CN101897478A - Filter stick for cigarettes and preparation method thereof - Google Patents
Filter stick for cigarettes and preparation method thereof Download PDFInfo
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- CN101897478A CN101897478A CN 201010250486 CN201010250486A CN101897478A CN 101897478 A CN101897478 A CN 101897478A CN 201010250486 CN201010250486 CN 201010250486 CN 201010250486 A CN201010250486 A CN 201010250486A CN 101897478 A CN101897478 A CN 101897478A
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Abstract
The invention discloses a filter material of a filter stick for cigarettes and a composite filter stick prepared from the material. The filter material comprises a fiber substrate and a plasticizer, wherein blackberry lily particles and tobacco powder particles are added into the fiber substrate; the ratio (parts by weight) of the blackberry lily to the tobacco powder is 3-4:6-7; the fraction of the mixed particles is 40-80 meshes; and 1.0-1.5mg of Chinese herbal medicine mixed particles are added into each millimeter of filter stick in length. In the invention, the blackberry lily particles and the tobacco powder particles are taken as the adsorbing materials of a functional composite filter stick, and the adding proportion, the adding amount and the particle fraction of the blackberry lily particles and the tobacco powder particles, the adding proportion of the plasticizer and other factors are determined. After the composite filter stick, tobacco shreds and cigarette paper are coiled into finished products of cigarettes, harmful substances in the smoke can be effectively reduced; and meanwhile, the composite filter stick can not influence the suction taste of the cigarettes and has the functions of moistening the throat, preserving the moisture, relieving the stimulation of the smoke to the throat, and the like.
Description
Technical field
The invention belongs to the production of cigarettes field, be specifically related to a kind of filter bar for cigarette and preparation method thereof.
Background technology
Cigarette produces harmful substances such as CO, tar in aspiration procedure, the smoking time one is long, and that smoker throat just has is dry, itch, cough even sore symptom.Along with the raising of health of people consciousness, the security of cigarette is had higher requirement.Cigarette filter rod to promoting the cigarette smoking quality, filters the harmful substance in the flue gas as the filtering material of cigarette smoke, improves cigarette security aspect and all has important function.In recent years, countries in the world were also increasing to the research of new type functional filter stick.
Domestic applications patent " a kind of new cigarette filter stick with filtering material and preparation method ", application number: 200710066121.6, a kind of expanded cabo particle that adopts is disclosed as filter stick for cigarettes of filtering material and preparation method thereof.Number of patent application 200910172250.2 discloses a kind of new material that can effectively adsorb sour gas, and this material is introduced different basic groups by porous material is carried out chemical modification.This material is made an addition to cigarette filter rod, can reduce hydrogen cyanide burst size in the cigarette mainstream flue gas.Number of patent application 200720155556.3 discloses the filter stick that has Pu'er tea, adopts harmful substance that the cigarette of this filter stick can reduce volatility and half volatile in the main flume most effectively as nitrite, BaP, tar etc.Number of patent application: 03260500.5 discloses a kind of vinegar fibre adds nanometer noble metal catalyst binary compound filter candle, and this filter stick can effectively reduce the content of carbon monoxide in the cigarette smoke.
At present, most of both at home and abroad research all is that porous prilled material is added in the filter stick, when cigarette smoking, the main flume filter stick of flowing through, porous material in the filter stick produces suction-operated to flue gas, harmful substance is adsorbed on the porous particle, thereby has reduced the content of harmful substance in main flume.But in the harmful substance of porous material in the absorption flue gas, also the fragrance component in the flue gas has been adsorbed, thereby the suction quality of reduction cigarette.In addition, the particle majority that adds in the filter stick is to adopt chemical method to handle to obtain, and the security of himself remains further research, and material price cost such as noble metal is higher.Therefore, when because of the harmful components in the requirement reduction flue gas of reducing tar and reducing harm, how to keep the perfume quantity of cigarette, improve the suction quality of cigarette, become the difficult problem that scientific and technical personnel are badly in need of solving.
Summary of the invention
The purpose of this invention is to provide a kind of cigarette composite filter that contains Chinese herbal medicine and tobacco powder particle, the perfume quantity when aspirating to increase promotes the suction dry, alleviates the excitant of flue gas to smoker throat.
