BR0311688A - processo para a produção de cristais de carotenóides partindo de uma resina oleosa de um vegetal que contém carotenóide - Google Patents
processo para a produção de cristais de carotenóides partindo de uma resina oleosa de um vegetal que contém carotenóideInfo
- Publication number
- BR0311688A BR0311688A BRPI0311688-3A BR0311688A BR0311688A BR 0311688 A BR0311688 A BR 0311688A BR 0311688 A BR0311688 A BR 0311688A BR 0311688 A BR0311688 A BR 0311688A
- Authority
- BR
- Brazil
- Prior art keywords
- carotenoid
- production
- crystals
- saponification reaction
- organic
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
- A23L5/44—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives using carotenoids or xanthophylls
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCESSO PARA A PRODUçãO DE CRISTAIS DE CAROTENóIDES PARTINDO DE UMA RESINA OLEOSA DE UM VEGETAL QUE CONTêM CAROTENóIDE. Um processo para a produção de cristais de carotenóides partindo de uma resina oleosa de um vegetal que contém carotenóide cujo processo compreende (a) uma primeira etapa de introduzir a resina oleosa a um solvente orgânico, um álcool e uma base sob temperatura de refluxo do solvente orgânico para formar uma mistura da reação de saponificação; (b) manter a dita mistura da reação de saponificação durante um período de tempo suficiente para completar a reação de saponificação, desse modo produzindo um produto saponificado; (e) permitir que o produto saponificado resultante se separe em duas fases que compreendem uma fase orgânica e uma fase aquosa; (d) separar as duas fases e extraindo-se a fase aquosa; (e) destilar a dita fase orgânica para se obter os cristais de carotenóides.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02356104A EP1371641A1 (en) | 2002-06-10 | 2002-06-10 | Process for the formation and isolation of carotenoid crystals |
PCT/IB2003/002101 WO2003104190A1 (en) | 2002-06-10 | 2003-06-04 | Process for the formation and isolation of carotenoid crystals |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0311688A true BR0311688A (pt) | 2008-01-15 |
Family
ID=29558444
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0311688-3A BR0311688A (pt) | 2002-06-10 | 2003-06-04 | processo para a produção de cristais de carotenóides partindo de uma resina oleosa de um vegetal que contém carotenóide |
Country Status (14)
Country | Link |
---|---|
US (1) | US20050139145A1 (pt) |
EP (2) | EP1371641A1 (pt) |
JP (1) | JP2005535609A (pt) |
CN (1) | CN1283623C (pt) |
AU (1) | AU2003240153A1 (pt) |
BR (1) | BR0311688A (pt) |
CA (1) | CA2487013A1 (pt) |
MX (1) | MXPA04012134A (pt) |
PE (1) | PE20040141A1 (pt) |
PL (1) | PL372759A1 (pt) |
RU (1) | RU2004138796A (pt) |
UA (1) | UA77308C2 (pt) |
WO (1) | WO2003104190A1 (pt) |
ZA (1) | ZA200409355B (pt) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1877371B1 (en) * | 2005-04-25 | 2010-10-06 | Katra Phytochem Private Limited | Isolation and purification of carotenoids from marigold flowers |
ES2265787B1 (es) * | 2005-08-09 | 2007-11-16 | Carotenoid Technologies, S.A. | Procedimiento para la preparacion de un pigmento a partir de oleorresinas naturales ricas en esteres de xantofilas. |
WO2009027850A2 (en) * | 2007-06-06 | 2009-03-05 | Multi-Tech Specialty Chemicals Co., Ltd. | Process for the preparation of xanthophyll crystals |
CN101260071B (zh) * | 2008-04-15 | 2010-06-09 | 中国日用化学工业研究院 | 叶黄素的分离与纯化方法 |
US7875751B2 (en) * | 2008-11-07 | 2011-01-25 | Allied Biotech Corporation | Method for the purification of carotenoids from plant extracts and the products so obtained |
EP2196207B1 (en) * | 2008-12-12 | 2012-09-05 | Allied Biotech Corporation | Method for the purification of carotenoids from plant extracts and the products so obtained |
CN101828693B (zh) * | 2009-03-09 | 2013-01-02 | 浙江医药股份有限公司新昌制药厂 | 制备低粘度高流动性类胡萝卜素油悬浮液的方法及其应用 |
US8716533B2 (en) | 2009-05-29 | 2014-05-06 | Kalamazoo Holdings, Inc. | Methods of saponifying xanthophyll esters and isolating xanthophylls |
US8247615B2 (en) | 2010-05-14 | 2012-08-21 | Kalamazoo Holdings, Inc. | Process of converting esterified xanthophylls from Capsicum to non-esterified xanthophylls in high yields and purities |
