BR112020008913B1 - Processo para fracionamento a seco de uma oleína de óleo de palma, sistema de fracionamento e fração intermediária de óleo de palma - Google Patents

Processo para fracionamento a seco de uma oleína de óleo de palma, sistema de fracionamento e fração intermediária de óleo de palma Download PDF

Info

Publication number: BR112020008913B1
Authority: BR; Brazil
Prior art keywords: palm oil; olein; fraction; oil olein; fact
Prior art date: 2017-11-22

Application number

BR112020008913-3A

Other languages

English (en)

Portuguese (pt)

Other versions

BR112020008913A2 (pt

Inventor

Jeppe Lindegaard Hjorth

Original Assignee

Aak Ab (Publ)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2017-11-22

Filing date

2017-11-22

Publication date

2024-01-02

2017-11-22 Application filed by Aak Ab (Publ) filed Critical Aak Ab (Publ)

2020-10-20 Publication of BR112020008913A2 publication Critical patent/BR112020008913A2/pt

2024-01-02 Publication of BR112020008913B1 publication Critical patent/BR112020008913B1/pt

Links

235000019482 Palm oil Nutrition 0.000 title claims abstract description 513
239000002540 palm oil Substances 0.000 title claims abstract description 513
PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 title claims abstract description 421
238000005194 fractionation Methods 0.000 title claims abstract description 120
238000000034 method Methods 0.000 title claims abstract description 86
230000008569 process Effects 0.000 title claims abstract description 82
238000009210 therapy by ultrasound Methods 0.000 claims abstract description 71
238000001816 cooling Methods 0.000 claims abstract description 65
238000002604 ultrasonography Methods 0.000 claims abstract description 64
239000006228 supernatant Substances 0.000 claims abstract description 9
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 28
239000011630 iodine Substances 0.000 claims description 28
229910052740 iodine Inorganic materials 0.000 claims description 28
238000002425 crystallisation Methods 0.000 claims description 23
230000008025 crystallization Effects 0.000 claims description 23
238000013138 pruning Methods 0.000 claims description 19
239000003921 oil Substances 0.000 claims description 14
235000019198 oils Nutrition 0.000 claims description 14
SSZWWUDQMAHNAQ-UHFFFAOYSA-N 3-chloropropane-1,2-diol Chemical compound OCC(O)CCl SSZWWUDQMAHNAQ-UHFFFAOYSA-N 0.000 claims description 13
238000010438 heat treatment Methods 0.000 claims description 11
238000002844 melting Methods 0.000 claims description 11
230000008018 melting Effects 0.000 claims description 10
238000000926 separation method Methods 0.000 claims description 9
238000001914 filtration Methods 0.000 claims description 6
238000003825 pressing Methods 0.000 claims description 6
239000002002 slurry Substances 0.000 claims description 5
101150093727 sspO gene Proteins 0.000 abstract 3
240000005589 Calophyllum inophyllum Species 0.000 abstract 2
DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 32
150000003626 triacylglycerols Chemical class 0.000 description 11
239000000047 product Substances 0.000 description 8
230000008901 benefit Effects 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
238000013019 agitation Methods 0.000 description 4
239000000498 cooling water Substances 0.000 description 4
239000003925 fat Substances 0.000 description 4
235000019197 fats Nutrition 0.000 description 4
150000004665 fatty acids Chemical class 0.000 description 4
239000007788 liquid Substances 0.000 description 4
VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 3
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
235000014113 dietary fatty acids Nutrition 0.000 description 3
229930195729 fatty acid Natural products 0.000 description 3
239000000194 fatty acid Substances 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
239000002904 solvent Substances 0.000 description 3
230000003068 static effect Effects 0.000 description 3
DYPJJAAKPQKWTM-UHFFFAOYSA-N 2-chloropropane-1,3-diol Chemical compound OCC(Cl)CO DYPJJAAKPQKWTM-UHFFFAOYSA-N 0.000 description 2
OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 2
238000003723 Smelting Methods 0.000 description 2
238000010923 batch production Methods 0.000 description 2
235000009508 confectionery Nutrition 0.000 description 2
239000013078 crystal Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
238000005516 engineering process Methods 0.000 description 2
150000002148 esters Chemical class 0.000 description 2
239000012467 final product Substances 0.000 description 2
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
230000005012 migration Effects 0.000 description 2
238000013508 migration Methods 0.000 description 2
239000000203 mixture Substances 0.000 description 2
238000012986 modification Methods 0.000 description 2
230000004048 modification Effects 0.000 description 2
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical group CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 2
238000011020 pilot scale process Methods 0.000 description 2
238000005086 pumping Methods 0.000 description 2
239000000725 suspension Substances 0.000 description 2
235000013311 vegetables Nutrition 0.000 description 2
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
SSZWWUDQMAHNAQ-VMIGTVKRSA-N 3-chloropropane-1,2-diol Chemical class O[13CH2][13CH](O)[13CH2]Cl SSZWWUDQMAHNAQ-VMIGTVKRSA-N 0.000 description 1
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
239000005642 Oleic acid Substances 0.000 description 1
235000021314 Palmitic acid Nutrition 0.000 description 1
235000021355 Stearic acid Nutrition 0.000 description 1
241001062472 Stokellia anisodon Species 0.000 description 1
238000013459 approach Methods 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
235000014121 butter Nutrition 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
235000019219 chocolate Nutrition 0.000 description 1
239000002826 coolant Substances 0.000 description 1
239000012809 cooling fluid Substances 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
235000011194 food seasoning agent Nutrition 0.000 description 1
235000019869 fractionated palm oil Nutrition 0.000 description 1
235000021588 free fatty acids Nutrition 0.000 description 1
IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 description 1
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
230000002045 lasting effect Effects 0.000 description 1
229940049918 linoleate Drugs 0.000 description 1
235000020778 linoleic acid Nutrition 0.000 description 1
OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
150000002632 lipids Chemical class 0.000 description 1
239000000463 material Substances 0.000 description 1
239000012528 membrane Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
230000006911 nucleation Effects 0.000 description 1
238000010899 nucleation Methods 0.000 description 1
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
229940049964 oleate Drugs 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
238000011946 reduction process Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000008117 stearic acid Substances 0.000 description 1
UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
238000003828 vacuum filtration Methods 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0081—Use of vibrations, e.g. ultrasound
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Crystallography & Structural Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Thermal Sciences (AREA)
Physics & Mathematics (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Mechanical Engineering (AREA)
Microbiology (AREA)
Fats And Perfumes (AREA)
Edible Oils And Fats (AREA)