Another object of the present invention provides the preparation method of above-mentioned composite filter.
The present invention realizes above-mentioned purpose by following scheme.
A kind of filter stick for cigarettes contains the hybrid particles of blackberry lily particle and tobacco powder particle, as filtering material in the filter stick.The mass ratio of blackberry lily and tobacco powder particle is in the hybrid particles: 3～4 parts of blackberry lilys, 6～7 parts of tobacco powders.Hybrid particles is after blackberry lily and pipe tobacco are carried out preliminarily dried respectively and pulverizing, to cross 40～80 mesh sieves, further under 40～60 ℃, dry by the fire again after the mixing to moisture be 6～10%.
Can adopt following step to prepare the hybrid particles of this filter stick for cigarettes:
(1) get the blackberry lily rhizome 40～60 ℃ of down oven dry, dry to moisture be 8%～12%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 40～80 mesh sieves, get the blackberry lily particle.
(2) get the cigarette pipe tobacco of certain trade mark, under 40～60 ℃, dry by the fire to moisture be 8%～10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 40～80 mesh sieves, get the tobacco powder particle.
(3) above-mentioned two kinds of powder particles are mixed, the quality of various particles is: 3～4 parts of blackberry lily particles, and 6～7 parts of tobacco powder particles, then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.
(4) processed is carried out to compound particles in moisture regain back, at low temperatures (40～60 ℃) dry to moisture be 6%～10%.Promptly get the cigarette hybrid particles.
In this filter stick for cigarettes, the content of hybrid particles is to contain in the filter stick of every mm length to mix particle 1～1.5mg.The blackberry lily hybrid particles is dispersed in the tow of filter stick.Its manufacturing process comprises the steps:
(1) compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.
(2) adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up, then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm, 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.0～1.5mg/mm.
Test is found, blackberry lily that the present invention is used and tobacco powder particle, and its particle size just is applicable to and is added in the filter stick, and it comparatively stably is dispersed in the filter stick tow, is difficult for being scattered; The filter stick compound particles has the cigarette flavor of increasing amount simultaneously, reduces the flue gas excitant, promotes the effect of cigarette smoking quality, can reduce the harmful substance contents in the flue gas simultaneously effectively.The more important thing is, different with most of harm reduction filter sticks, the blackberry lily particle makes an addition in the filter stick, reduce the harmful substance contents in the main flume, the fragrance component in the time of still can't adsorbing the cigarette suction, the active ingredient that blackberry lily evaporated can be alleviated the stimulation of flue gas, but can not produce the assorted flavor of peculiar smell, even promoted the perfume quantity of cigarette, infer that this may be that the cooperative effect that produces behind blackberry lily and the tobacco particle compatibility helps promoting the fragrance of cigarette, and then promote the suction quality of cigarette.These characteristics are fit to it very much should be in cigarette filter rod.
Under the situation of the applied amount of 1～1.5mg, compound particles is present in the filter stick, can not cause the cigarette odor-absorbing obvious variation.
Compared with prior art, the present invention has following beneficial effect:
1. the present invention creatively adds blackberry lily and tobacco particle in the filter stick, is applied on the cigarette, when not changing the cigarette smoking style, can increase the perfume quantity of cigarette, thereby effectively improve the cigarette smoking quality.
2. though composite filter provided by the present invention has added the blackberry lily particle, but can't cause negative effect to the suction style of cigarette product, simultaneously during cigarette smoking, the volatilization of being heated of active ingredient in the blackberry lily, suck together in smoker's mouth in company with main flume, can alleviate the excitant of flue gas to a certain extent, have and wet one's whistle, preserve moisture, alleviate the effects such as excitant of flue gas throat to smoker throat.
3. composite filter provided by the present invention cigarette mainstream flue gas is had certain dam, filtering function, can reduce the harmful substance contents in the main flume to a certain extent.
4. blackberry lily that composite filter provided by the present invention added and tobacco composition particle can firmly be scattered in the filter stick, are difficult for being scattered, and filter stick is made moulding and the equal easy operating of cigarette finished product preparation process.
5. the material that adds on filter stick of the present invention is a natural plants, without chemical treatment, and safety and sanitation, and cheap, obtain easily.
