WO2021085221A1 - 高炉操業方法 - Google Patents
高炉操業方法 Download PDFInfo
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- WO2021085221A1 WO2021085221A1 PCT/JP2020/039288 JP2020039288W WO2021085221A1 WO 2021085221 A1 WO2021085221 A1 WO 2021085221A1 JP 2020039288 W JP2020039288 W JP 2020039288W WO 2021085221 A1 WO2021085221 A1 WO 2021085221A1
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- Prior art keywords
- coke
- amount
- ratio
- blast furnace
- threshold value
- Prior art date
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- 238000000034 method Methods 0.000 title claims abstract description 35
- 239000000571 coke Substances 0.000 claims abstract description 228
- 239000000843 powder Substances 0.000 claims abstract description 76
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 84
- 239000002245 particle Substances 0.000 claims description 74
- 230000008859 change Effects 0.000 claims description 59
- 238000011017 operating method Methods 0.000 claims description 14
- 238000007664 blowing Methods 0.000 claims 1
- 238000005259 measurement Methods 0.000 abstract description 2
- 230000035699 permeability Effects 0.000 description 29
- 230000007423 decrease Effects 0.000 description 20
- 239000002994 raw material Substances 0.000 description 20
- 238000009423 ventilation Methods 0.000 description 13
- 238000003384 imaging method Methods 0.000 description 10
- 230000006866 deterioration Effects 0.000 description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 6
- 230000009467 reduction Effects 0.000 description 6
- 230000004044 response Effects 0.000 description 5
- 229910000805 Pig iron Inorganic materials 0.000 description 4
- 238000005273 aeration Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000007873 sieving Methods 0.000 description 4
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 230000006641 stabilisation Effects 0.000 description 3
- 238000011105 stabilization Methods 0.000 description 3
- 238000012935 Averaging Methods 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B7/00—Blast furnaces
- C21B7/007—Controlling or regulating of the top pressure
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
- C21B5/001—Injecting additional fuel or reducing agents
- C21B5/003—Injection of pulverulent coal
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
- C21B5/007—Conditions of the cokes or characterised by the cokes used
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
- C21B5/008—Composition or distribution of the charge
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B7/00—Blast furnaces
- C21B7/16—Tuyéres
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B7/00—Blast furnaces
- C21B7/24—Test rods or other checking devices
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/02—Investigating particle size or size distribution
- G01N15/0205—Investigating particle size or size distribution by optical means
- G01N15/0227—Investigating particle size or size distribution by optical means using imaging; using holography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/10—Investigating individual particles
- G01N15/14—Optical investigation techniques, e.g. flow cytometry
- G01N15/1429—Signal processing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/10—Investigating individual particles
- G01N15/14—Optical investigation techniques, e.g. flow cytometry
- G01N15/1429—Signal processing
- G01N15/1433—Signal processing using image recognition
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/10—Investigating individual particles
- G01N15/14—Optical investigation techniques, e.g. flow cytometry
- G01N15/1456—Optical investigation techniques, e.g. flow cytometry without spatial resolution of the texture or inner structure of the particle, e.g. processing of pulse signals
- G01N15/1459—Optical investigation techniques, e.g. flow cytometry without spatial resolution of the texture or inner structure of the particle, e.g. processing of pulse signals the analysis being performed on a sample stream
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B2300/00—Process aspects
- C21B2300/04—Modeling of the process, e.g. for control purposes; CII
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/10—Investigating individual particles
- G01N15/14—Optical investigation techniques, e.g. flow cytometry
- G01N2015/1493—Particle size
Definitions
- the present invention relates to a blast furnace operating method in which the amount of air blown from the tuyere at the bottom of the furnace is controlled in response to a change in the powder ratio of coke charged into the blast furnace.
- iron raw materials mainly composed of iron oxide and coke are alternately charged from the top of the furnace, and the coke is burned by the hot air blown from the tuyere at the bottom of the furnace and burned with the reducing gas containing CO generated.
- Pig iron is produced by reducing iron oxide in coke and lump ore.
- the air permeability of the blast furnace greatly affects the stable operation of the blast furnace.
- the air permeability in the furnace deteriorates, and the operation of the blast furnace becomes unstable.
- the raw materials charged into the blast furnace are generally adjusted in particle size to 25 to 35 mm or more for coke and 5 to 25 mm or more for sinter and iron ore by sieving before charging into the blast furnace. is there.
- the blast furnace can be operated according to the amount of the powder.
- Patent Document 1 and Patent Document 2 disclose a powder ratio measuring device capable of measuring the powder ratio of powder adhering to coke conveyed on a conveyor.
- the powder ratio measuring apparatus disclosed in Patent Document 1 and Patent Document 2 the relationship between the powder ratio of the powder adhering to the coke and the average brightness in the image data obtained by imaging the coke is grasped in advance.