BR112020008913-3A 2017-11-22 2017-11-22 Processo para fracionamento a seco de uma oleína de óleo de palma, sistema de fracionamento e fração intermediária de óleo de palma BR112020008913B1 (pt)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PCT/SE2017/051160 WO2019103667A1 (fr)	2017-11-22	2017-11-22	Procédé de fractionnement à sec d'une oléine d'huile de palme

Publications (2)

Publication Number	Publication Date
BR112020008913A2 BR112020008913A2 (pt)	2020-10-20
BR112020008913B1 true BR112020008913B1 (pt)	2024-01-02

Family

ID=66632041

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
BR112020008913-3A BR112020008913B1 (pt)	2017-11-22	2017-11-22	Processo para fracionamento a seco de uma oleína de óleo de palma, sistema de fracionamento e fração intermediária de óleo de palma

Country Status (3)

Country	Link
BR (1)	BR112020008913B1 (fr)
MY (1)	MY195987A (fr)
WO (1)	WO2019103667A1 (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN112639063A (zh) *	2018-08-24	2021-04-09	Aak股份有限公司	用于干式分提以获得最终硬棕榈油中间馏分的方法
CN110257169A (zh) *	2019-06-12	2019-09-20	深圳精益油脂技术有限公司	一种制备低缩水甘油酯及低3-mcpd酯含量的棕榈油的方法
CN110982616A (zh) *	2019-11-20	2020-04-10	东莞理工学院	一种棕榈油的超声波分提设备
CN110655981A (zh) *	2019-11-20	2020-01-07	中储粮油脂工业东莞有限公司	一种结合两个结晶罐的棕榈油超声波分提设备