The specific embodiment
Below further specify technical scheme of the present invention by specific embodiment.In order to verify that further beneficial effect of the present invention, the present invention also will adopt this filter stick cigarette that makes and the contrast cigarette contrast of not using this filter stick, carry out sensory evaluating smoking and flue gas analysis test.
Embodiment 1
The blackberry lily rhizome 5kg that takes from right drying is 60 ℃ of oven dry down, dry to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the Blackberrylily Rhizome particle.Get cigarette A trade mark cigarette pipe tobacco in the Guangdong, under 60 ℃, dry by the fire to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the tobacco powder particle.The ratio of above-mentioned two kinds of powder particles with 4: 6 mixed, and then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.Processed is carried out to compound particles in moisture regain back, at low temperatures (60 ℃) to dry to moisture be 6% promptly to get cigarette composite filter compound particles.
Compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.Adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up, then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm, 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.5mg/mm.
Adopt A trade mark pipe tobacco, cigarette paper, the tipping paper of Guangdong China Tobacco Industry Co.,Ltd and the composite filter that makes as stated above to roll into cigarette finished product together.
To contain the following experiment of cigarette process of above-mentioned composite filter:
Experimental group: cigarette is 400 as mentioned above; Control group: do not adopt above-mentioned filter stick, but 400 of all identical regular-size cigarettes of pipe tobacco and cigarette paper, tipping paper.
Embodiment 2
The blackberry lily rhizome 5kg that takes from right drying is 60 ℃ of oven dry down, dry to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the Blackberrylily Rhizome particle.Get cigarette A trade mark cigarette pipe tobacco in the Guangdong, under 60 ℃, dry by the fire to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the tobacco powder particle.The ratio of above-mentioned two kinds of powder particles with 3: 7 mixed, and then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.Processed is carried out to compound particles in moisture regain back, at low temperatures (60 ℃) to dry to moisture be 8% promptly to get cigarette composite filter compound particles.
Compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.Adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up, then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm, 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.5mg/mm.
Adopt A trade mark pipe tobacco, cigarette paper, the tipping paper of Guangdong China Tobacco Industry Co.,Ltd and the composite filter that makes as stated above to roll into cigarette finished product together.
To contain the following experiment of cigarette process of above-mentioned composite filter:
Experimental group: cigarette is 400 as mentioned above; Control group: do not adopt above-mentioned filter stick, but 400 of all identical regular-size cigarettes of pipe tobacco and cigarette paper, tipping paper.
Embodiment 3
The blackberry lily rhizome 5kg that takes from right drying is 60 ℃ of oven dry down, dry to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the Blackberrylily Rhizome particle.Get cigarette A trade mark cigarette pipe tobacco in the Guangdong, under 60 ℃, dry by the fire to moisture be 10%.Adopt pulverizer to pulverize respectively, pulverize the back and cross 60 mesh sieves, get the tobacco powder particle.The ratio of above-mentioned two kinds of powder particles with 3: 7 mixed, and then with the processing that gets damp again, the moisture that makes compound particles is 30%, stores 12h.Processed is carried out to compound particles in moisture regain back, at low temperatures (60 ℃) to dry to moisture be 8% promptly to get cigarette composite filter compound particles.
Compound particles is evenly added in the diacetate fiber tow, alternately arrange with the tow that does not add particle.Adopt filter rod forming paper that tow is rolled into continuous filter stick, the filter stick length of adding particle in the filter stick is 1: 1 with the filter stick length ratio that does not add particle.Filter stick is cut into 120mm/ to be propped up, then to contain particle length be 60mm to filter stick, and not containing particle length is 60mm, and concrete particle distribution range is for to contain the particle filter stick at filter stick 15mm～45mm place for 30mm, 75mm～105mm place contains the particle filter stick for 30mm, and the particle addition is 1.2mg/mm.
Adopt A trade mark pipe tobacco, cigarette paper, the tipping paper of Guangdong China Tobacco Industry Co.,Ltd and the composite filter that makes as stated above to roll into cigarette finished product together.