- the powder ratio of the powder adhering to the coke is measured online using the average brightness of the image data obtained by imaging the coke that is transported to the blast furnace on the conveyor.
- Patent Document 3 discloses a powder ratio estimation method for estimating the powder ratio of the blast furnace raw material from the raw material deposition angle of the blast furnace top bunker.
- the powder ratio of the blast furnace raw material is estimated by using the raw material deposition angle of the furnace top bunker and the correlation between the raw material deposition angle and the powder ratio.
- Patent Document 1 discloses only a powder ratio measuring device and a powder ratio measuring system capable of measuring the powder ratio of coke breeze charged into a blast furnace, and a specific operation of the blast furnace using the powder ratio. The method is not described.
- Patent Document 2 discloses an apparatus for measuring the porosity of a blast furnace using the powder ratio, but does not describe a method for operating the blast furnace.
- Patent Document 3 What is disclosed in Patent Document 3 is a method of estimating the powder ratio of the blast furnace raw material from the raw material deposition angle of the blast furnace top bunker and setting a specific threshold value for the powder ratio to operate the blast furnace.
- management with a specific threshold value cannot prevent the deterioration of the blast furnace condition caused by the fluctuation of the powder ratio.
- the present invention measures the particle size distribution of coke charged into the blast furnace, and uses the index obtained from the measured particle size distribution to blow air from the tuyere and coke. It is an object of the present invention to provide a blast furnace operation method capable of stabilizing blast furnace operation by adjusting at least one of the ratios.
- the means for solving the above problems are as follows. (1) A blast furnace operating method in which air is blown from a tuyere provided at the bottom of the furnace to operate the blast furnace. The particle size distribution of coke transported to the blast furnace is sequentially measured, and according to an index obtained from the particle size distribution. A method of operating a blast furnace that adjusts at least one of the air volume and the coke ratio. (2) When the amount of air blown is adjusted, a first threshold value is set in advance with respect to the amount of change of the index over a certain period of time, and when the first threshold value is a positive value, the index is described.
- the amount of change in a certain time is equal to or greater than a preset first threshold value
- the amount of air blown is reduced, and when the first threshold value is a negative value, the amount of change in the index in a certain time.
- the blast furnace operating method according to (1) wherein the amount of air blown is reduced when is equal to or less than a preset first threshold value.
- a second threshold value is set in advance with respect to the amount of change of the index over a certain period of time, and when the second threshold value is a positive value, the index is used.
- the coke ratio When the amount of change in a certain period of time is equal to or greater than a preset second threshold value, the coke ratio is increased, and when the second threshold value is a negative value, the amount of change in the index in a certain period of time is increased.
- a first threshold value and a second threshold value having an absolute value larger than the absolute value of the first threshold value are set in advance with respect to the amount of change of the index over a certain period of time, and the first threshold value and the first threshold value are set.
- the second threshold value is a positive value
- the amount of air blown is reduced when the amount of change of the index in a certain time is equal to or more than the first threshold value and less than the second threshold value, and the index is used.
- the amount of change in a certain period of time is equal to or greater than the second threshold value
- the coke ratio is increased
- the first threshold value and the second threshold value are negative values
- the index is used for a certain period of time.
- the amount of change in the index is equal to or less than the first threshold value and larger than the second threshold value
- the amount of air blown is reduced, and when the amount of change in the index in a certain period of time becomes equal to or less than the second threshold value.
- At least one of the air volume from the tuyere and the coke ratio can be adjusted according to the index obtained from the particle size distribution.
- the turbulence of the gas flow in the furnace can be reduced, and the pressure balance in the furnace can be suppressed from being greatly disturbed.
- Stabilization of blast furnace operation can be realized by suppressing the pressure balance in the furnace from being greatly disturbed in this way.
- FIG. 1 is a schematic view showing an example of the configuration of the particle size distribution measuring device 10 and its surroundings.
- FIG. 2 is a graph showing the relationship between the average brightness and the powder ratio of lump coke having a particle size of 35 mm or more to which coke powder is attached.
- FIG. 3 is a graph showing the relationship between the change in the coke powder ratio and the in-core aeration index in 4 hours.
- FIG. 4 is a graph showing the relationship between the amount of change in porosity and the air permeability index in 4 hours.
- FIG. 5 is a graph showing an example of fluctuations in the coke powder ratio.
- FIG. 1 is a schematic view showing an example of the configuration of the particle size distribution measuring device 10 and its surroundings.
- FIG. 2 is a graph showing the relationship between the average brightness and the powder ratio of lump coke having a particle size of 35 mm or more to which coke powder is attached.
- FIG. 3 is a graph showing the relationship between the change in the coke powder ratio and the in-core
- FIG. 6 is a graph showing an example of fluctuations in the coke powder ratio (a), the amount of air blown from the tuyere (b), and the upper pressure loss (c) of the blast furnace.
