CN106723306B - A kind of method that cigarette filter rod additive is prepared with American mint - Google Patents
A kind of method that cigarette filter rod additive is prepared with American mint Download PDFInfo
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- CN106723306B CN106723306B CN201710032545.4A CN201710032545A CN106723306B CN 106723306 B CN106723306 B CN 106723306B CN 201710032545 A CN201710032545 A CN 201710032545A CN 106723306 B CN106723306 B CN 106723306B
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- cigarette
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- powder
- american mint
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of methods that cigarette filter rod additive is prepared with American mint.Raw material is wanted based on the American mint leaf of freeze-drying, fireworks petal and red big tobacco leaf, and pass through that low-temperature submicron powder is broken to crush processing to three kinds of raw materials, then tobacco jelly powder is added in raw material powder again, subsequent material by mixing, extruding, broken, shaping and screening process, forms the granular material that granularity is 30~60 mesh successively.It is added to by the dosage of 1~3mg/mm in filter stick tow, the sweet sense of cigarette smoke can be increased and sense of promoting the production of body fluid, reduction cigarette smoke irritation enrich cigarette flavor, the suction quality of cigarette made to be promoted with obtaining conspicuousness.
Description
Technical field
The invention belongs to cigarette supplementary technical fields, are related to cigarette filter material, are specifically related to one kind with American mint
The method that cigarette filter rod additive is prepared as primary raw material.
Background technology
As the public is to the pay attention to day by day smoked with health problem, produces and be harmful in low-coke tar cigarette, reduction cigarette smoke
Content of material improves smoking property of cigarette security, becomes one of main direction of studying of tobacco researcher.
By numerous studies and experiment, it can be designed by tobacco leaf formulation and the system design of cigarette auxiliary material realizes cigarette
The purpose of lowering harm and decreasing coking.In tobacco leaf formulation design process, using materials such as reconstituted tobacoo, expanded cut stem, expanding tobacco particles,
Significantly reduce cigarette tar content；In auxiliary material design process, filtered by high porosity plug wrap paper, hole-punching huon pine paper, high resistance to suction
Materials and the skills such as stick, the high filter stick (such as papery composite filter, activated carbon composite filter) of cigarette paper and high adsorption base material thoroughly
The application of art realizes the reduction of coke tar in cigarette and flue gas harmful substance contents.But these technologies, material are applied to cigarette
Afterwards, although harmfulness reduces, the sucking quality of cigarette is also adversely affected.
Cigarette how is balanced while reducing tar and reducing harm sucks mouthfeel and quality, scientific research personnel from essence spice for cigarette and
Cigarette filter-tip additive agent and material set out, and have carried out numerous studies and experiment.Wherein, although the use of essence spice for cigarette can be with
The fragrance loss after Harm reduction techniques tar reduction is made up, the sweet sense of cigarette smoke is improved, reduces the irritation of cigarette smoke, but cigarette
With essence and flavoring agent during participating in pipe tobacco and burning and sucking due to complicated heat scission reaction so that original Flavoring Components
It can change, so as to influence its original Objective fragrance, it is therefore desirable to which adjustment formula can be with pipe tobacco phase repeatedly, in large quantities
Matching has the function that improve cigarette smoking quality.At present, the utilization of the technology is quite ripe, further improves cigarette suction
The space of food matter is little.
