CN104705783A - Filter tip additive material capable of improving sensory characteristics of smoke and application thereof - Google Patents
Filter tip additive material capable of improving sensory characteristics of smoke and application thereof Download PDFInfo
- Publication number
- CN104705783A CN104705783A CN201510029425.XA CN201510029425A CN104705783A CN 104705783 A CN104705783 A CN 104705783A CN 201510029425 A CN201510029425 A CN 201510029425A CN 104705783 A CN104705783 A CN 104705783A
- Authority
- CN
- China
- Prior art keywords
- filter tip
- cigarette
- flue gas
- adding material
- filter
- Prior art date
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
Abstract
The invention discloses a filter tip additive material capable of improving the sensory characteristics of smoke and the application thereof. The filter tip additive material is characterized by being prepared by carrying a mixed solution of propylene glycol and sorbitol on a carrier which is a mixture of porous SiO2 and Al2O3 particles. A two-element or multi-element combined filter tip can be manufactured by adding the prepared filter tip additive material into a cigarette filter stick. The filter tip additive material prepared through the method contains a low-molecular hydrophilic moisture-retaining agent, moisture can be effectively retained for a long time and can be rapidly released when a cigarette is smoked, the moisture content in the smoke of the cigarette is increased, and the sensory quality of the cigarette is improved. Meanwhile, by means of the method, the content of harmful ingredients such as tar and total particulate matter in the smoke can be effectively reduced. In addition, the filter tip additive material is nontoxic, harmless and low in cost and has broad industrial prospects, and the preparation process is simple and easy to implement.
Description
Technical field
The present invention relates to cigarette filter adding material, specifically a kind of additives of filter tip improving cigarette smoke organoleptic feature.This additive can improve the moisture in cigarette smoke, improves the organoleptic quality of cigarette.Effectively can reduce the content of the harmful components such as tar in flue gas and TPM, and material easily obtains, preparation process is simple simultaneously.
Background technology
In cigarette smoke, moisture is the very important factor affecting Sensory Quality of Cigarette.Flue gas moisture content is lower, and flue gas can be caused dry, stimulates and increases, and comfortableness reduces, the significant organoleptic quality reducing cigarette.And current increasing low-coke tar cigarette, and increasing harm reduction technology, be mostly to adopt a large amount of aeration technologies or adsorption technology, so just cause moisture in main flume to reduce, thus affect aesthetic quality.
Traditional cigarette humectation technology, mainly for adding a certain amount of flavouring humectant in cigarette leaves and tobacco, while lifting flue gas fragrance, keeps the moisture content of pipe tobacco.Along with the development of low tar height ventilation cigarette technology, increasing people improve cigarette quality to have focused on filter tip technical, the adding material of the improvement cigarette smoke quality of research and development mainly contains following two kinds:
The first directly some essence and flavoring agents and humectant is sprayed directly on filter tip.As the condensation product of organic acid, ethylene glycol, pyrrolidones, essence and flavoring agent etc. mix as additive by patent CN200610048649, be sprayed onto in pipe tobacco or filter tip, improve cigarette smoke moisture; Patent CN200710036161, by mixing such as jasmine tea, Radix Glycyrrhizae, polyethylene glycol, honey and triacetyl glycerines, is sprayed on cigarette third fibre or the fine mouth rod of vinegar.From effect, above method and traditional pipe tobacco humectant method close, effect is not remarkable.
The second utilizes certain specific material as carrier, then some fragrance matter of load and humectant promote flue gas fragrance.If patent CN201210344409 is using porous cellulose as carrier, load tobacco essence is in fiber tow filter rods.Patent CN201310354368 with Chinese herbal medicine as Radix Isatidis, the Radix Astragali, glossy ganoderma, rhizoma alismatis or Poria cocos for carrier material prepared by raw material, the agent of load Harm reduction techniques, flavouring agent or after chemical modification, add in cigarette filter rod.Patent CN201310354373, adds in cigarette filter rod after the agent of load Harm reduction techniques, flavouring agent as agricultural crop straw, corncob prepare carrier material for raw material with agricultural waste material.Hyaluronic acid and glycerine are fully mixed obtained resin as filter tip adding material with ion exchange resin by patent CN201310035857, are prepared into binary combined filter tip.Pipe tobacco or expanded cut tobacco, tobacco stem shred or expanding tobacco stem, reconstituted tobacoo are pulverized and mixed by patent CN200710169786, with its load flavouring agent or (with) lowering harm and decreasing coking agent is applied in cigarette composite filter tip.More than invent mainly through filter tip or carrier adsorption essence and flavoring agent or humectant, increase smoke perfume and humectation, though these humectants play certain effect.But used carrier material often obtains with vegetable material modification, the organoleptic quality of product can be affected with peculiar smell, adopt the material costs such as ion exchange resin then higher in addition.