- FIG. 7 is a graph showing the relationship between the coke ratio and the upper pressure loss.
- FIG. 8 is a graph showing the relationship between the coke ratio and the upper pressure loss.
- FIG. 1 is a schematic view showing an example of the configuration of the particle size distribution measuring device 10 and its surroundings.
- the particle size distribution measuring device 10 will be described with reference to FIG. 1, but the particle size distribution measuring device 10 is not limited to the particle size distribution measuring device 10 shown in FIG. Good.
- the particle size distribution measuring device 10 includes an imaging device 12, a lighting device 14, and an arithmetic unit 16.
- the coke 20 charged in the blast furnace is stored in the hopper 22.
- the coke 20 discharged from the hopper 22 is sieved by a sieve 24 to remove powder having a particle size smaller than the opening of the sieve 24, and then conveyed to the blast furnace 30 by a conveyor 26.
- the mesh size of the sieve 24 is 35 mm. Therefore, the coke 20 conveyed by the conveyor 26 includes coke having a particle size of 35 mm or more and coke powder adhering to the coke that does not fall even when sieved using a sieve 24.
- the particle size of the coke powder adhering to the lump coke was measured, it was a coke powder having a particle size of 5 mm or less.
- the coke powder having a particle size of 5 mm or less means coke powder that passes through a sieve having a mesh size of 5 mm.
- the image pickup device 12 is provided above the conveyor 26 and images the coke 20 conveyed by the conveyor 26 to create image data.
- the image pickup device 12 is, for example, a digital camera having a CCD or CMOS type image pickup sensor and a lens.
- the height at which the image pickup device 12 is provided is preferably 500 mm or more and 1000 mm or less on the conveyor 26, but the size and lens of the image pickup sensor included in the image pickup device 12 so that the entire width of the transported coke can be imaged.
- the height at which the image pickup apparatus 12 is provided may be adjusted according to the angle of view of.
- the image pickup device 12 receives light including reflected light from the surface of the coke 20 by the image pickup sensor and creates image data.
- the coke powder adhering to the surface of the coke 20 affects the reflected light reflected from the surface of the coke 20. Therefore, the image data created by receiving the light including the reflected light reflected from the surface of the coke 20 includes information on the coke powder adhering to the surface of the coke 20.
- the image data created by the image pickup device 12 is output to the arithmetic unit 16 having a calculation unit and a conversion unit (not shown).
- the arithmetic unit 16 processes the image data output from the image pickup device 12.
- the calculation unit of the arithmetic unit 16 calculates the feature amount including the information on the coke powder from the image data.
- the calculation unit calculates the average luminance by arithmetically averaging the luminance (0 to 255) of each pixel in the image data, for example.
- FIG. 2 is a graph showing the relationship between the average brightness and the powder ratio of lump coke having a particle size of 35 mm or more to which coke powder is attached.
- the vertical axis of FIG. 2 is an actually measured value of the powder ratio (mass%) of the coke powder adhering to the coke blob.
- the horizontal axis is the average brightness of the image data obtained by imaging the lump coke to which the coke powder is attached.
- Massive coke having a particle size of 35 mm or more was prepared by sieving the coke using a sieve having a mesh size of 35 mm.
- the powder ratio of the coke powder adhering to the surface of the coke coke is determined by drying the coke coke at 120 to 200 ° C.
- the average brightness calculated by the calculation unit is converted into the powder ratio of the adhered powder by the conversion unit.
- a regression equation showing the correspondence between the powder ratio of the coke powder adhering to the coke surface and the average brightness shown in FIG. 2 is stored in advance in the conversion unit, and the conversion unit uses the regression equation to calculate.
- the average brightness calculated by is converted into the powder ratio of the coke powder adhering to the surface of the coke 20.
- the image pickup device 12 captures the coke 20 again and creates image data after a predetermined time has elapsed.
- the predetermined time may be determined, for example, by the imaging range of the coke 20 imaged by the imaging device 12 and the transport speed of the conveyor 26. That is, the predetermined time may be set as the time calculated by dividing the length of the imaging range in the transport direction of the conveyor 26 by the transport speed of the conveyor 26.
- the image pickup apparatus 12 can image the coke 20 without a gap in the transport direction of the conveyor 26.
- the image pickup apparatus 12 preferably images the coke 20 from a direction perpendicular to the transport direction of the conveyor 26.
- the image data created by the imaging device 12 is output to the arithmetic unit 16 again, and the arithmetic unit 16 calculates the powder ratio of the coke powder adhering to the coke 20.
- the particle size distribution measuring device 10 repeatedly executes the above process to obtain a powder ratio of coke powder adhering to the surface of the coke 20 conveyed by the conveyor 26, that is, coke powder having a particle size of 5 mm or less.