In addition, tobacco scientific research personnel is also attempted from natural perfume plant particle, the physics eluted using cigarette smoke
The fragrance matter introduced into cigarette smoke with cigarette flavor phase harmony is acted on, to achieve the purpose that improve smoking property of cigarette quality,
Some achievements are had been achieved at present.Such as：Patent CN103126072A《It is a kind of to increase cigarette sweet rhythm and the natural plant of infiltration sense
Composition granule and its application》The particle of announcement using rose and peppermint as raw material, by crush, pelletize and heated-air drying formed finished product
Grain plays an important role of to promote infiltration sense and comfort while sweet tea rhythm is increased.Patent CN105132167A《A kind of profit that increases carries perfume
Plant granule and its preparation method and application》Disclosed particle with Aplotaxis auriculata, Tibet inula root, fragrant purple perilla, rose, lavender, peppermint,
Radix Angelicae Sinensis and rice tea extraction are raw material, pass through extruding granulation, the fragrant formation finished particle of dry and load；Patent CN105124758A
《A kind of profit that increases carries fragrant plant granule and preparation method thereof and uses》The particle of announcement with rose, peppermint, Siraitia grosvenorii, rosemary,
Tribute chrysanthemum and rice tea extraction are raw material；Patent CN101912161B《A kind of cigarette peppermint filter stick and preparation method thereof》Disclosed filter
Peppermint, blackberry lily and tobacco leaf particle are with the addition of in stick fiber base material, have wet one's whistle, moisturizing, reduce the irritating effect of flue gas.
In terms of preparation method of granules, disclosed method mainly has fluidized bed granulation one-step method and wet granulation knot at present
Close dry two-step method.Although particle prepared by both approaches can improve or improve cigarette smoking quality to a certain extent,
But due to there is also some problems in preparation method and raw material selection and in terms of assembling so that existing plants particles material addition
Advantage function into cigarette filter rod also fails to give full play of.
For one-step preparation process, there are 2 points of deficiencies：1) particle surface made from covers macromolecule membrane layer, certain
Migration of the vegetable material aroma substance to cigarette smoke has been obstructed in degree；2) in granulation process, since air-flow is to plant material
The flushing repeatedly and elution of material have lost most of aroma substance of script in vegetable material.
For two-step method preparation process, there are 3 points of deficiencies：1) drying temperature is high, easily leads to the damage of vegetable material aroma substance
It becomes estranged destruction；2) if heated-air drying, hot wind can also take away part aroma substance in vegetable material；3) wet granulation is formed
Wet granular contains substantial amounts of moisture, and in the drying process, part aroma substance can be dissipated with the evaporation of moisture in vegetable material
It loses.
It selection as raw material and assembles, each plant material and the harmony of cigarette flavor that the prior art is announced are still
It needs to improve, this perfume of tobacco is abundant not enough, also to be improved.
For disadvantages mentioned above, appropriate material and technology how are selected, promoting granular materials is increasing cigarette smoke
Effect in terms of sweet sense and sense of promoting the production of body fluid, reducing, cigarette smoke is irritating simultaneously, assigns cigarette certain characteristic perfume, just
The technical issues of as needing further to solve.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide it is a kind of with American mint prepare cigarette filter rod add
The method of object, with reduce the fragrance loss in particulate production, promote cigarette burn and suck when particle in fragrance matter release, system
Standby obtained composite particles can be obviously improved cigarette smoking quality.
Unless otherwise indicated, percentage of the present invention is weight percent.
The purpose of the present invention is achieved by the following technical programs.
A kind of method that cigarette filter rod additive is prepared with American mint, it is characterised in that have following steps：
(1) vacuum freeze drying：When under the conditions of -20 DEG C to American mint leaf, fireworks petal and small red big tobacco leaf precooling 12,
Then it is 5%~8% by its vacuum freeze drying to moisture content under the conditions of -110 DEG C of condenser temperature；
(2) raw material crushes：Using the broken machine of low-temperature submicron powder respectively to after freeze-drying American mint leaf, fireworks petal and
Red big tobacco leaf crushes processing, its micro powder granule is enable to pass through 100 mesh screens；
(3) stock up：40~60 parts of American mint leaf powder, 5~10 parts of fireworks petal powder, red big tobacco leaf powder are weighed by mass parts
10~20 parts spare with 20~30 parts of tobacco jelly powder；
(4) raw material mixes：Each raw material of step (3) is mixed, then addition is equivalent to the water of mixture weight 2%~5%
It is uniformly mixed with high-speed mixer；
(5) squeeze：Extruding film-making is carried out to uniformly mixed raw material using water-cooled dry granulating machine, controls the thickness of tabletting
Degree is at 1.5~2.5 millimeters, and pressure roller cooling coolant-temperature gage is at 30~45 DEG C；
(6) tabletting crushes：Break process is carried out to raw material tabletting using hammer crusher；
(7) particle shaping：Shaping is carried out to broken granular materials using pelletizing machine, makes it completely by 30 mesh shapings
Net；
(8) particle screening：Coarse granule is removed using vibrating screen and fine powder, the bulk material of isolated 30~60 mesh obtain
To required cigarette filter rod additive.