Summary of the invention
Object of the present invention provides a kind of adding material of novel improvement flue gas organoleptic feature just for above-mentioned prior art situation, and provides the application of material processing method in tobacco filler.Use this material, the moisture in main flume can be significantly improved, obviously promote the organoleptic quality of cigarette, and the tar that can reduce in flue gas and TPM content.
The object of the invention is to be achieved by following technical proposals:
Can improve a filter tip adding material for flue gas organoleptic feature, be with the mixture of porous sio2, Al2O3 particle for carrier, and obtained after the mixed solution of load propane diols and sorbierite, concrete grammar step is as follows:
(1) choosing particle diameter is 0.5 ~ 3mm, and specific area is 100-600m
2the SiO of/g
2and Al
2o
3, mix, as humectant carrier by the ratio uniform of 3:1 ~ 1:3;
(2) propane diols and sorbierite are mixed in the ratio of 1:9 ~ 9:1, be configured to the aqueous solution that concentration is 0.1 ~ 5%, stir;
(3) by solution obtained in step (2) by 0.5% ~ 2% percentage by weight evenly send forth on the humectant carrier that obtains in step (1), in temperature lower than 30 DEG C, humidity is balance 24 hours under the environment of 40% ~ 80%, is the filter tip adding material that can improve flue gas organoleptic feature of the present invention.
In the present invention, SiO
2and Al
2o
3the preferred 1:2 of mixed proportion, particle diameter preferred 1mm, SiO
2the preferred 500m of specific area
2/ g, Al
2o
3the preferred 100m of specific area
2/ g.The preferred 1:1 of mixed proportion of propane diols and sorbierite.
Temperature in step (3) is preferably 10-25 DEG C
.
Put in cigarette filter rod by filter tip adding material and make binary or multiple elements design filter tip, this adding material can be installed in the middle of two-section fiber tow filter rods, also can be loose being sprinkling upon in tow.The moisture of flue gas when filter tip after interpolation can improve cigarette smoking, improves the organoleptic quality of cigarette.
Feature of the present invention adopts porous sio2 and Al2O3 particle as absorption carrier, adopts special pre-treating method, be prepared into binary combined filter tip, can obviously improve pipe tobacco moist feeling during suction, effectively can reduce tarry matters in smoke, CO content and granule phase substance simultaneously.And material therefor is harmless to human non-toxic, with low cost, preparation technology is simply easy to realize.
Principle of the present invention: the porous sio2 adopted in the present invention and Al2O3 belong to porous adsorption carrier, has good absorption property to moisture, has good water tariff collection function at normal temperatures; The propane diols simultaneously added and sorbierite are humectant, and the water tariff collection time in filter tip can be made to extend further; When cigarette is aspirated, in the temperature of filter tip front end cigarette mainstream flue gas more than 70 DEG C, by desorption can be carried out to the moisture on material during filter tip, discharge the moisture that sufficient moisture comes in supplementary main flume, improve the aesthetic quality of cigarette.Simultaneously moistening porous material effectively can adsorb tar in flue gas and TPM, reduces harmful ingredients in flue gas.Adopt the method load water and humectant that spray, and balance under constant-temperature constant-humidity environment, keep its uniformity, the moisture quantitatively supplementing flue gas can be stablized.
Porous material in the present invention, to the moistening, moisturizing successful of flue gas, can significantly improve cigarette aesthetic quality, reduces harmful ingredients in flue gas, and adding material free from extraneous odour.Material is harmless to human non-toxic, with low cost, preparation technology is simply easy to realize, and has good industrial prospect.