- the powder ratio (hereinafter, may be referred to as "coke powder ratio”) can be measured online, and the powder ratio of coke powder having a particle size of 5 mm or less of coke charged into the blast furnace 30 can be grasped by the measurement. it can.
- the powder ratio of coke powder having a particle size of 5 mm or less indicates the mass ratio of coke powder having a particle size of 5 mm or less to the total mass of coke, which is a particle size of coke having a particle size of 5 mm or less and a particle size of more than 5 mm. It can be said that the particle size distribution is. That is, the powder ratio of the coke powder having a particle size of 5 mm or less according to the present embodiment is an example of an index obtained from the particle size distribution of coke.
- coke 20 and iron raw materials such as sintered ore are alternately charged from the top of the furnace, and hot air is blown from the tuyere at the bottom of the furnace to burn the coke 20 with the reducing gas containing CO generated.
- Pig iron is produced by reducing iron oxide.
- the powder ratio of the coke 20 charged into the blast furnace 30 becomes high, the coke powder enters the gaps between the cokes, the porosity decreases, and the air permeability in the furnace deteriorates.
- the air permeability in the furnace deteriorates, the gas flow in the furnace is disturbed, the pressure balance in the furnace is disturbed, and the operation of the blast furnace becomes unstable.
- FIG. 3 is a graph showing the relationship between the change in coke powder ratio and the in-core aeration index over 4 hours.
- the horizontal axis of FIG. 3 is the amount of change (mass%) in the coke powder ratio having a particle size of 5 mm or less in 4 hours.
- "-0.5" in the horizontal axis means that the coke powder ratio is 0 in 4 hours. It shows a decrease of 5.5% by mass. That is, the amount of change in the powder ratio on the horizontal axis is a value obtained by subtracting the powder ratio of coke 4 hours ago from the current coke powder ratio.
- the current coke powder rate is the powder rate of each charge of coke charged into the blast furnace in the last hour, and the average value is taken as the average value of the charges, and the average value of each charge in the last hour is used. It is a further averaged value.
- the average value of the powder ratio of the past 4 charges of coke may be used as the current coke powder ratio, and these moving average values may be used as the current coke. It may be the powder ratio of.
- the amount of change in the coke rate on the horizontal axis is a value obtained by performing this operation every hour and subtracting the coke powder rate 4 hours ago from the current coke powder rate.
- the vertical axis in FIG. 3 is the current in-core ventilation index, and a large in-core ventilation index indicates that there is a large variation in the air permeability in the furnace in the circumferential direction.
- the in-furnace ventilation index is an index that evaluates the variation in gas flow in the blast furnace from the variation in temperature in the circumferential direction in the blast furnace.
- the height is about 5 m below the stock line of the blast furnace. It is a numerical value measured as a standard deviation value of the value measured by the temperature of the gas in the peripheral part of the blast furnace with seven thermometers installed at equal intervals in the circumferential direction of the blast furnace.
- the in-furnace ventilation index 120 is a value used as a control value for air permeability in blast furnace operation, and when the in-furnace ventilation index exceeds 120, the pressure balance in the furnace is lost and the blast furnace operation becomes unstable. Therefore, it is necessary to control the in-core ventilation index to be 120 or less.
- the plot in FIG. 3 shows the measured values of the in-core ventilation index when the in-core ventilation index was 120 or less 4 hours ago and the blast furnace operating conditions were not changed in the subsequent 4 hours.
- the coke powder ratio increases by 0.5% by mass or more in 4 hours, it is highly possible that the in-core aeration index exceeds 120. Therefore, in the blast furnace operation method according to the present embodiment, when the average value of the coke powder rate charged into the blast furnace for 1 hour increases by 0.5% by mass or more within 4 hours, air is blown from the tuyere. The amount of hot air blown is reduced by, for example, 5% or more.
- the turbulence of the gas flow in the furnace can be reduced by reducing the amount of air blown from the tuyere, and the pressure in the furnace can be reduced. It is possible to prevent the balance from being greatly lost.
- the coke powder ratio may always exceed the threshold value, so it is necessary to change the threshold value according to the conditions of the raw materials charged into the blast furnace. For this reason, it is difficult to prevent the pressure balance in the furnace from being significantly disturbed by controlling the powder ratio with a specific threshold value.
- powder that represents changes in the powder ratio of coke powder rather than being controlled by a specific powder ratio threshold. It can be said that it is preferable to manage by the amount of change in the rate.
- the increase in the coke powder ratio within 4 hours of 0.5% by mass is an example of the first threshold value of the predetermined change amount in a certain time.
- the decrease in the amount of air blown from the tuyere is an example of adjusting the amount of air blown from the tuyere.