To contain the following experiment of cigarette process of above-mentioned composite filter:
Experimental group: cigarette is 400 as mentioned above; Control group: do not adopt above-mentioned filter stick, but 400 of all identical regular-size cigarettes of pipe tobacco and cigarette paper, tipping paper.
Cigarette smoke analytical test: press GB/T 19609-2004 " cigarette is measured TPM and tar with conventional analysis with smoking machine " and GB/T 23356-2009 " the non-scattering infrared method of the mensuration of carbon monoxide in the cigarette smoke gas phase " and measure flue gas TPM (TPM), tar and carbon monoxide (CO) content, press GB/T 21130-2007 " benzo in the cigarette smoke TPM
The mensuration of pyrene " measure the benzo in the main flume
Pyrene, press YC/T 255-2008 " the mensuration high performance liquid chromatography of main phenolic compound in the cigarette mainstream flue gas " and measure phenol, press YC/T 254-2008 " the mensuration high performance liquid chromatography of main carbonyls in the cigarette mainstream flue gas " and measure the crotonaldehyde in the main flume, press the hydrogen cyanide in YC/T253-2008 " the mensuration continuous flow method of hydrogen cyanide in the cigarette mainstream flue gas " the mensuration main flume.The measuring result is as shown in table 1.
Table 1 flue gas analysis result
As known from Table 1, under the approaching situation of both puff numbers, embodiment 1, embodiment 2, and embodiment 3 cigarette samples with to comparing in the same old way, in the main flume except that the CO content not quite, all the other smoke components such as phenol, crotonaldehyde, hydrogen cyanide and benzo
The content of pyrene all has reduction in various degree, and this shows that the particle in the filter stick all has certain adsorption filtration effect to the harmful substance in the main flume, can effectively reduce harmful substance contents in the flue gas.
Sensory evaluating smoking test: according to GB GB 5606.5-2005 " cigarette the 4th part: sense organ specification requirement " to embodiment 1, embodiment 2, and embodiment 3 cigarette samples with to carry out the sensory evaluating smoking in the same old way, smoking result is as shown in table 2.
Table 2 cigarette sample sensory evaluating smoking gets submeter
Sensory evaluating smoking result shows, with to compare in the same old way, aesthetic quality's integrate score of embodiment sample improves 2.36～2.92, be mainly reflected in three aspect scores such as fragrance, excitant and pleasant impression and be improved, especially the score aspect fragrance is more remarkable, and the lifting amplitude reaches 1.10～1.29, and aspect assorted gas, the embodiment sample is approaching with the contrast sample, and the score of assorted gas aspect does not obviously reduce, and this shows that this filter stick can't bring unnecessary assorted gas.According to judging panel's conclusion, the embodiment sample can effectively alleviate the stimulation of flue gas to throat, has certain effect that wets one's whistle, promotes the production of body fluid, and helps to improve the suction quality of cigarette.
In sum, composite filter of the present invention can effectively reduce the harmful substance contents in the flue gas, can alleviate the stimulation of flue gas to throat simultaneously, has certain effect that wets one's whistle, promotes the production of body fluid, thereby promotes the suction quality of cigarette.Added the filter stick of hybrid particles, not only do not produced unnecessary assorted gas, and further lifting has been arranged on fragrance.
Claims (10)
1. a filter stick for cigarettes comprises fiber base material and plasticizer, it is characterized in that: the hybrid particles that contains blackberry lily particle and tobacco powder particle in the described fiber base material.
2. filter stick as claimed in claim 1 is characterized in that: the weight ratio of blackberry lily and tobacco powder is in the described mixture: 3～4 parts of blackberry lilys, 6～7 parts of tobacco powders.
3. filter stick as claimed in claim 2 is characterized in that: described hybrid particles is after blackberry lily and pipe tobacco are carried out preliminarily dried respectively and pulverizing, to cross 40～80 mesh sieves, mix the back further under 40～60 ℃, dry by the fire to moisture be 6～10%.
4. filter stick as claimed in claim 2 is characterized in that: described tobacco particle is after pipe tobacco is pulverized, the tobacco powder that obtains after 40～80 mesh sieves, under 40～60 ℃, dry by the fire to moisture be 6～10%.
