ATE13355T1 - Vorrichtung zum verdampfen von proben, die in eine gaschromatographische kolonne injiziert wurden. - Google Patents

Vorrichtung zum verdampfen von proben, die in eine gaschromatographische kolonne injiziert wurden.

Info

Publication number
ATE13355T1
ATE13355T1 AT81108799T AT81108799T ATE13355T1 AT E13355 T1 ATE13355 T1 AT E13355T1 AT 81108799 T AT81108799 T AT 81108799T AT 81108799 T AT81108799 T AT 81108799T AT E13355 T1 ATE13355 T1 AT E13355T1
Authority
AT
Austria
Prior art keywords
column
oven
injection
gas chromatographic
vaporization
Prior art date
Application number
AT81108799T
Other languages
English (en)
Inventor
Giorgio Sisti
Mario Galli
Sorin Trestianu
Original Assignee
Erba Strumentazione
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=11217819&utm_source=***_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ATE13355(T1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Erba Strumentazione filed Critical Erba Strumentazione
Application granted granted Critical
Publication of ATE13355T1 publication Critical patent/ATE13355T1/de

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/30Control of physical parameters of the fluid carrier of temperature
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • G01N2030/121Preparation by evaporation cooling; cold traps
    • G01N2030/122Preparation by evaporation cooling; cold traps cryogenic focusing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/16Injection
    • G01N2030/165Injection retention gaps
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/16Injection
    • G01N2030/167Injection on-column injection
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/30Control of physical parameters of the fluid carrier of temperature
    • G01N2030/3046Control of physical parameters of the fluid carrier of temperature temperature control of column inlet
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/38Flow patterns
    • G01N2030/382Flow patterns flow switching in a single column
    • G01N2030/383Flow patterns flow switching in a single column by using auxiliary fluid
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/10Preparation using a splitter

Landscapes

  • Immunology (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
AT81108799T 1980-11-06 1981-10-23 Vorrichtung zum verdampfen von proben, die in eine gaschromatographische kolonne injiziert wurden. ATE13355T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IT25818/80A IT1134198B (it) 1980-11-06 1980-11-06 Dispositivo per l'iniezione a vaporizzazione in una colonna gas-cromatografica
EP81108799A EP0051778B1 (de) 1980-11-06 1981-10-23 Vorrichtung zum Verdampfen von Proben, die in eine gaschromatographische Kolonne injiziert wurden

Publications (1)

Publication Number Publication Date
ATE13355T1 true ATE13355T1 (de) 1985-06-15

Family

ID=11217819

Family Applications (1)

Application Number Title Priority Date Filing Date
AT81108799T ATE13355T1 (de) 1980-11-06 1981-10-23 Vorrichtung zum verdampfen von proben, die in eine gaschromatographische kolonne injiziert wurden.

Country Status (6)