- the amount of air blown may be reduced in a plurality of times. When the amount of air blown is reduced in a plurality of times, the total amount of the amount of air blown reduced within 1 hour may be 5% or more. If the total reduction in the amount of air blown within 1 hour is less than 5%, the effect of reducing the turbulence of the gas flow in the furnace cannot be obtained.
- the total decrease in the amount of air blown within 1 hour is preferably 5% or more and 15% or less, and more preferably 5% or more and 10% or less.
- the air is blown from the tuyere. It is preferable to further reduce the air volume by 5% or more. As a result, even if the air permeability in the furnace is further deteriorated by further increasing the amount of coke powder having a particle size of 5 mm or less, the turbulence of the gas flow in the furnace can be reduced by reducing the amount of air blown from the tuyere. It is possible to further prevent the pressure balance in the furnace from being greatly disturbed.
- the blast furnace operation method In response to the deterioration of air permeability in the furnace, increase the amount of coke that functions as a spacer in the furnace, or reduce the amount of iron ore raw material charged to the amount of coke charged to increase the coke ratio of the raw material. It is common to correspond. However, increasing the coke ratio increases CO 2 emissions and reduces pig iron production.
- the particle size distribution of coke transported to the blast furnace 30 is sequentially measured, and the air volume is adjusted according to the index obtained from the particle size distribution.
- the coke ratio means the amount of coke (kg) used to produce 1 ton of hot metal, and its unit is kg / t-pig.
- the average value of the coke powder ratio for 1 hour increases by 1.0% by mass or more within 4 hours when the air volume is reduced by 5% or more as described above, in addition to the decrease in the air volume. It is preferable to increase the coke ratio of the raw material. Specifically, the coke ratio is increased by 20 kg / t-pig or more within a range in which the reducing agent ratio does not exceed 600 kg / t-pig (the amount of reducing agent (kg) used to produce 1 ton of hot metal).
- the coke ratio is 360 kg / t-pig or less while pulverized coal is blown in at 50 to 200 kg / t-pig
- the coke ratio is increased to 380 kg / t-pig and the coke ratio is 360 kg / t. If it is larger than -pig and less than 400 kg / t-pig, the coke ratio is increased to 400 kg / t-pig. If the coke ratio is already 400 kg / t-pig or more, the coke ratio is not increased any more.
- the increase in the coke powder rate within 4 hours is 0.5% by mass, which is the absolute value of this value.
- Two thresholds of 1.0% by mass of an increase in the coke powder ratio, which is an absolute value larger than that of the coke, are set in advance.
- the increase in the coke powder ratio within 4 hours is 0.5% by mass or more and less than 1.0% by mass, the amount of air blown from the tuyere is reduced without changing the coke ratio.
- the amount of increase in the coke powder ratio within 4 hours is 1.0% by mass or more, the coke ratio is increased without changing the amount of air blown.
- the pressure balance in the furnace Can be prevented from collapsing significantly.
- the increase in the coke powder ratio within 4 hours of 1.0% by mass is an example of the second threshold value of the preset amount of change in a certain period of time.
- increasing the coke ratio is an example of adjusting the coke ratio.
- the response to the increase in the coke powder ratio is explained by increasing the coke ratio as the amount of air blown from the tuyere decreases. It may be dealt with only by increasing the ratio.
- the blast furnace operation method in the blast furnace operation method according to the present embodiment, at least one of the air volume and the coke ratio is adjusted according to the index calculated from the particle size distribution.
- the turbulence of the gas flow in the furnace can be reduced, the pressure balance in the furnace can be suppressed from being greatly disturbed, and the operation of the blast furnace can be stabilized.
- the control of the air volume using the particle size distribution measuring device 10 may be stopped.
- the total reduction in air volume is 15% or more, or the air volume ratio is 1.2 or less, another problem occurs, not due to the deterioration of air permeability due to coke powder with a particle size of 5 mm or less. It is highly possible that you are doing it. Therefore, controlling the amount of air blown by using the particle size distribution measuring device 10 may rather worsen the furnace condition.
- the average value of the coke powder ratio for 1 hour is lower than when the amount of air blown is reduced. Is preferably returned to the amount of air blown before reducing the amount of air blown from the tuyere.
- the amount of air blown from the tuyere is reduced by 5%
- the amount of air blown from the tuyere is increased by 5%
- the amount of air blown from the tuyere is reduced by 10% (decrease of 5%). It is preferable to increase the amount of air blown from the tuyere by 10% to return the amount of air blown to the original amount.
- the gas flow in the furnace stabilizes. Therefore, if the average value of the coke powder ratio for 1 hour does not increase after 4 hours have passed since the amount of air blown from the tuyere was reduced, and the average value of the powder ratio decreases, the coke powder ratio is reduced. It is preferable to return to the amount of air blown before the amount of air blown was reduced. By returning the amount of air from the tuyere to the original amount after 4 hours have passed since the amount of air was reduced, the amount of air from the tuyere is returned to the original amount without significantly disturbing the pressure balance in the furnace. be able to.