Fireworks petal described in step (1), kind are K326 fireworks, the big gold dollar fireworks of safflower or two kinds of fireworks
Mixture.
The cigarette filter rod additive that the above method is prepared is added to cigarette by the dosage of every millimeter of 1~3mg of filter stick
In filter stick tow.
The American mint that the present invention selects is by spearmint (Mentha spicata) and fish mint (Mentha
Canadaensis) hybridize, the aroma substance contained is mainly menthol, menthones, cineole, methyl acetate, methyl
Ethyl alcohol furans, limonene, sobrerone or firpene, sabinene hydroxide and pulegone, have graceful fragrant and fragrant and sweet breath with
Typical cooling taste, fragrance is compared with horn of plenty, and cool taste is pure, lasting, intensity is high.The irritation of cigarette smoke can be reduced, is changed
The comfort of kind cigarette smoke and sweet sense；Fireworks petal, red big tobacco leaf and the equal source of tobacco jelly powder that the present invention selects
Tobacco plant has common ancestry homologous with cigarette shreds, has excellent hamony and matching.Fireworks petal sweetness note elegance,
Aroma substance is extremely abundant, such as damascenone, Megastigmatrienone, dihydroactinidiolide, benzaldehyde etc.；Red big tobacco leaf is made
For a kind of Yunnan sound tobacco, for fresh and sweet note than more typical, fragrance is also very abundant, and auxiliary fireworks petal, which has, promotes fragrance
Matter enriches the effect of cigarette flavor；Tobacco jelly powder is a kind of polysaccharide hydrocarbon, not only with excellent caking property,
And with cigarette flavor phase harmony, functions and effects are different from other caking property materials such as natural plant, starch.
Compared to the combination of other vegetable materials, the particle that thus Four Plants raw material is combined can not only be effectively
Abundant cigarette flavor, promotes comfort during cigarette smoking, and is better able to effectively be promoted the sweet tea sense of cigarette smoke, moisture feeling
And sense of promoting the production of body fluid, effectively alleviate the sense of discomfort of smoking cigarette, and assign a kind of pleasant cool sense of taste of cigarette and feel.
Compared with the prior art, the present invention has the following advantages and effect：
(1) fragrance harmony：American mint is aided in using fireworks petal powder, red big tobacco leaf powder and tobacco jelly powder, it can
The fragrance of American mint and the cigarette perfume of cigarette is made to combine together, generates harmonious, graceful, abundant and sweet cool taste cigarette perfume.This hair
Bright gained American mint particle is added to the sweet sense that can increase cigarette smoke in cigarette filter rod tow and sense of promoting the production of body fluid, and reduces cigarette
Flue gas irritation enriches cigarette flavor, the suction quality of cigarette is made to be promoted with obtaining conspicuousness；
(2) fragrance loss is low in preparation process：Raw material uses freeze-drying method, reduces aroma substance in drying process
Scatter and disappear.Material is pelletized using water-cooled dry granulating machine, and nip rolls cooling water temperature is controlled in pelletization.From
Granular material is to finished granule whole process without by drying, compared with other method of granulating, effectively reducing raw material
The loss of aroma substance；
(3) aroma substance release is easy：Due to American mint leaf, red big tobacco leaf and the fireworks Petal after freeze-drying
Short texture is porous, has larger specific surface area by the particle formed that crushes, pelletizes so that particle has with cigarette smoke
There is larger mass exchange area, enhance the eluting effect of cigarette smoke, promote particulate aroma substance moving to cigarette smoke
It moves.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, by the following examples to the present invention
It is described in further detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not to this
The restriction of inventive technique scheme.