US8008532B2 (en) * | 2009-09-15 | 2011-08-30 | Unibar Corporation | Processes and methods for extraction and purification of lutein from marigold esters |
WO2011145112A1 (en) | 2010-05-17 | 2011-11-24 | Dynadis Biotehc (India) Private Limited | Process for isolation and purification of carotenoids |
CN102139877A (zh) * | 2011-01-26 | 2011-08-03 | 山东盛华光伏材料有限公司 | 一种采用含铁化合物去除工业硅中硼磷杂质的方法 |
US9271935B2 (en) | 2012-12-19 | 2016-03-01 | Novus International, Inc. | Xanthophyll compositions and methods of use |
CN104447464B (zh) * | 2013-09-24 | 2016-11-23 | 浙江医药股份有限公司新昌制药厂 | 一种植物来源含天然虾青素的类胡萝卜素化合物及其制备方法和组合物 |
CN106280542B (zh) * | 2016-08-15 | 2017-11-17 | 晨光生物科技集团股份有限公司 | 一种提高番茄红素油树脂品质的生产方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2572467A (en) * | 1949-08-04 | 1951-10-23 | Colgate Palmolive Peet Co | Concentration and recovery of carotenoid pigments from palm oil |
US5382714A (en) * | 1994-03-17 | 1995-01-17 | The Catholic University Of America | Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof |
JP3398248B2 (ja) * | 1995-03-16 | 2003-04-21 | 新日本石油株式会社 | キサントフィル化合物の精製方法 |
US5648564A (en) * | 1995-12-21 | 1997-07-15 | Kemin Industries, Inc. | Process for the formation, isolation and purification of comestible xanthophyll crystals from plants |
WO1999020587A1 (en) * | 1997-10-21 | 1999-04-29 | Office Of Technology Liaison | Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants |
US6191293B1 (en) * | 1998-04-20 | 2001-02-20 | Inexa, Industria Extractora C.A. | Trans-xanthophyll ester concentrates of enhanced purity and methods of making same |
JP5220255B2 (ja) * | 2000-01-27 | 2013-06-26 | コニンクリーケ デーエスエム ナムローゼ フェンノートシャップ | カロテノイド結晶の単離 |
WO2002004415A2 (en) * | 2000-07-12 | 2002-01-17 | University Of Maryland, College Park | Process for purification and crystallization of palm oil carotenoids |
EP1253131A1 (en) * | 2001-04-24 | 2002-10-30 | Aventis Animal Nutrition S.A. | Process for the preparation of an xanthophyll |
US6380442B1 (en) * | 2001-10-10 | 2002-04-30 | Bioactives, Llc | Process for the isolation of mixed carotenoids from plants |
-
2002
- 2002-06-10 EP EP02356104A patent/EP1371641A1/en not_active Withdrawn
-
2003
- 2003-04-06 UA UA20041210601A patent/UA77308C2/uk unknown
- 2003-06-04 AU AU2003240153A patent/AU2003240153A1/en not_active Abandoned
- 2003-06-04 MX MXPA04012134A patent/MXPA04012134A/es not_active Application Discontinuation
- 2003-06-04 JP JP2004511260A patent/JP2005535609A/ja active Pending
- 2003-06-04 WO PCT/IB2003/002101 patent/WO2003104190A1/en not_active Application Discontinuation
- 2003-06-04 RU RU2004138796/04A patent/RU2004138796A/ru not_active Application Discontinuation
- 2003-06-04 US US10/514,044 patent/US20050139145A1/en not_active Abandoned
- 2003-06-04 CA CA002487013A patent/CA2487013A1/en not_active Abandoned
- 2003-06-04 BR BRPI0311688-3A patent/BR0311688A/pt not_active IP Right Cessation
- 2003-06-04 EP EP03732768A patent/EP1515948A1/en not_active Withdrawn
- 2003-06-04 CN CNB038133989A patent/CN1283623C/zh not_active Expired - Fee Related
- 2003-06-04 PL PL03372759A patent/PL372759A1/xx not_active Application Discontinuation
- 2003-06-06 PE PE2003000568A patent/PE20040141A1/es not_active Application Discontinuation
-
2004
- 2004-11-19 ZA ZA200409355A patent/ZA200409355B/en unknown
Also Published As
Publication number | Publication date |
---|---|
CA2487013A1 (en) | 2003-12-18 |
ZA200409355B (en) | 2005-05-19 |
EP1371641A1 (en) | 2003-12-17 |
EP1515948A1 (en) | 2005-03-23 |
PE20040141A1 (es) | 2004-05-04 |
PL372759A1 (en) | 2005-08-08 |
JP2005535609A (ja) | 2005-11-24 |
CN1659140A (zh) | 2005-08-24 |
AU2003240153A1 (en) | 2003-12-22 |
RU2004138796A (ru) | 2005-06-27 |
UA77308C2 (en) | 2006-11-15 |
US20050139145A1 (en) | 2005-06-30 |
MXPA04012134A (es) | 2005-04-19 |
WO2003104190A1 (en) | 2003-12-18 |
CN1283623C (zh) | 2006-11-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE 7A., E 8A. ANUIDADE(S). |
|
B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: NAO APRESENTADA A GUIA DE CUMPRIMENTO DE EXIGENCIA. REFERENTE AS 7A E 8A ANUIDADES. |