5. filter stick as claimed in claim 1 is characterized in that: in the described filter stick, the content of compound particles is to contain particle 1.0～1.5mg in the filter stick of every mm length.
6. filter stick as claimed in claim 2 is characterized in that: described hybrid particles evenly makes an addition in the fiber base material; Fiber base material is the diacetate fiber tow.
7. filter stick as claimed in claim 1 is characterized in that: described plasticizer addition is 5%～8% of a filtering material gross weight.
8. a filter stick for cigarettes comprises filter core and the shaping paper that wraps up filter core, it is characterized in that described filter core saves the identical filter core of cross-sectional areas by at least two and forms, and described filter core adjacent face contacts with each other; Described filter core has at least a joint to contain mixture as claimed in claim 1.
9. filter stick as claimed in claim 8 is characterized in that the joint that described filter core contacts with cigarette shreds contains mixture as claimed in claim 1.
10. filter stick according to claim 8 is characterized in that described shaping paper air permeability is 10000CU (Coresta), quantitatively is 28g/m
2
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102504866A CN101897478B (en) | 2010-08-10 | 2010-08-10 | Filter stick for cigarettes and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102504866A CN101897478B (en) | 2010-08-10 | 2010-08-10 | Filter stick for cigarettes and preparation method thereof |
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| CN101897478A true CN101897478A (en) | 2010-12-01 |
| CN101897478B CN101897478B (en) | 2012-06-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2010102504866A Active CN101897478B (en) | 2010-08-10 | 2010-08-10 | Filter stick for cigarettes and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102691170A (en) * | 2012-06-06 | 2012-09-26 | 云南瑞升烟草技术（集团）有限公司 | High tar reduction diacetate fiber non-woven fabric filter material for cigarettes and preparation method for filter material |
| CN105996119A (en) * | 2016-06-22 | 2016-10-12 | 云南中烟工业有限责任公司 | Composite filter tip and application of composite filter tip in heating and incombustible cigarette |
| CN110561840A (en) * | 2019-08-20 | 2019-12-13 | 牡丹江恒丰纸业股份有限公司 | Preparation process of paper filter tip body paper |
| CN111406971A (en) * | 2019-01-04 | 2020-07-14 | 上海新型烟草制品研究院有限公司 | Reconstituted tobacco powder and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1025545C (en) * | 1989-08-10 | 1994-08-03 | R.J.雷诺兹烟草公司 | Tobacco processing |
| CN1194806A (en) * | 1998-04-28 | 1998-10-07 | 华磊 | Nutritive health cigarette and its preparing process |
| CN101711601A (en) * | 2009-12-28 | 2010-05-26 | 四川农业大学 | Drug cigarette and processing method thereof |
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2010
- 2010-08-10 CN CN2010102504866A patent/CN101897478B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1025545C (en) * | 1989-08-10 | 1994-08-03 | R.J.雷诺兹烟草公司 | Tobacco processing |
| CN1194806A (en) * | 1998-04-28 | 1998-10-07 | 华磊 | Nutritive health cigarette and its preparing process |
| CN101711601A (en) * | 2009-12-28 | 2010-05-26 | 四川农业大学 | Drug cigarette and processing method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102691170A (en) * | 2012-06-06 | 2012-09-26 | 云南瑞升烟草技术（集团）有限公司 | High tar reduction diacetate fiber non-woven fabric filter material for cigarettes and preparation method for filter material |
| CN102691170B (en) * | 2012-06-06 | 2014-12-24 | 云南瑞升烟草技术（集团）有限公司 | High tar reduction diacetate fiber non-woven fabric filter material for cigarettes and preparation method for filter material |
| CN105996119A (en) * | 2016-06-22 | 2016-10-12 | 云南中烟工业有限责任公司 | Composite filter tip and application of composite filter tip in heating and incombustible cigarette |
| CN111406971A (en) * | 2019-01-04 | 2020-07-14 | 上海新型烟草制品研究院有限公司 | Reconstituted tobacco powder and preparation method thereof |
| CN110561840A (en) * | 2019-08-20 | 2019-12-13 | 牡丹江恒丰纸业股份有限公司 | Preparation process of paper filter tip body paper |
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| Publication number | Publication date |
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| CN101897478B (en) | 2012-06-27 |
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