ATE430169T1 - Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung fluorierter olefine und olefinischer kohlenwasserstoffcopolymere - Google Patents
Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung fluorierter olefine und olefinischer kohlenwasserstoffcopolymereInfo
- Publication number
- ATE430169T1 ATE430169T1 AT03768534T AT03768534T ATE430169T1 AT E430169 T1 ATE430169 T1 AT E430169T1 AT 03768534 T AT03768534 T AT 03768534T AT 03768534 T AT03768534 T AT 03768534T AT E430169 T1 ATE430169 T1 AT E430169T1
- Authority
- AT
- Austria
- Prior art keywords
- emulsion polymerization
- aqueous emulsion
- emulgator
- free aqueous
- polymerization process
- Prior art date
Links
- 239000004215 Carbon black (E152) Substances 0.000 title abstract 4
- 150000001336 alkenes Chemical class 0.000 title abstract 4
- 229930195733 hydrocarbon Natural products 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 229920001577 copolymer Polymers 0.000 title abstract 2
- 238000007720 emulsion polymerization reaction Methods 0.000 title abstract 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 abstract 6
- -1 hydrocarbon olefin Chemical class 0.000 abstract 4
- 238000007334 copolymerization reaction Methods 0.000 abstract 1
- 239000003995 emulsifying agent Substances 0.000 abstract 1
- 229920002313 fluoropolymer Polymers 0.000 abstract 1
- 239000004811 fluoropolymer Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US42277002P | 2002-10-31 | 2002-10-31 | |
| PCT/US2003/033233 WO2004041878A1 (en) | 2002-10-31 | 2003-10-21 | Emulsifier free aqueous emulsion polymerization to produce copolymers of a fluorinated olefin and hydrocarbon olefin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE430169T1 true ATE430169T1 (de) | 2009-05-15 |
Family
ID=32312556
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03768534T ATE430169T1 (de) | 2002-10-31 | 2003-10-21 | Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung fluorierter olefine und olefinischer kohlenwasserstoffcopolymere |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US7064170B2 (de) |
| EP (1) | EP1556426B1 (de) |
| JP (1) | JP2006504844A (de) |
| CN (1) | CN100354324C (de) |
| AT (1) | ATE430169T1 (de) |
| AU (1) | AU2003291646A1 (de) |
| DE (1) | DE60327452D1 (de) |
| RU (1) | RU2342403C2 (de) |
| WO (1) | WO2004041878A1 (de) |
| ZA (1) | ZA200504411B (de) |
Families Citing this family (46)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7125941B2 (en) * | 2001-03-26 | 2006-10-24 | 3M Innovative Properties Company | Aqueous emulsion polymerization process for producing fluoropolymers |
| CA2446014A1 (en) * | 2001-05-02 | 2002-11-07 | 3M Innovative Properties Company | Aqueous emulsion polymerization in the presence of ethers as chain transfer agents to produce fluoropolymers |
| US7279522B2 (en) * | 2001-09-05 | 2007-10-09 | 3M Innovative Properties Company | Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant |
| WO2004041878A1 (en) * | 2002-10-31 | 2004-05-21 | 3M Innovative Properties Company | Emulsifier free aqueous emulsion polymerization to produce copolymers of a fluorinated olefin and hydrocarbon olefin |
| ATE502062T1 (de) | 2003-10-24 | 2011-04-15 | 3M Innovative Properties Co | Wässrige dispersionen von polytetrafluorethylenteilchen |
| DE602004021467D1 (de) * | 2004-03-01 | 2009-07-23 | 3M Innovative Properties Co | Verfahren zum Beschichten eines Gegenstands mit einer fluorhaltigen Kunststoffsdispersion |
