to a certain extent.
4. Chinese herbal medicine that composite filter provided by the present invention added and tobacco composition particle can firmly be scattered in the filter stick, are difficult for being scattered, and filter stick is made moulding and cigarette finished product prepares the equal easy operating of process.
5. the material that on filter stick, adds of the present invention is a natural plants, without chemical treatment, and safety and sanitation, and cheap, obtain easily.
The specific embodiment
Below further specify technical scheme of the present invention through concrete embodiment.In order to verify that further beneficial effect of the present invention, the present invention also will adopt this filter stick cigarette that makes and the contrast cigarette contrast of not using this filter stick, carry out sensory evaluating smoking and flue gas analysis test.
Embodiment 1
Take from the peppermint base of leaf 5kg of right drying, blackberry lily rhizome 5kg is 60 ℃ of down oven dry, dry to moisture be 12%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get peppermint powder particle and Blackberrylily Rhizome particle.Get in the Guangdong cigarette A trade mark peppermint cigarette and use pipe tobacco, under 60 ℃, dry by the fire to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the tobacco powder particle.Above-mentioned three kinds of powder particles are even with 3: 3: 4 mixed, and then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.Processed is carried out to compound particles in moisture regain back, at low temperatures (60 ℃) dry to moisture be 10%.Carry out perfuming after the dehydration and handle, the ratio with 0.05% adds menthol to compound particles, mixes, and leaves standstill and stores 48h, promptly gets the peppermint cigarette and uses the composite filter particle.
Compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.Adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up; Then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm; 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.5mg/mm.
Adopt A trade mark peppermint pipe tobacco, cigarette paper, the tipping paper of Guangdong China Tobacco Industry Co.,Ltd and the composite filter that makes as stated above to roll into cigarette finished product together.
To contain the following experiment of cigarette process of above-mentioned composite filter:
Experimental group: cigarette is 400 as stated; Control group: do not adopt above-mentioned filter stick, but 400 of all identical regular-size cigarettes of pipe tobacco and cigarette paper, tipping paper.
Cigarette smoke analytical test: press GB/T 19609-2004 " cigarette is measured TPM and tar with conventional analysis with smoking machine " and GB/T 23356-2009 " the non-scattering infrared method of the mensuration of carbon monoxide in the cigarette smoke gas phase " and measure flue gas TPM (TPM), tar and carbon monoxide (CO) content; Press GB/T 21130-2007 " mensuration of benzo in the cigarette smoke TPM
pyrene " and measure benzo
pyrene in the main flume; Press YC/T 255---2008 " the mensuration high performance liquid chromatographies of main phenolic compound in the cigarette mainstream flue gas " are measured phenol; Press YC/T 254---2008 " the mensuration high performance liquid chromatographies of main carbonyls in the cigarette mainstream flue gas " are measured the crotonaldehyde in the main flume, press YC/T253-2008 " the mensuration continuous flow method of hydrogen cyanide in the cigarette mainstream flue gas " and measure the hydrogen cyanide in the main flume.The measuring result is as shown in table 1.
Table 1 flue gas analysis result
Can know from table 1; Compare with control samples; Under the approaching situation of both puff numbers; In the test appearance main flume except that the CO content not quite; The content of all the other smoke components such as phenol, crotonaldehyde, hydrogen cyanide and benzo
pyrene all has reduction in various degree, and this shows that the particle in the filter stick all has certain adsorption filtration effect to the harmful substance in the main flume, can effectively reduce harmful substance contents in the flue gas.
Sensory evaluating smoking's test: according to GB GB 5606.5-2005 " cigarette the 4th part: sense organ specification requirement " cigarette sample is carried out the sensory evaluating smoking, smoking result is as shown in table 2.
Table 2 cigarette sample sensory evaluating smoking gets submeter
Sensory evaluating smoking result shows; Compare with control samples, aesthetic quality's integrate score of embodiment 1 sample improves 2.86, is mainly reflected in three aspect scores such as fragrance, excitant and pleasant impression and is improved; Especially the score aspect excitant is more remarkable, and the lifting amplitude reaches 0.83.According to judging panel's conclusion, embodiment 1 sample can effectively alleviate the stimulation of flue gas to throat, has certain effect that wets one's whistle, promotes the production of body fluid.
In sum, composite filter of the present invention can effectively reduce the harmful substance contents in the flue gas, can alleviate the stimulation of flue gas to throat simultaneously, has certain effect that wets one's whistle, promotes the production of body fluid, thereby promotes the suction quality of cigarette.