Accompanying drawing explanation
Fig. 1 is that adding material of the present invention puts in filter stick the cigarette schematic diagram making binary combined filter tip.
In figure: 1 is cigarette, 2 is filter tip, and 3 is adding material.
Detailed description of the invention
The present invention is described further below with reference to example, but does not limit the present invention.
Improve a filter tip adding material for flue gas organoleptic feature, its preparation process is as follows:
1. choosing particle diameter is 1mm, and specific area is 500m
2the porous SiO of/g
2with 100m2/g Al
2o
3, mix, as humectant carrier in the ratio of 1:2; 2. propane diols and sorbierite are mixed in the ratio of 1:1, be configured to the aqueous solution that concentration is 0.5 %, stir; 3. by obtained solution by 1% percentage by weight evenly send forth on humectant carrier, temperature 22 DEG C, humidity be under the environment of 60% balance 24 hours; 4. using step 3 kind of obtained adding material as filter tip adding material.5. added in cigarette filter by this material and make binary combined filter tip, addition is that 500mg/ props up.
Rolling cigarette under condition is rolled same respectively with common filter tip and above-mentioned binary combined filter tip.According to YC/T 138 method, cigarette is smoked panel test; Measure TPM and tar content according to GB/T 19609, adopt YC/T30 to measure CO content in main flume, adopt gas chromatography to measure moisture in main flume.The results are shown in Table one and table two.
Table one composite filter tip cigarette compares with common filter tip cigarette organoleptic attribute
| Sample | Aesthetic quality marks | Remarks |
| Regular-size cigarette | 8.5 | |
| Composite filter tip cigarette | 9.0 | Style and features does not change, and moist feeling strengthens, and stimulation alleviates |
Table two composite filter tip cigarette compares with common filter tip cigarette smoke components
| Project | TPM (mg/cig) | Nicotine (mg/cig) | Moisture (mg/cig) | Tar (mg/cig) | Carbon monoxide (mg/cig) |
| Regular-size cigarette | 7.05 | 0.57 | 0.44 | 6.04 | 6.55 |
| Composite filter tip cigarette | 6.74 | 0.58 | 0.74 | 5.51 | 6.30 |
The above results shows, filter tip adding material of the present invention can be used for production of cigarettes, can significantly improve cigarette aesthetic quality, improves the moisture of flue gas, and reduces granule phase substance in flue gas, tar and carbon monoxide content, and do not have peculiar smell.Adopt the cigarette sample of the present invention's making as shown in Figure 1, in figure, 1 place's filter tip mid portion interstitial site is granular materials of the present invention.
Claims (5)
1. can improve a filter tip adding material for flue gas organoleptic feature, it is characterized in that: be with the mixture of porous sio2, Al2O3 particle for carrier, obtained after the mixed solution of load propane diols and sorbierite, concrete grammar step is as follows:
(1) choosing particle diameter is 0.5-3mm, and specific area is 100-600m
2the SiO of/g
2and Al
2o
3, mix, as humectant carrier by the ratio uniform of 3:1-1:3;
(2) propane diols and sorbierite are mixed in the ratio of 1:9-9:1, be configured to the aqueous solution that concentration is 0.1%-5%, stir;
(3) solution obtained in step (2) is evenly sent forth on humectant carrier obtained in step (1) by the percentage by weight of 0.5%-2%, in temperature lower than 30 DEG C, humidity is balance 24 hours under the environment of 40%-80%, is the filter tip adding material that can improve flue gas organoleptic feature of the present invention.
2. the filter tip adding material that can improve flue gas organoleptic feature according to claim 1, is characterized in that: SiO
2and Al
2o
3the preferred 1:2 of mixed proportion, particle diameter preferred 1mm, SiO
2the preferred 500m of specific area
2/ g, Al
2o
3the preferred 100m of specific area
2/ g.
3. the filter tip adding material that can improve flue gas organoleptic feature according to claim 1, is characterized in that: the preferred 1:1 of mixed proportion of propane diols and sorbierite.