| US7691932B2 (en) | 2004-09-27 | 2010-04-06 | 3M Innovative Properties Company | Method of making a composition and nanocomposites therefrom |
| US20060270780A1 (en) * | 2005-05-25 | 2006-11-30 | Ping Xu | High purity perfluoroelastomer composites and a processes to produce the same |
| US7488781B2 (en) | 2005-05-25 | 2009-02-10 | Gore Enterprise Holdings, Inc. | High purity transparent perfluoroelastomer parts and a process to produce the same |
| GB2427170A (en) * | 2005-06-17 | 2006-12-20 | 3M Innovative Properties Co | Fluoropolymer film having glass microspheres |
| GB0525978D0 (en) * | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
| GB0514398D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| US20080015304A1 (en) | 2006-07-13 | 2008-01-17 | Klaus Hintzer | Aqueous emulsion polymerization process for producing fluoropolymers |
| GB0514387D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| GB0523853D0 (en) | 2005-11-24 | 2006-01-04 | 3M Innovative Properties Co | Fluorinated surfactants for use in making a fluoropolymer |
| US7671112B2 (en) | 2005-07-15 | 2010-03-02 | 3M Innovative Properties Company | Method of making fluoropolymer dispersion |
| GB2430437A (en) * | 2005-09-27 | 2007-03-28 | 3M Innovative Properties Co | Method of making a fluoropolymer |
| US7728087B2 (en) | 2005-12-23 | 2010-06-01 | 3M Innovative Properties Company | Fluoropolymer dispersion and method for making the same |
| CN101443366B (zh) | 2006-05-10 | 2012-07-18 | 大金工业株式会社 | 含氟聚合物的制造方法 |
| US7754795B2 (en) * | 2006-05-25 | 2010-07-13 | 3M Innovative Properties Company | Coating composition |
| US20070276103A1 (en) * | 2006-05-25 | 2007-11-29 | 3M Innovative Properties Company | Fluorinated Surfactants |
| US8119750B2 (en) * | 2006-07-13 | 2012-02-21 | 3M Innovative Properties Company | Explosion taming surfactants for the production of perfluoropolymers |
| EP2132143B1 (de) * | 2007-02-16 | 2012-12-26 | 3M Innovative Properties Company | System und verfahren zur entfernung von fluorchemikalien aus wasser |
| US20080264864A1 (en) * | 2007-04-27 | 2008-10-30 | 3M Innovative Properties Company | PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT |
| EP2155830A1 (de) * | 2007-05-23 | 2010-02-24 | 3M Innovative Properties Company | Wässrige zusammensetzungen von fluortensiden und ihre verwendung |
| CN101679569A (zh) * | 2007-06-06 | 2010-03-24 | 3M创新有限公司 | 氟化醚组合物以及使用该组合物的方法 |
| GB0712191D0 (en) * | 2007-06-25 | 2007-08-01 | 3M Innovative Properties Co | Process for removing fluorinated compounds for an aqueous phase originating from the preparation of fluoropolymers |
| JP5532532B2 (ja) * | 2007-06-25 | 2014-06-25 | ダイキン工業株式会社 | 低分子量ポリテトラフルオロエチレン水性分散液及びその製造方法 |
| US9040646B2 (en) * | 2007-10-04 | 2015-05-26 | W. L. Gore & Associates, Inc. | Expandable TFE copolymers, methods of making, and porous, expanded articles thereof |
| US8637144B2 (en) * | 2007-10-04 | 2014-01-28 | W. L. Gore & Associates, Inc. | Expandable TFE copolymers, method of making, and porous, expended articles thereof |
| US9650479B2 (en) | 2007-10-04 | 2017-05-16 | W. L. Gore & Associates, Inc. | Dense articles formed from tetrafluoroethylene core shell copolymers and methods of making the same |
| WO2010009191A2 (en) * | 2008-07-18 | 2010-01-21 | 3M Innovative Properties Company | Fluorinated ether compounds and methods of using the same |
