CN101857949A - PVD vacuum ion plating method - Google Patents

PVD vacuum ion plating method Download PDF

Info

Publication number
CN101857949A
CN101857949A CN 201010208324 CN201010208324A CN101857949A CN 101857949 A CN101857949 A CN 101857949A CN 201010208324 CN201010208324 CN 201010208324 CN 201010208324 A CN201010208324 A CN 201010208324A CN 101857949 A CN101857949 A CN 101857949A
Authority
CN
China
Prior art keywords
plated film
vacuum ion
pvd vacuum
carry out
ion membrane
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN 201010208324
Other languages
Chinese (zh)
Inventor
吴睿恩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dongguan Quanshuo Metal Processing Co.,Ltd.
Original Assignee
吴睿恩
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 吴睿恩 filed Critical 吴睿恩
Priority to CN 201010208324 priority Critical patent/CN101857949A/en
Publication of CN101857949A publication Critical patent/CN101857949A/en
Pending legal-status Critical Current

Links

Landscapes

  • Physical Vapour Deposition (AREA)

Abstract

The invention belongs to the technical field of plating, and particularly relates to a PVD vacuum ion plating method, which comprises the following preparation steps: (1) pretreating the substrate; (2) dewatering and drying the pre-treated substrate; (3) putting the substrate into a furnace for first plating; (4) taking the substrate out of the furnace for screen printing or offset printing and drying; (5) putting the substrate into the furnace again for second plating; (6) soaking with an organic solvent to remove printing ink in screen printing or offset printing; and (7) cleaning with water to obtain the finished product. The invention introduces the step of screen printing or offset printing in the process of vacuum ion plating so as to make the manufactured product have rich colors.

Description

A kind of method of PVD vacuum ion membrane plating
Technical field
The invention belongs to the coating technique field, be specifically related to a kind of method of PVD vacuum ion membrane plating.
Background technology
Physical vapor deposition (PVD) is by evaporation, and processes such as ionization or sputter produce metallics and are deposited on workpiece surface with reactant gases reaction formation compound.The physical vapor deposition coating film technology mainly is divided three classes, vacuum vapor plating, vacuum sputtering plating and vacuum ion membrane plating.
Wherein, vacuum ion membrane plating is by means of rare gas element glow discharge, makes plating material (as metal titanium) steam raising ionization, and ion quickens through electric field, and with higher-energy bombardment workpiece surface, this moment is as feeding CO 2, N 2Deng reactant gases, just can obtain TiC, TiN tectum at workpiece surface, hardness is up to 2000HV.The important feature of vacuum ion membrane plating is that depositing temperature has only about 500 ℃, and the tectum strong adhesion.Closely during the last ten years, the development of vacuum ion plating membrane technique is the fastest, and it has become one of current state-of-the-art surface treatment mode.
At present, the product colour dullness of vacuum ion membrane plating has only a kind of color, does not have the gradual change of color, does not have color combinations, also the pattern that does not embody by change in color.
Summary of the invention
One of purpose of the present invention provides the method for the abundant vacuum ion membrane plating of a kind of prepared color that plating is combined with wire mark or offset printing.
The object of the present invention is achieved like this.
A kind of method of PVD vacuum ion membrane plating, it comprises and is prepared as follows step:
(1) base material is carried out pre-treatment;
(2) base material with pre-treatment dewaters and oven dry;
(3) advance stove, carry out the plated film first time;
(4) come out of the stove, carry out wire mark or offset printing, drying;
(5) advance stove once more, carry out the plated film second time;
Printing ink when (6) removing wire mark or offset printing with the organic solvent immersion;
(7) water cleans, and gets product.
Wherein, described plated film and wire mark can replace repeatedly and carry out.
Wherein, described plated film and offset printing can replace repeatedly and carry out.
Wherein, described base material is stainless steel, copper or titanium.
Wherein, described pre-treatment comprises successively except that cured ultrasonic cleaning, hot degreasing, electrolysis membrane removal.
Wherein, plated film carries out at vaccum ion coater, at logical N 2Condition under, the plated film time is 2.5-4 hour, coating temperature is 200-350 ℃.
Wherein, the used raw material of plated film is a kind of or several arbitrarily in titanium nitride, TiCN, TiAlN, titanium carbide, zirconium nitride, the hafnium nitride.
Beneficial effect of the present invention is: the method for this kind PVD vacuum ion membrane plating, and it comprises and is prepared as follows step: (1) carries out pre-treatment to base material; (2) base material with pre-treatment dewaters and oven dry; (3) advance stove, carry out the plated film first time; (4) come out of the stove, carry out wire mark or offset printing, drying; (5) advance stove once more, carry out the plated film second time; Printing ink when (6) removing wire mark or offset printing with the organic solvent immersion; (7) water cleans, and gets product.The present invention has introduced wire mark or this step of offset printing in the process of vacuum ion membrane plating, make the product colour that makes abundant.
Embodiment
The invention will be further described below by embodiment, but practical range of the present invention is not limited to this.
A kind of method of PVD vacuum ion membrane plating, it comprises and is prepared as follows step:
(1) base material is carried out pre-treatment, strengthen the sticking power of substrate surface;
(2) base material with pre-treatment dewaters and oven dry;
(3) advance stove, carry out the plated film first time;
(4) come out of the stove, carry out wire mark or offset printing, drying, existing wire mark or offset printing are adopted in wire mark or offset printing, form a pattern by wire mark or offset printing at the substrate surface of plated film, described pattern is the protection pattern, protect primary plated film, for the second time plated film prepare, but both Air drying of drying, also can carry out drying, be preferably 150 ℃ and carry out drying at 120 ℃-160 ℃;
(5) advance stove once more, carry out the plated film second time, for the first time plated film with the second time plated film color different;
Printing ink when (6) removing wire mark or offset printing with the organic solvent immersion, then for the first time plated film and for the second time plated film all can manifest, because the protection pattern that printing ink forms has been protected the color of plated film for the first time, remove the color that then can show plated film for the first time behind the removal ink and be shown as wire mark or the pattern during offset printing;
(7) water cleans, and gets product.
Wherein, described plated film and wire mark or offset printing can replace repeatedly and carry out, and can make the more product of horn of plenty of color like this.
Wherein, described base material is stainless steel, copper or titanium, can certainly can adopt the material of vacuum ion membrane plating for other.
Wherein, described pre-treatment comprises successively except that cured ultrasonic cleaning, hot degreasing (immersion), electrolysis membrane removal.The used raw material of electrolysis membrane removal is activation hydrochlorate and tartrate, carries out anode electrolysis, removes the sull of substrate surface.
Wherein, plated film carries out at vaccum ion coater, at logical N 2Condition under, the plated film time is 2.5-4 hour, coating temperature is 200-350 ℃, specifically can regulate according to the thickness of base material, wherein base vacuum is 6 * 10 -3Pa, making the goods vacuum is 2 * 10 -1Pa.
Wherein, the used raw material of plated film is a kind of or several arbitrarily in titanium nitride, TiCN, TiAlN, titanium carbide, zirconium nitride, the hafnium nitride.
The above only is a better embodiment of the present invention, so all equivalences of doing according to the described structure of patent claim of the present invention, feature and principle change or modify, is included in the patent claim of the present invention.