Exemplified by preparing 100 kilograms of plant composite particles products, the present invention is specifically described.
Embodiment 1：Prepare American mint filter stick additive：
First when under the conditions of -20 DEG C to American mint leaf, K326 fireworks petal and small red big tobacco leaf precooling 12, then cold
Under the conditions of -110 DEG C of trap temperature by American mint leaf, fireworks petal and red big tobacco leaf vacuum freeze drying to moisture content be 5% shape
State；American mint leaf, fireworks petal and the red big tobacco leaf after freeze-drying are crushed respectively using the broken machine of low-temperature submicron powder
Processing, enables its micro powder granule to pass through 100 mesh screens；50 kilograms of American mint leaf powder, 7 kilograms of fireworks petals are weighed respectively
Powder, 18 kilograms of red big tobacco leaf powders, 25 kilograms of tobacco jelly powder input high-speed mixers, and 3 kilograms are additionally added into mixer
Water afterwards, is sufficiently stirred；Extruding film-making is carried out to uniformly mixed material using water-cooled dry granulating machine, and is controlled
The thickness of tabletting is in 1.5~2.0mm, and nip rolls cooling water temperature is at 30~40 DEG C.Using hammer crusher to materials result
Carry out break process.Shaping is carried out to broken granular materials using pelletizing machine, makes it completely by 30 mesh shaping nets.It uses
Vibrating screen removes coarse granule and fine powder, the bulk material of isolated 30~60 mesh.
By the dosage of 1.5mg/mm, prepared bulk material is added in filter stick tow, formed charge bar, then with white stick
It is compound, binary compound filter candle is prepared into, and rolls into cigarette.It is control sample to set the cigarette without particle addition, and sensory evaluating smoking ties
Fruit is shown in Table 1.
Embodiment 2：
Embodiment 1 is repeated, there is following difference：The big gold dollar fireworks petal of American mint leaf, safflower and red big tobacco leaf vacuum
Freeze-drying to moisture content is 5% state.Weigh 60 kilograms of American mint leaf powder, 5 kilograms of fireworks petal powder, 12 kilograms of red opium
Ye Fen, 23 kilograms of tobacco jelly powders, and add 2 kg of water.The thickness of tabletting is controlled in 1.8~2.5mm, nip rolls coolant water temperature
Degree is at 35~45 DEG C.By the dosage of 1.0mg/mm, the American mint composite particles of 2 gained of embodiment are added to filter stick tow
In.
Embodiment 3：
Embodiment 1 is repeated, there is following difference：American mint leaf, K326 fireworks petal and red big tobacco leaf vacuum refrigeration are done
It is dry to moisture content be 6% state.Weigh 40 kilograms of American mint leaf powder, 10 kilograms of fireworks petal powder, 20 kilograms of red big tobacco leaf powders,
30 kilograms of tobacco jelly powders, and 2.5 kg of water are added, the thickness of tabletting is controlled in 1.5~2.0mm, nip rolls cooling water temperature
At 30~40 DEG C.By the dosage of 2.0mg/mm, the American mint composite particles of 3 gained of embodiment are added in filter stick tow.
Embodiment 4：
Embodiment 1 is repeated, there is following difference：The big gold dollar fireworks petal of American mint leaf, safflower and red big tobacco leaf vacuum
Freeze-drying to moisture content is 7% state.Weigh 52 kilograms of American mint leaf powder, 8 kilograms of fireworks petal powder, 20 kilograms of red opium
Ye Fen, 20 kilograms of tobacco jelly powders, and add 4 kg of water.The thickness of tabletting is controlled in 1.5~2.0mm, nip rolls coolant water temperature
Degree is at 30~45 DEG C.By the dosage of 2.5mg/mm, the American mint composite particles of 4 gained of embodiment are added to filter stick tow
In.