| CN102282191A (zh) * | 2008-11-25 | 2011-12-14 | 3M创新有限公司 | 氟化醚尿烷及其使用方法 |
| US8629089B2 (en) | 2008-12-18 | 2014-01-14 | 3M Innovative Properties Company | Method of contacting hydrocarbon-bearing formations with fluorinated ether compositions |
| JP5407643B2 (ja) * | 2009-07-31 | 2014-02-05 | 旭硝子株式会社 | 含フッ素共重合体の製造方法 |
| US9255164B2 (en) | 2010-11-09 | 2016-02-09 | The Chemours Company Fc, Llc | Aqueous polymerization of perfluoromonomer using hydrocarbon surfactant |
| EP2638083B1 (de) | 2010-11-09 | 2019-04-10 | The Chemours Company FC, LLC | Wässrige polymerisation von fluorierten monomeren unter verwendung eines polymerisationsmittels, das kohlenwasserstofftensid umfasst |
| JP6201236B2 (ja) | 2010-11-09 | 2017-09-27 | ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー | フルオロモノマーの水性重合における核形成 |
| CN103748123B (zh) * | 2011-05-03 | 2017-02-15 | 索尔维特殊聚合物意大利有限公司 | 用于制造含氟弹性体的方法 |
| US10079388B2 (en) | 2011-07-15 | 2018-09-18 | Solvay Specialty Polymers Italy S.P.A. | Aqueous vinylidene fluoride-(meth)acrylic co-polymer latex, electrode and lithium ion secondary battery using the same |
| EP2927246B1 (de) * | 2013-01-23 | 2017-10-25 | Daikin Industries, Ltd. | Verfahren zur rückgewinnung von fluorhaltigem ether |
| US9676929B2 (en) | 2013-11-26 | 2017-06-13 | The Chemours Company Fc, Llc | Employing polyalkylene oxides for nucleation in aqueous polymerization of fluoromonomer |
| US9644054B2 (en) | 2014-12-19 | 2017-05-09 | W. L. Gore & Associates, Inc. | Dense articles formed from tetrafluoroethylene core shell copolymers and methods of making the same |
| KR20190130135A (ko) * | 2017-04-11 | 2019-11-21 | 솔베이 스페셜티 폴리머스 이태리 에스.피.에이. | 플루오로중합체의 입자를 포함하는 수성 라텍스의 제조 방법 |
| CN110078855B (zh) * | 2019-04-22 | 2020-07-14 | 中昊晨光化工研究院有限公司 | 一种含氟聚合物及其制备方法 |
| CN116178598A (zh) * | 2022-06-20 | 2023-05-30 | 福建海德福新材料有限公司 | 一种四氟乙烯基聚合物树脂及其制备方法 |
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|---|---|---|---|---|
| US2567011A (en) | 1949-01-10 | 1951-09-04 | Minnesota Mining & Mfg | Fluorocarbon acids and derivatives |
| US2732398A (en) | 1953-01-29 | 1956-01-24 | cafiicfzsojk | |
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| JPS4928026B1 (de) * | 1965-01-12 | 1974-07-23 | ||
| GB1291936A (en) | 1970-11-19 | 1972-10-04 | Asahi Glass Co Ltd | Process for producing a copolymer of tetrafluoroethylene and propylene |
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| JPS497058B1 (de) | 1970-12-30 | 1974-02-18 | ||
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| US4000356A (en) | 1972-06-19 | 1976-12-28 | Dynamit Nobel Aktiengesellschaft | Process for the preparation of thermoplastically workable fluoro-olefin polymers |
| US4277586A (en) * | 1974-11-20 | 1981-07-07 | Asahi Glass Company, Ltd. | Process for preparing a propylene-tetrafluoroethylene copolymer |
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| US4029868A (en) | 1976-03-10 | 1977-06-14 | E. I. Du Pont De Nemours And Company | Tetrafluoroethylene terpolymers |
| JPS539848A (en) | 1976-07-16 | 1978-01-28 | Asahi Glass Co Ltd | Heat treatment of fluorine-containing elastomers |
| JPS53125491A (en) | 1977-04-08 | 1978-11-01 | Daikin Ind Ltd | Fluorine-containing polymer easily curable and its curable composition |
| JPS54132691A (en) * | 1978-04-06 | 1979-10-15 | Asahi Glass Co Ltd | Preparation of ethylene-tetrafluoroethylene copolymer |