Claims (7)

1. the method for a PVD vacuum ion membrane plating is characterized in that: it comprises and is prepared as follows step:
(1) base material is carried out pre-treatment;
(2) base material with pre-treatment dewaters and oven dry;
(3) advance stove, carry out the plated film first time;
(4) come out of the stove, carry out wire mark or offset printing, drying;
(5) advance stove once more, carry out the plated film second time;
Printing ink when (6) removing wire mark or offset printing with the organic solvent immersion;
(7) water cleans, and gets product.
2. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: described plated film and wire mark can replace repeatedly and carry out.
3. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: described plated film and offset printing can replace repeatedly and carry out.
4. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: described base material is stainless steel, copper or titanium.
5. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: described pre-treatment comprises successively except that cured ultrasonic cleaning, hot degreasing, electrolysis membrane removal.
6. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: plated film carries out at vaccum ion coater, at logical N 2Condition under, the plated film time is 2.5-4 hour, coating temperature is 200-350 ℃.
7. the method for a kind of PVD vacuum ion membrane plating according to claim 1 is characterized in that: the used raw material of plated film is a kind of or several arbitrarily in titanium nitride, TiCN, TiAlN, titanium carbide, zirconium nitride, the hafnium nitride.
CN 201010208324 2010-06-24 2010-06-24 PVD vacuum ion plating method Pending CN101857949A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201010208324 CN101857949A (en) 2010-06-24 2010-06-24 PVD vacuum ion plating method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201010208324 CN101857949A (en) 2010-06-24 2010-06-24 PVD vacuum ion plating method

Publications (1)

Publication Number Publication Date
CN101857949A true CN101857949A (en) 2010-10-13

Family

ID=42944104

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201010208324 Pending CN101857949A (en) 2010-06-24 2010-06-24 PVD vacuum ion plating method

Country Status (1)

Country Link
CN (1) CN101857949A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102501463A (en) * 2011-11-03 2012-06-20 厦门建霖工业有限公司 Method for preparing simulated metal drawn wire on surface of plastic
CN103085575A (en) * 2011-11-02 2013-05-08 森科五金(深圳)有限公司 Preparation and color separation method of double-color film
CN110616411A (en) * 2019-09-23 2019-12-27 海盐鑫中岳电子科技有限公司 PVD vacuum coating process and coated workpiece