Country Link
US (1) US4383839A (de)
EP (1) EP0051778B1 (de)
JP (1) JPS57108660A (de)
AT (1) ATE13355T1 (de)
DE (1) DE3170534D1 (de)
IT (1) IT1134198B (de)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0048917B1 (de) * 1980-09-30 1985-12-27 CARLO ERBA STRUMENTAZIONE S.p.A. Verfahren und Vorrichtung zur Eingabe kleiner Flüssigkeitsproben, hinsichtlich ihres Volumens kontrollier- und reproduzierbar, in chromatographische Analysensysteme
US4440550A (en) * 1983-06-28 1984-04-03 J & W Scientific, Inc. On-column injector
DE3475569D1 (en) * 1983-09-09 1989-01-12 Erba Strumentazione Multi-purpose on column injector
US4477266A (en) * 1983-09-15 1984-10-16 Varian Associates, Inc. Solute focusing technique for on-column injection in capillary gas chromatography
US4869876A (en) * 1984-04-30 1989-09-26 International Business Machines Corp. Multi-purpose plural-oven gas chromatography system with shared controls
US5522988A (en) * 1985-01-25 1996-06-04 The Dow Chemical Company On-line coupled liquid and gas chromatography system with an interface capillary tube interposed between a pair of capillary chromatographic columns
US5236593A (en) * 1985-01-25 1993-08-17 The Dow Chemical Company On-line coupled liquid and gas chromatography system with an interface capillary tube interposed between a pair of capillary chromatographic columns
JPH0695089B2 (ja) * 1985-01-25 1994-11-24 ザ ダウ ケミカル カンパニ− 液体クロマトグラフ装置から気体クロマトグラフ装置へ試料をリテンションギャップを用いて中断なしに送ることを含むクロマトグラフ分析法
US4935145A (en) * 1985-01-25 1990-06-19 The Dow Chemical Company On-line coupled liquid and gas chromatography system
IT1184320B (it) * 1985-02-21 1987-10-28 Erba Strumentazione Procedimento e dispositivo per l'iniezione diretta in colonna di campioni contenenti composti alto bollenti e/o mediovolatili
FR2599152B1 (fr) * 1986-05-22 1989-07-28 Flopetrol Procede et appareil d'analyse chromatographique, en particulier pour liquides petroliers
US5083450A (en) * 1990-05-18 1992-01-28 Martin Marietta Energy Systems, Inc. Gas chromatograph-mass spectrometer (gc/ms) system for quantitative analysis of reactive chemical compounds
DE69023513T2 (de) * 1990-12-04 1996-04-04 Dow Chemical Co Gaschromatographieverfahren und -vorrichtung.
US5135549A (en) * 1991-01-30 1992-08-04 The Board Of Trustees Of Southern Illinois University Chromatographic technique and apparatus
US6058789A (en) * 1994-03-26 2000-05-09 Kohsaka; Hiroji Sampling device for gas analyzers
JPH07260644A (ja) * 1994-03-26 1995-10-13 Horiba Ltd ガス分析におけるサンプリング装置
WO1996000388A2 (en) * 1994-06-24 1996-01-04 Universite De Montreal Selective removal of volatile substances injected into a chromatographic packing filled column
DE9421595U1 (de) * 1994-12-10 1996-04-11 Hewlett-Packard GmbH, 71034 Böblingen Flüssigkeitschromatographiesystem zur Thermostatisierung einer Vorsäule und einer Trennsäule eines Flüssigkeitschromatographiesystems
IT1275526B (it) * 1995-07-14 1997-08-07 Fisons Instr Spa Procedimento e dispositivo per l'iniezione di volumi elevati di campioni liquidi in un gascromatografo
US5760291A (en) * 1996-09-03 1998-06-02 Hewlett-Packard Co. Method and apparatus for mixing column effluent and make-up gas in an electron capture detector
US6131440A (en) 1996-10-15 2000-10-17 Universite De Montreal Selective removal of volatile substances injected into a chromatographic packing filled column
US5846292A (en) * 1997-05-06 1998-12-08 Board Of Supervisors At Louisiana State University & Agricultural & Mechanical College Chromatograph with column extraction
ES2369636T3 (es) 2000-01-12 2011-12-02 Zoex Licensing Corporation Modulación térmica transversal.
IT1318194B1 (it) 2000-07-19 2003-07-28 Thermoquest Italia Spa Metodo e dispositivo per l'iniezione a vaporizzazione
DE10133774B4 (de) * 2001-07-16 2012-03-22 Joint Analytical Systems Gmbh Verdampferrohr zum Verdampfen von flüssigen Proben für die Kapillar-Gaschromatographie
ITMI20030332A1 (it) * 2003-02-25 2004-08-26 Mega S N C Di Barbieri Edda Metodo ed iniettore per l'iniezione diretta in colonna per gascromatografia e splittaggio in fase liquida.
US7520920B1 (en) * 2005-03-04 2009-04-21 Griffin Analytical Technologies Guard columns for gas chromatographs and gas chromatograph-mass spectrometers
US8506688B2 (en) * 2008-01-18 2013-08-13 Restek Corporation Gas chromatographic device
US7867325B2 (en) * 2008-01-18 2011-01-11 Restek Corporation Gas chromatographic device

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2841005A (en) * 1956-12-11 1958-07-01 Gulf Oil Corp Chromatographic method and apparatus
US3225521A (en) * 1962-06-04 1965-12-28 Gulf Research Development Co Serially connected thermochromatographic columns
US3225520A (en) * 1962-06-04 1965-12-28 Gulf Research Development Co Sample preparation and collection means for gas chromatographic columns
US3263493A (en) * 1964-04-13 1966-08-02 Exxon Research Engineering Co Gas chromatograph moisture analyzer
US3518059A (en) * 1967-05-31 1970-06-30 Hewlett Packard Co Method and apparatus for determining chemical structure
US3592064A (en) * 1969-02-18 1971-07-13 Bryggeriindustriens Forsknings Method for transferring a sample to be analyzed into the column of a gas chromatograph, and system for carrying out the method
US3841059A (en) * 1972-09-25 1974-10-15 W Mccabe Compressed and thermostated air regulated gas liquid chromatography oven with simultaneously operated multiple chromatography columns
JPS5183596A (ja) * 1975-01-20 1976-07-22 Hitachi Ltd Ryurokirikaesochi
US4007626A (en) * 1975-04-18 1977-02-15 Phillips Petroleum Company Chromatographic analysis
DE2823445A1 (de) * 1978-05-29 1979-12-06 Inst Chromatographie System zur elektronischen oder elektromechanischen polaritaetsoptimierung in der gas-chromatographie
GB2030055B (en) * 1978-09-26 1983-01-12 Erba Strumentazione Sample injection into gas chromatorgraphic columns

Also Published As

Publication number Publication date
DE3170534D1 (en) 1985-06-20
IT1134198B (it) 1986-07-31
US4383839A (en) 1983-05-17
EP0051778A2 (de) 1982-05-19
EP0051778B1 (de) 1985-05-15
JPS57108660A (en) 1982-07-06
EP0051778A3 (en) 1982-07-21
IT8025818A0 (it) 1980-11-06

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Legal Events

Date Code Title Description
UEP Publication of translation of european patent specification
REN Ceased due to non-payment of the annual fee