| JPS5529519A (en) * | 1978-08-22 | 1980-03-01 | Asahi Glass Co Ltd | Preparation of fluorocopolymer |
| DE2903981A1 (de) | 1979-02-02 | 1980-08-07 | Hoechst Ag | Rueckgewinnung fluorierter emulgatorsaeuren aus basischen anionenaustauschern |
| US4233421A (en) | 1979-02-26 | 1980-11-11 | Minnesota Mining And Manufacturing Company | Fluoroelastomer composition containing sulfonium curing agents |
| US4463144A (en) | 1980-09-10 | 1984-07-31 | Asahi Glass Company Ltd. | Process for producing propylene-tetrafluoroethylene copolymer |
| DE3135598A1 (de) | 1981-09-09 | 1983-03-17 | Hoechst Ag, 6000 Frankfurt | "kontinuierliches verfahren zur agglomerierung von ptee-pulvern im fluessigen medium und damit gewonnenes modifiziertes ptee-pulver" |
| JPS5920310A (ja) | 1982-07-27 | 1984-02-02 | Daikin Ind Ltd | 含フッ素ポリマー硬化用組成物 |
| US5086123A (en) | 1984-02-27 | 1992-02-04 | Minnesota Mining And Manufacturing Company | Fluoroelastomer compositions containing fluoroaliphatic sulfonamides as curing agents |
| JPS60248710A (ja) * | 1984-05-22 | 1985-12-09 | Daikin Ind Ltd | 新規エチレン／テトラフルオロエチレン系共重合体 |
| DE3662142D1 (en) * | 1985-03-28 | 1989-03-30 | Daikin Ind Ltd | Novel fluorovinyl ether and copolymer comprising the same |
| IT1187684B (it) | 1985-07-08 | 1987-12-23 | Montefluos Spa | Procedimento per la preparazione di fluoroelastomeri vulcanizzabili e prodotti cosi' ottenuti |
| JPS62260807A (ja) | 1986-05-07 | 1987-11-13 | Nippon Mektron Ltd | 含フッ素重合体の製造方法 |
| IT1204903B (it) | 1986-06-26 | 1989-03-10 | Ausimont Spa | Processo di polimerizzazione in dispersione acquosa di monomeri florati |
| GB8728884D0 (en) * | 1987-12-10 | 1988-01-27 | Ici Plc | Aqueous-based fluoropolymer compositions |
| US4912171A (en) | 1988-04-01 | 1990-03-27 | Minnesota Mining And Manufacturing Company | Fluoroelastomer curing process with phosphonium compound |
| IT1235545B (it) | 1989-07-10 | 1992-09-09 | Ausimont Srl | Fluoroelastomeri dotati di migliore processabilita' e procedimento di preparazione |
| US5037921A (en) * | 1990-03-01 | 1991-08-06 | E. I. Du Pont De Nemours And Company | Base resistant fluoroelastomers with improved processibility and curability |
| US5453477A (en) * | 1992-05-01 | 1995-09-26 | Alliedsignal Inc. | Process of polymerizing chloroetrifluoroethylene with alkyl hydroperoxide and metal metabisulfite |
| US5262490A (en) | 1992-08-24 | 1993-11-16 | Minnesota Mining And Manufacturing Company | Fluoroelastomer composition with organo-onium compounds |
| US5285002A (en) | 1993-03-23 | 1994-02-08 | Minnesota Mining And Manufacturing Company | Fluorine-containing polymers and preparation and use thereof |
| IT1265461B1 (it) | 1993-12-29 | 1996-11-22 | Ausimont Spa | Fluoroelastomeri comprendenti unita' monomeriche derivanti da una bis-olefina |
| WO1996024622A1 (en) | 1995-02-10 | 1996-08-15 | Alliedsignal Inc. | Production of fluoropolymers, fluoropolymer suspension and polymer formed therefrom |
| JP3223776B2 (ja) | 1995-03-31 | 2001-10-29 | 日本メクトロン株式会社 | 含フッ素エラストマー組成物 |
| JP3082626B2 (ja) | 1995-07-19 | 2000-08-28 | 日本メクトロン株式会社 | 含フッ素エラストマー組成物 |
| JPH0977829A (ja) * | 1995-09-08 | 1997-03-25 | Toagosei Co Ltd | パーハロオレフィン共重合体及び該共重合体からなる架橋成形体の製造方法 |
| IT1276979B1 (it) | 1995-10-20 | 1997-11-03 | Ausimont Spa | Composizioni fluoroelastomeriche |
| US5955556A (en) * | 1995-11-06 | 1999-09-21 | Alliedsignal Inc. | Method of manufacturing fluoropolymers |