Claims (10)
1. a cigarette is used the peppermint filter stick, comprises fiber base material and plasticizer, it is characterized in that: contain the Chinese herbal medicine hybrid particles be made up of peppermint, blackberry lily and the mixture of tobacco leaf powder particle in the described fiber base material.
2. filter stick as claimed in claim 1 is characterized in that: the weight ratio of peppermint, blackberry lily and tobacco leaf powder is in the described mixture: 3～4 parts of peppermints, 2～3 parts of blackberry lilys, 4 parts in tobacco leaf powder.
3. filter stick as claimed in claim 2 is characterized in that: described Chinese herbal medicine hybrid particles is after peppermint and blackberry lily are pulverized, after 40～80 mesh sieves, the peppermint of acquisition and blackberry lily mix powder, under 40～60 ℃, dry by the fire to moisture be 6～10%.
4. filter stick as claimed in claim 1 is characterized in that: in the described filter stick, the content of Chinese herbal medicine hybrid particles is to contain Chinese herbal medicine hybrid particles 1.0～1.5mg in the filter stick of every mm length.
5. filter stick as claimed in claim 4 is characterized in that: described Chinese herbal medicine hybrid particles evenly makes an addition in the fiber base material.
6. filter stick as claimed in claim 1 is characterized in that: described fiber base material is the diacetate fiber tow.
7. filter stick as claimed in claim 1 is characterized in that: described plasticizer addition is 5%～8% of a filtering material gross weight.
8. a cigarette is used the peppermint filter stick, comprises the shaping paper of filter core and parcel filter core, it is characterized in that said filter core saves the identical filter core of cross-sectional areas by at least two and forms, and said filter core adjacent face contacts with each other; Said filter core has at least a joint to contain the Chinese herbal medicine hybrid particles be made up of peppermint, blackberry lily and the mixture of tobacco leaf powder particle.
9. filter stick according to claim 8 is characterized in that a joint that described filter core contacts with cigarette shreds contains the Chinese herbal medicine hybrid particles be made up of peppermint, blackberry lily and the mixture of tobacco leaf powder particle.
10. filter stick according to claim 8 is characterized in that described shaping paper air permeability is 10000CU (Coresta), quantitatively is 28g/m
2
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010102536439A CN101912161B (en) | 2010-08-13 | 2010-08-13 | Mint tobacco filter stick and preparation method thereof |
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| CN2010102536439A CN101912161B (en) | 2010-08-13 | 2010-08-13 | Mint tobacco filter stick and preparation method thereof |
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| CN101912161A CN101912161A (en) | 2010-12-15 |
| CN101912161B true CN101912161B (en) | 2012-05-02 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302220A (en) * | 2011-08-28 | 2012-01-04 | 云南烟草科学研究院 | Application of lemon balm to binary composite filter tips |
| CN102423135A (en) * | 2011-08-28 | 2012-04-25 | 云南烟草科学研究院 | Application of mint leaves and Pu'er tea in ternary composite filter tips |
| CN102691170B (en) * | 2012-06-06 | 2014-12-24 | 云南瑞升烟草技术（集团）有限公司 | High tar reduction diacetate fiber non-woven fabric filter material for cigarettes and preparation method for filter material |
| CN103054186B (en) * | 2012-12-27 | 2014-12-10 | 广东中烟工业有限责任公司 | Chinese medicinal composite particle filter stick and preparation method thereof |
| CN103126072A (en) * | 2013-02-22 | 2013-06-05 | 红云红河烟草(集团)有限责任公司 | Natural plant particles capable of improving sweetness and moisture retention of cigarette and application thereof |
| CN103393219B (en) * | 2013-08-14 | 2014-09-24 | 中国烟草总公司郑州烟草研究院 | Modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and preparation method of modified natural plant filter tip additive material |
| CN106723306B (en) * | 2017-01-16 | 2018-05-18 | 云南中烟新材料科技有限公司 | A kind of method that cigarette filter rod additive is prepared with American mint |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US5025812A (en) * | 1989-08-10 | 1991-06-25 | R. J. Reynolds Tobacco Company | Tobacco processing |
| CN1064221C (en) * | 1998-04-28 | 2001-04-11 | 华磊 | Nutritive health cigarette and its preparing process |
| CN101711601B (en) * | 2009-12-28 | 2012-12-05 | 四川农业大学 | Drug cigarette and processing method thereof |
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