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6630185B2 (en) *	2000-07-18	2003-10-07	Lipton, Division Of Conopco, Inc.	Crystallization process using ultrasound
ES2279109T3 (es) *	2002-05-31	2007-08-16	Accentus Plc	Produccion de materiales cristalinos utilizando un ultrasonido de alta intensidad.
EP1889898B1 (fr) *	2005-04-14	2014-11-12	Adeka Corporation	Procede de fractionnement a sec pour les graisses
JP4091099B1 (ja) *	2007-08-28	2008-05-28	株式会社Ｊ−オイルミルズ	乾式分別法、これを用いた高液状性パーム油および油脂組成物
JP2014162859A (ja) *	2013-02-26	2014-09-08	Fuji Oil Co Ltd	油脂の乾式分別方法
GB2548117B (en) *	2016-03-08	2022-10-26	Lewtas Science & Tech Ltd	Use of ultrasound and acoustics to control crystallisation

2017
- 2017-11-22 BR BR112020008913-3A patent/BR112020008913B1/pt active IP Right Grant
- 2017-11-22 WO PCT/SE2017/051160 patent/WO2019103667A1/fr active Application Filing
- 2017-11-22 MY MYPI2020002145A patent/MY195987A/en unknown

Also Published As

Publication number	Publication date
BR112020008913A2 (pt)	2020-10-20
WO2019103667A1 (fr)	2019-05-31
MY195987A (en)	2023-02-27

Legal Events

Date	Code	Title	Description
2021-08-10	B06W	Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette]
2021-11-23	B350	Update of information on the portal [chapter 15.35 patent gazette]
2023-08-22	B06A	Patent application procedure suspended [chapter 6.1 patent gazette]
2023-11-28	B09A	Decision: intention to grant [chapter 9.1 patent gazette]
2024-01-02	B16A	Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]	Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 22/11/2017, OBSERVADAS AS CONDICOES LEGAIS
2024-02-27	B25G	Requested change of headquarter approved	Owner name: AAK AB (PUBL) (SE)

Publication	Publication Date	Title
BR112020008913B1 (pt)	2024-01-02	Processo para fracionamento a seco de uma oleína de óleo de palma, sistema de fracionamento e fração intermediária de óleo de palma
JP5827568B2 (ja)	2015-12-02	食用油の精製
JP5654355B2 (ja)	2015-01-14	パーム油製品の製造方法
JPH0216960B2 (fr)	1990-04-18
JPS63162796A (ja)	1988-07-06	脂肪酸の分画方法
JP2011506710A5 (fr)	2014-03-27
CN103614239B (zh)	2014-11-05	抗低温高碘值棕榈油的制备方法
US9051533B2 (en)	2015-06-09	Continuous fractionation of triglyceride oils
EP3227418B1 (fr)	2019-09-04	Procédé continu de fractionnement à sec d'huiles glycéridiques
BR112021003367A2 (pt)	2021-05-11	processo para o fracionamento seco para se obter uma fração média de óleo de palma duro final
JP2009215437A (ja)	2009-09-24	米ぬか油の製造方法
Peters‐Erjawetz et al.	1999	Milk fat fractionation by solid‐layer melt crystallization
EP3294851B1 (fr)	2021-02-17	Frigélisation d'huile de poisson
Calliauw et al.	2007	Phase composition during palm olein fractionation and its effect on soft PMF and superolein quality
US2910363A (en)	1959-10-27	Method for the fractional crystallization of cottonseed oil
JP2009051973A (ja)	2009-03-12	乾式分別法、これを用いた高液状性パーム油および油脂組成物
Yahya et al.	2015	Effect of coolant temperature on progressive freeze concentration of refined, bleached and deodorised palm oil based on process efficiency and heat transfer
JP3656863B2 (ja)	2005-06-08	高度不飽和脂肪酸残基含量の高い油脂の製造方法
JP2014162859A (ja)	2014-09-08	油脂の乾式分別方法
US8962874B2 (en)	2015-02-24	Process for fractionating crude triglyceride oil
WO2013036096A1 (fr)	2013-03-14	Procédé pour la production d'huile de triacylglycérol
Jusoh et al.	2014	Effect of Flowrate and Circulation Time on Fractionation of Refined Bleached and Deodorised Palm Oil using Progressive Freeze Concentration Method
JP2005281462A (ja)	2005-10-13	油脂類の分別方法、それに用いるシード及び分別油脂
Hishamuddin et al.	2023	MORPHOLOGY AND SIZE DISTRIBUTION OF PALM OLEIN CRYSTALS DURING FRACTIONAL CRYSTALLIZATION WITH BEHENIC ACID
Jusoh et al.	2014	Effect of coolant temperature on progressive freeze concentration of refined, bleached and deodorised palm oil