- the average value of the coke powder ratio for 1 hour is the coke ratio. If the powder ratio does not increase more than the powder ratio at the time of increasing, and the average value of the powder ratio decreases, the coke ratio before increasing the coke ratio may be restored. In this way, by returning the coke ratio to the original value after 4 hours have passed since the coke ratio was increased, the coke ratio can be returned to the original coke ratio without significantly disturbing the pressure balance in the furnace.
- the present invention is not limited to this.
- the porosity of the coke-filled layer in the blast furnace (hereinafter, referred to as “coke porosity”) may be used as an index obtained from the particle size distribution.
- the porosity of coke is determined by the particle size distribution of fine coke particles charged into the blast furnace measured by the particle size distribution measuring device 10 and, for example, the particle size distribution of coarse coke particles measured sequentially by a laser distance meter. It can be calculated using the models of Sato and Taguchi described in Patent Document 1. According to the above model, the porosity ⁇ can be calculated by the following mathematical formula (1).
- D P is the harmonic mean particle size
- I SP is following equation (2)
- Equation (3) is a value defined by the equation (4).
- Di is the center diameter of each particle size
- Wi is the mass ratio under the sieve of each particle size.
- the I P defined by Equation (3) is a quantity indicating the variance of particle size distribution
- I S defined by Equation (22) is a quantity indicating the distribution of specific surface area, features extracted from the image Can be calculated from.
- the porosity thus obtained may be used as an index obtained from the particle size distribution in the blast furnace operating method according to the present embodiment.
- FIG. 4 is a graph showing the relationship between the amount of change in porosity and the air permeability index in 4 hours.
- the horizontal axis of FIG. 4 is the amount of change (volume%) in the porosity in 4 hours.
- “-5” on the horizontal axis indicates that the porosity decreased by 5% by volume in 4 hours. That is, the amount of change in the porosity on the horizontal axis is a value obtained by subtracting the porosity 4 hours ago from the current porosity.
- the current porosity is the porosity of each charge of coke charged into the blast furnace in the last hour, and the average of the charges is taken as the average value, and the average value of each charge in the last hour is further averaged. The value.
- the average value of the porosity of the past 4 charges of coke may be used as the current porosity, and these moving average values may be used as the current porosity. May be good.
- the amount of change in the porosity on the horizontal axis is a value obtained by performing this operation every hour and subtracting the porosity 4 hours ago from the current porosity.
- the vertical axis of FIG. 4 is the current in-core ventilation index, and a large in-core ventilation index indicates that there is a large variation in the air permeability in the furnace in the circumferential direction.
- the meaning and measurement method of the in-core ventilation index are the same as those shown in the vertical axis of FIG.
- the plot in FIG. 4 shows the measured values of the in-core ventilation index when the in-core ventilation index was 120 or less 4 hours ago and the blast furnace operating conditions were not changed in the subsequent 4 hours.
- the amount of change in porosity becomes -5% by volume or less in 4 hours, there is a high possibility that the in-core aeration index exceeds 120. Therefore, in the blast furnace operation method according to the embodiment using the porosity as an index, the amount of change in the average value of the porosity for 1 hour obtained from the coke charged in the blast furnace is -5% by volume or less within 4 hours. If this happens, reduce the amount of air blown from the tuyere by 5% or more.
- the amount of change of porosity ⁇ 5% by volume within 4 hours is another example of the first threshold value of the preset amount of change in a certain time.
- the amount of air blown from the tuyere may be reduced once or divided into a plurality of times.
- the porosity may always exceed the threshold value, so it is necessary to change the threshold value according to the situation of the raw materials charged into the blast furnace. Therefore, it is difficult to prevent the pressure balance in the furnace from being significantly disturbed by controlling the porosity with a specific threshold value.
- it can be said that it is preferable to control by the amount of change in the porosity, not by the control by the threshold value of the specific porosity.
- the amount of air blown from the tuyere After reducing the amount of air blown from the tuyere by 5% or more, if the average value of porosity for 1 hour changes by -5% by volume or less within 2 hours without increasing, the amount of air blown from the tuyere is further increased. It is preferable to reduce by 5% or more. As a result, even if the air permeability in the furnace is further deteriorated by further reducing the porosity, the turbulence of the gas flow in the furnace can be reduced by reducing the amount of air blown from the tuyere, and the pressure in the furnace can be reduced. It is possible to further prevent the balance from being greatly lost.