Embodiment 5：
Embodiment 1 is repeated, there is following difference：American mint leaf, K326 fireworks petal and red big tobacco leaf vacuum refrigeration are done
It is dry to moisture be 8% state.Weigh 60 kilograms of American mint leaf powder, 10 kilograms of fireworks petal powder, 10 kilograms of red big tobacco leaves
Powder, 20 kilograms of tobacco jelly powders, and add 5 kg of water.The thickness of tabletting is controlled in 1.5~2.0mm, nip rolls cooling water temperature
At 30~40 DEG C.By the dosage of 3.0mg/mm, the American mint composite particles of 5 gained of embodiment are added in filter stick tow.
1 cigarette sensory evaluating smoking's result of table
As seen from the above table, present invention gained American mint filter stick additive, which is added in cigarette filter rod tow, can increase cigarette
The sweet sense of flue gas and sense of promoting the production of body fluid reduce cigarette smoke irritation, enrich cigarette flavor, the suction quality of cigarette is made to obtain significantly
Promoted to property.It is mainly shown as in terms of flavouring and promotes flue gas elegance and sophistication, it is cool savory to assign cigarette for this perfume of increase tobacco
Gas；The sweet sense of supplement and sense of promoting the production of body fluid are mainly shown as in terms of pleasant impression improvement；Work(is covered to wooden, raw blue foreign smell in terms of miscellaneous gas cover
Effect is apparent, there is certain cover effect to dried-up miscellaneous gas；Stining for throat and lingual surface can be substantially reduced by being mainly shown as in terms of drop thorn
Thorn sense.
Claims (2)
- A kind of 1. method that cigarette filter rod additive is prepared with American mint, it is characterised in that have following steps：(1) vacuum freeze drying：When under the conditions of -20 DEG C to American mint leaf, fireworks petal and small red big tobacco leaf precooling 12, then By its vacuum freeze drying to moisture content it is 5%~8% under the conditions of -110 DEG C of condenser temperature；(2) raw material crushes：Using the broken machine of low-temperature submicron powder respectively to American mint leaf, the fireworks petal and red big after freeze-drying Tobacco leaf crushes processing, its micro powder granule is enable to pass through 100 mesh screens；(3) stock up：By mass parts weigh 40~60 parts of American mint leaf powder, 5~10 parts of fireworks petal powder, red big tobacco leaf powder 10~ 20 parts spare with 20~30 parts of tobacco jelly powder；(4) raw material mixes：Each raw material of step (3) is mixed, then addition is equivalent to the water height of mixture weight 2%~5% Fast mixer is uniformly mixed；(5) squeeze：Extruding film-making is carried out to uniformly mixed raw material using water-cooled dry granulating machine, the thickness of tabletting is controlled to exist 1.5~2.5 millimeters, pressure roller cooling coolant-temperature gage is at 30~45 DEG C；(6) tabletting crushes：Break process is carried out to raw material tabletting using hammer crusher；(7) particle shaping：Shaping is carried out to broken granular materials using pelletizing machine, makes it completely by 30 mesh shaping nets；(8) particle screening：Coarse granule is removed using vibrating screen and fine powder, the bulk material of isolated 30~60 mesh obtain institute The cigarette filter rod additive needed.
- 2. the method for cigarette filter rod additive is prepared with American mint according to claim 1, it is characterised in that：Step (1) Described in fireworks petal, kind is K326 fireworks, the mixture of the big gold dollar fireworks of safflower or two kinds of fireworks.
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Families Citing this family (4)
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| CN107746748A (en) * | 2017-11-08 | 2018-03-02 | 湖北中烟工业有限责任公司 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
| CN108143005A (en) * | 2017-12-22 | 2018-06-12 | 安徽中烟工业有限责任公司 | A kind of peripheral electrical heating aerosol generation system for including tobacco particle |
| CN113576020A (en) * | 2021-08-02 | 2021-11-02 | 云南中烟工业有限责任公司 | Preparation method of smoke generating material for smoking product |
| KR20240027484A (en) * | 2022-08-23 | 2024-03-04 | 주식회사 케이티앤지 | Method for manufacturing tobacco granules, and aerosol generating article comprising the tobacco granules manufactured thereby |
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