4. the filter tip adding material that can improve flue gas organoleptic feature according to claim 1, is characterized in that: the temperature in step (3) is preferably 10-25 DEG C.
5. the application of a filter tip adding material according to claim 1 in cigarette filter, it is characterized in that: filter tip adding material is put in cigarette filter rod and makes binary or multiple elements design filter tip, this adding material can be installed in the middle of two-section fiber tow filter rods, also can be to fall apart to be sprinkling upon in tow; The moisture of flue gas when filter tip after interpolation can improve cigarette smoking, improves the organoleptic quality of cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510029425.XA CN104705783A (en) | 2015-01-21 | 2015-01-21 | Filter tip additive material capable of improving sensory characteristics of smoke and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510029425.XA CN104705783A (en) | 2015-01-21 | 2015-01-21 | Filter tip additive material capable of improving sensory characteristics of smoke and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104705783A true CN104705783A (en) | 2015-06-17 |
Family
ID=53405880
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510029425.XA Pending CN104705783A (en) | 2015-01-21 | 2015-01-21 | Filter tip additive material capable of improving sensory characteristics of smoke and application thereof |
Country Status (1)
| Country | Link |
|---|---|
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107183787A (en) * | 2017-06-30 | 2017-09-22 | 云南中烟工业有限责任公司 | A kind of sense organ material aspirator with atomizing functions |
| CN113287784A (en) * | 2021-06-25 | 2021-08-24 | 云南中烟工业有限责任公司 | Cigarette filter particles capable of reducing release amount of hydrogen sulfide in smoke, preparation method and filter |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1043412A (en) * | 1962-04-09 | 1966-09-21 | Eastman Kodak Co | Tobacco smoke filter |
| US3285255A (en) * | 1965-06-07 | 1966-11-15 | Eastman Kodak Co | Polyolefin filter |
| JP2001095552A (en) * | 1999-09-28 | 2001-04-10 | Daicel Chem Ind Ltd | Filter for cigarette smoke |
| CN1538815A (en) * | 2001-08-02 | 2004-10-20 | �ձ��̲ݲ�ҵ��ʽ���� | Filter for cigarette |
| CN102240071A (en) * | 2011-07-02 | 2011-11-16 | 云南瑞升烟草技术（集团）有限公司 | Filter tip stick for low-tar cigarette |
| CN102885401A (en) * | 2011-07-19 | 2013-01-23 | 夏涛 | Efficient cigarette filter containing nano bamboo charcoal material |
| CN104116133A (en) * | 2014-07-31 | 2014-10-29 | 云南中烟工业有限责任公司 | Application of polymers rich in amino groups in paper filter stick |
-
2015
- 2015-01-21 CN CN201510029425.XA patent/CN104705783A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1043412A (en) * | 1962-04-09 | 1966-09-21 | Eastman Kodak Co | Tobacco smoke filter |
| US3285255A (en) * | 1965-06-07 | 1966-11-15 | Eastman Kodak Co | Polyolefin filter |
| JP2001095552A (en) * | 1999-09-28 | 2001-04-10 | Daicel Chem Ind Ltd | Filter for cigarette smoke |
| CN1538815A (en) * | 2001-08-02 | 2004-10-20 | �ձ��̲ݲ�ҵ��ʽ���� | Filter for cigarette |
| CN102240071A (en) * | 2011-07-02 | 2011-11-16 | 云南瑞升烟草技术（集团）有限公司 | Filter tip stick for low-tar cigarette |
| CN102885401A (en) * | 2011-07-19 | 2013-01-23 | 夏涛 | Efficient cigarette filter containing nano bamboo charcoal material |
| CN104116133A (en) * | 2014-07-31 | 2014-10-29 | 云南中烟工业有限责任公司 | Application of polymers rich in amino groups in paper filter stick |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107183787A (en) * | 2017-06-30 | 2017-09-22 | 云南中烟工业有限责任公司 | A kind of sense organ material aspirator with atomizing functions |
| CN113287784A (en) * | 2021-06-25 | 2021-08-24 | 云南中烟工业有限责任公司 | Cigarette filter particles capable of reducing release amount of hydrogen sulfide in smoke, preparation method and filter |
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Application publication date: 20150617 |