- the amount of change in the average value of the porosity for 1 hour becomes -10% by volume or less within 4 hours, the air permeability in the furnace will be significantly deteriorated. It becomes difficult to deal with it. Therefore, when the amount of decrease in porosity is large, it is preferable to adjust the amount of air blown from the tuyere and also adjust the coke ratio. If the amount of change in the average value of the porosity for 1 hour becomes -10% by volume or less within 4 hours when the amount of air blown is reduced by 5% or more as described above, in addition to the decrease in the amount of air blown. It is preferable to increase the coke ratio of the raw material.
- the coke ratio is increased by 20 kg / t-pig or more within the range where the reducing agent ratio does not exceed 600 kg / t-pig (kg per ton of hot metal).
- the coke ratio is 360 kg / t-pig or less while pulverized coal is blown in at 50 to 200 kg / t-pig
- the coke ratio is increased to 380 kg / t-pig and the coke ratio is 360 kg / t.
- it is larger than -pig and less than 400 kg / t-pig the coke ratio is increased to 400 kg / t-pig. If the coke ratio is already 400 kg / t-pig or more, the coke ratio is not increased any more.
- the amount of change in porosity within 4 hours is -5% by volume, which is an absolute value larger than the absolute value of this value.
- Two thresholds of the amount of change in the porosity ⁇ 10% by volume are set in advance.
- the amount of change in porosity within 4 hours is greater than -10% by volume and less than -5% by volume, the amount of air blown from the tuyere is reduced without changing the coke ratio, and the porosity within 4 hours.
- the amount of change in is -10% by volume or less, the coke ratio is increased without reducing the amount of air blown.
- the amount of change in the average value of the porosity for 1 hour becomes -10% by volume or less within 4 hours, and even if it is considered that the air permeability in the furnace is significantly deteriorated, the pressure balance in the furnace is large. It can be suppressed from collapsing.
- the amount of change in porosity ⁇ 10% by volume within 4 hours is another example of a second threshold of a preset amount of change in a given time.
- the amount of air blown from the tuyere When the amount of air blown from the tuyere is reduced, if the average value of the porosity for 1 hour is higher than when the amount of air blown is reduced after 4 hours have passed since the amount of air was reduced. It is preferable to return the air volume from the tuyere to the air volume before the reduction.
- the amount of air blown from the tuyere When the amount of air blown from the tuyere is reduced by 5%, the amount of air blown from the tuyere is increased by 5%, and when the amount of air blown from the tuyere is reduced by 10% (5% reduction is performed twice). It is preferable to increase the amount of air blown from the tuyere by 10% to return the amount of air blown to the original amount.
- the gas flow in the furnace stabilizes. Therefore, if the 1-hour average value of the porosity does not decrease 4 hours after the airflow from the tuyere is reduced and the average value of the porosity increases, the airflow from the tuyere is increased. It is preferable to return to the air volume before the reduction. By returning the amount of air from the tuyere to the original amount after 4 hours have passed since the amount of air was reduced, the amount of air from the tuyere is returned to the original amount without significantly disturbing the pressure balance in the furnace. be able to.
- the coke ratio may be returned to that before the coke ratio was increased. In this way, by returning the coke ratio to the original value after 4 hours have passed since the coke ratio was increased, the coke ratio can be returned to the original coke ratio without significantly disturbing the pressure balance in the furnace.
- the amount of change in the index value over a certain period of time is the value obtained by subtracting the value of the index before a certain time from the value of the current index.
- the coke powder ratio when used as an index, it is preferable to set a positive value as the first or second threshold value and adjust the air flow amount and the coke ratio when the change amount becomes equal to or more than the threshold value. ..
- the porosity when used as an index, it is preferable to set a negative value as the first or second threshold value and adjust the amount of air blown or the coke ratio when the amount of change becomes equal to or less than the threshold value.
- Example 1 in which the blast furnace operation method according to the present embodiment is implemented will be described.
- the coke powder ratio was used as an index obtained from the particle size distribution.
- the coke sieved by a sieve having a mesh size of 35 mm was conveyed to the blast furnace skeleton tank using a conveyor, and the powder ratio of the coke conveyed using the particle size distribution measuring device 10 was measured online.
- Coke was charged into the blast furnace from the corpse tank at 4 charges / hour.
- the average value of the measured coke powder ratio of each charge was calculated, and the average of 4 charges was used as the coke powder ratio.
- the amount of air blown from the tuyere and the coke ratio were controlled using the coke powder ratio.
- the amount of air blown from the tuyere As a control of the amount of air blown from the tuyere, if the coke powder ratio increases by 0.5% by mass within 4 hours, the amount of air blown from the tuyere is reduced by 5%, and the powder ratio is further reduced within 2 hours. When it increased by 0.5% by mass or more, the amount of air blown from the tuyere was reduced by 5%. As a control of the coke ratio, when the coke powder ratio increases by 1.0% by mass or more within 4 hours and the coke ratio is 360 kg / t-pig or less, the coke ratio is 380 kg / t-pig.