| US5591804A (en) | 1995-12-21 | 1997-01-07 | Minnesota Mining And Manufacturing Company | Fluorinated onium salts, curable compositions containing same, and method of curing using same |
| US5936060A (en) | 1996-11-25 | 1999-08-10 | E. I. Du Pont De Nemours And Company | Perfluoroelastomer composition having improved processability |
| US5677389A (en) | 1996-11-25 | 1997-10-14 | E. I. Du Pont De Nemours | Perfluoroelastomer composition having enhanced curing performance |
| US5728773A (en) | 1997-02-21 | 1998-03-17 | Minnesota Mining And Manufacturing Company | Fluoroelastomer composition with organo-onium and blocked-carbonate compounds |
| US6281296B1 (en) | 1998-08-10 | 2001-08-28 | Dupont Dow Elastomers L.L.C. | Curable perfluoroelastomer composition |
| WO2000022002A1 (fr) | 1998-10-13 | 2000-04-20 | Daikin Industries, Ltd. | Procede de production de fluoropolymeres |
| DE69940558D1 (en) | 1998-11-30 | 2009-04-23 | Du Pont | Fluoromonomerpolymerisation |
| DE19857111A1 (de) | 1998-12-11 | 2000-06-15 | Dyneon Gmbh | Wäßrige Dispersionen von Fluorpolymeren |
| JP5092184B2 (ja) * | 1999-02-15 | 2012-12-05 | ダイキン工業株式会社 | フルオロポリマーの製造法 |
| US6429258B1 (en) * | 1999-05-20 | 2002-08-06 | E. I. Du Pont De Nemours & Company | Polymerization of fluoromonomers |
| JP4352546B2 (ja) | 1999-12-22 | 2009-10-28 | ユニマテック株式会社 | フルオロエラストマー、その製造方法、架橋性組成物およびその硬化物 |
| EP1392744B1 (de) * | 2001-05-02 | 2008-07-09 | 3M Innovative Properties Company | Emulgatorfreies wässriges emulsionspolymerisationsverfahren zur herstellung von fluorpolymeren |
| BR0212308A (pt) * | 2001-09-05 | 2004-10-13 | 3M Innovative Properties Co | Dispersão de fluoropolìmero, e, método para prover uma dispersão de partìculas de fluoropolìmero |
| EP1364972B1 (de) | 2002-05-22 | 2006-08-30 | 3M Innovative Properties Company | Prozess zur Reduzierung des Gehaltes an fluorierten Emulgatoren in wässrigen Fluorpolymer-Dispersionen |
| WO2004041878A1 (en) * | 2002-10-31 | 2004-05-21 | 3M Innovative Properties Company | Emulsifier free aqueous emulsion polymerization to produce copolymers of a fluorinated olefin and hydrocarbon olefin |
-
2003
- 2003-10-21 WO PCT/US2003/033233 patent/WO2004041878A1/en active Application Filing
- 2003-10-21 EP EP03768534A patent/EP1556426B1/de not_active Expired - Lifetime
- 2003-10-21 DE DE60327452T patent/DE60327452D1/de not_active Expired - Fee Related
- 2003-10-21 RU RU2005111865/04A patent/RU2342403C2/ru not_active IP Right Cessation
- 2003-10-21 US US10/690,088 patent/US7064170B2/en not_active Expired - Fee Related
- 2003-10-21 AU AU2003291646A patent/AU2003291646A1/en not_active Abandoned
- 2003-10-21 AT AT03768534T patent/ATE430169T1/de not_active IP Right Cessation
- 2003-10-21 CN CNB2003801022455A patent/CN100354324C/zh not_active Expired - Fee Related
- 2003-10-21 JP JP2004550055A patent/JP2006504844A/ja active Pending
-
2005
- 2005-05-30 ZA ZA200504411A patent/ZA200504411B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US20040087703A1 (en) | 2004-05-06 |
| RU2005111865A (ru) | 2005-10-27 |
| CN1708519A (zh) | 2005-12-14 |
| WO2004041878A1 (en) | 2004-05-21 |
| EP1556426A1 (de) | 2005-07-27 |
| ZA200504411B (en) | 2006-02-22 |
| DE60327452D1 (de) | 2009-06-10 |
| CN100354324C (zh) | 2007-12-12 |
| US7064170B2 (en) | 2006-06-20 |
| RU2342403C2 (ru) | 2008-12-27 |
| AU2003291646A1 (en) | 2004-06-07 |
| EP1556426B1 (de) | 2009-04-29 |
| JP2006504844A (ja) | 2006-02-09 |
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