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6475660A (en) * 1987-09-18 1989-03-22 Kowa Eng Kk Multicoloration method for metallic surface
CN101376602A (en) * 2008-09-23 2009-03-04 林敏� Method for forming one layer or multiple layers of metal patterns on surface of ceramic products
CN201309290Y (en) * 2008-07-01 2009-09-16 比亚迪股份有限公司 Metal plate
CN101654769A (en) * 2009-08-26 2010-02-24 杭州泛亚水暖器材有限公司 Vacuum ion plating method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6475660A (en) * 1987-09-18 1989-03-22 Kowa Eng Kk Multicoloration method for metallic surface
CN201309290Y (en) * 2008-07-01 2009-09-16 比亚迪股份有限公司 Metal plate
CN101376602A (en) * 2008-09-23 2009-03-04 林敏� Method for forming one layer or multiple layers of metal patterns on surface of ceramic products
CN101654769A (en) * 2009-08-26 2010-02-24 杭州泛亚水暖器材有限公司 Vacuum ion plating method

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103085575A (en) * 2011-11-02 2013-05-08 森科五金(深圳)有限公司 Preparation and color separation method of double-color film
CN102501463A (en) * 2011-11-03 2012-06-20 厦门建霖工业有限公司 Method for preparing simulated metal drawn wire on surface of plastic
CN102501463B (en) * 2011-11-03 2015-04-08 厦门建霖工业有限公司 Method for preparing simulated metal drawn wire on surface of plastic
CN110616411A (en) * 2019-09-23 2019-12-27 海盐鑫中岳电子科技有限公司 PVD vacuum coating process and coated workpiece
CN110616411B (en) * 2019-09-23 2021-09-07 海盐鑫中岳电子科技有限公司 PVD vacuum coating process and coated workpiece

Similar Documents

Publication Publication Date Title
CN102345099B (en) Preparation method of multilayer pitting corrosion-resistant coating of steam turbine blade material surface
TW201317381A (en) Method for manufacturing a housing and the housing
CN101985738A (en) Method for depositing metal or hard ornament film on plastic substrate
WO2009014394A3 (en) Method for depositing ceramic thin film by sputtering using non-conductive target
CN103590082B (en) A kind of without phosphorus, non-hexavalent chromium environment friendly shape glue electro-plating method
CN101337831B (en) Method for metalizing surface of ceramic
CN108220959B (en) Plastic chromium-free coarsening treatment method and water-saving electroplating method thereof
CN108588643B (en) Method for preparing black tungsten carbide composite coating by physical vapor deposition method
CN101857949A (en) PVD vacuum ion plating method
CN102029765B (en) Method for manufacturing multicolor wear-resistant metal decorative film layer
CN105779943A (en) Method of preparing hydrophobic membrane through physical vapor deposition of fluoroalkyl silane
CN113174570A (en) High-toughness TiAlNiN coating and preparation method and application thereof
CN100439100C (en) Composite coat capable of replacing piston ring surface electroplating hard chrome and processing method thereof
CN110438461B (en) TiBxPreparation method of/Cr (x = 1.9-3.5) antioxidant multilayer coating
CN108265271A (en) A kind of method that physical vaporous deposition makes blue film on product
CN117626195A (en) Preparation method of silicon carbide protective coating based on high-power pulse magnetron sputtering
CN204661820U (en) A kind of PVD vaccum ion coater
US20200347490A1 (en) Metal surface protective layer and preparation method thereof
CN109487214A (en) A kind of magnesium-alloy surface coating method and Corrosion-resistant magnesia alloy prepared therefrom
CN113617610B (en) Method for preparing metallic luster faucet by coating brass or zinc alloy base material
TW201250018A (en) Coated articles and mathod for making the same
CN107130275A (en) A kind of method of zinc alloy anode oxidation
CN208440686U (en) The coated objects made from precious metals of surface band
CN113549869A (en) Vacuum coating method with antique grain effect
CN109666912B (en) Hf/TiBxMethod for producing an anti-corrosion multilayer coating

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: DONGGUAN QUANSHUO HARDWARE MACHINING CO., LTD.

Free format text: FORMER OWNER: WU RUIEN

Effective date: 20110812

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 523850 DONGGUAN, GUANGDONG PROVINCE TO: 523860 DONGGUAN, GUANGDONG PROVINCE

TA01 Transfer of patent application right

Effective date of registration: 20110812

Address after: 523860 Guangdong city of Dongguan province Changan Zhen Xiao Chong Industrial Zone Dongguan City Quan Shuo Hardware Processing Co. Ltd.

Applicant after: Dongguan Quanshuo Metal Processing Co.,Ltd.

Address before: 523850, Changan Town, Guangdong City, Dongguan Province, Changan automobile station opposite Changan industrial city, Dongguan Quan Shuo Hardware Processing Co., Ltd.

Applicant before: Wu Ruien

C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Open date: 20101013