- the coke ratio was larger than 360 kg / t-pig and less than 400 kg / t-pig, the coke ratio was increased to 400 kg / t-pig.
- the coke ratio was 400 kg / t-pig or more, the coke ratio was not increased any more.
- the amount of air blown from the tuyere When the amount of air blown from the tuyere is reduced, if the powder ratio of coke is lower than the powder ratio when the amount of air blown is reduced after 4 hours have passed since the amount of air blown was reduced, the tuyere The amount of air blown from was returned to the amount before it was reduced. Further, when the coke powder ratio was lower than the coke ratio when the coke ratio was increased after 4 hours had passed after the coke ratio was increased, the coke ratio was returned to the coke ratio before the coke ratio was increased.
- FIG. 5 is a graph showing an example of fluctuations in the coke powder ratio.
- the horizontal axis is time (day), and the vertical axis is the powder ratio (mass%) of coke having a particle size of 5 mm or less.
- ⁇ shown in FIG. 5 indicates that the amount of air blown from the tuyere was reduced by 5%, and ⁇ indicates that the coke ratio was increased. On the other hand, ⁇ indicates that the air volume or the coke ratio was returned before being changed.
- FIG. 6 is a graph showing an example of fluctuations in the coke powder ratio (a), the amount of air blown from the tuyere (b), and the upper pressure loss (c) of the blast furnace.
- the horizontal axis is time (h)
- the vertical axis of FIG. 6A is the powder ratio (mass%) of coke having a particle size of 5 mm or less
- the vertical axis of FIG. 6B is the amount of air blown. It is (Nm 3 / min)
- the vertical axis in FIG. 6 (c) is the upper pressure loss (kPa).
- the upper pressure loss is a differential pressure (kPa) between the pressure at the top of the furnace and the pressure of a pressure gauge provided about 10 m below the stock line in the furnace.
- the coke powder ratio measured by the particle size distribution measuring device 10 starts to increase after 6.0 h, and at 8.5 h, the average value of the powder ratio for 1 hour is within 4 hours. Since it was detected that the air volume increased by 0.5%, the amount of air blown was reduced by 5% ( ⁇ in FIG. 6A).
- the 1-hour average value of the powder ratio having a particle size of 5 mm or less increases by 0.5% by mass within 4 hours, the air permeability in the furnace deteriorates and the upper pressure loss increases. As shown in FIG. 6 (c). The upper pressure loss did not increase.
- the coke powder ratio was lower than when the amount of air blown was reduced after 4 hours, so the amount of air blown from the tuyere was increased by 5%.
- the air volume was returned to the air volume before the change ( ⁇ in FIG. 6A).
- the 1-hour average value of the coke powder ratio increased by 0.5 mass within 4 hours, and the air volume was reduced by 5% in response to the deterioration of the air permeability in the furnace, so the air volume was increased by 5%.
- the upper pressure drop index would increase as the amount was increased, but the upper pressure drop index did not increase as shown in FIG. 6 (c).
- the pressure balance in the furnace is stabilized by setting the time to restore the amount of air blown from the tuyere to the original value 4 hours after the amount of air blown is reduced, and based on the amount of air blown from the tuyere. It was confirmed that the upper pressure loss index did not increase even when the pressure was returned, and it was possible to prevent the pressure balance in the furnace from being significantly disturbed.
- FIG. 7 is a graph showing the relationship between the coke ratio and the upper pressure loss.
- the horizontal axis of FIG. 7 is the coke ratio (kg / t-pig), and the vertical axis is the upper pressure loss (kPa).
- the average strength DI (150/15) of coke during the period of Comparative Example 1 was 82.8, the average particle size was 42.7 mm, and the average powder ratio was 0.6%.
- the average strength DI (150/15) of coke during the period of Example 1 was 82.7, the average particle size was 42.8 mm, and the average powder ratio was 0.7%. As described above, the average properties of coke were almost the same between the period of Comparative Example 1 and the period of Example 1.
- Example 2 in which the blast furnace operation method according to the present embodiment is implemented will be described.
- the porosity was used as an index obtained from the particle size distribution.
- the coke sieved by a sieve having a mesh size of 35 mm is conveyed to the blast furnace skeleton tank using a conveyor, and the particle size distribution and coarse grain size distribution of the coke transported by the method described in Patent Document 2 are used.
- the distribution was measured online to determine the porosity of coke.
- Coke was charged into the blast furnace from the corpse tank at 4 charges / hour.
- the average value of the measured coke porosity of each charge was calculated, and the average of 4 charges was used as the coke porosity.
- the porosity of this coke was used to control the amount of air blown from the tuyere and the coke ratio.
- the amount of air blown from the tuyere As a control of the amount of air blown from the tuyere, if the amount of change in the average value of the porosity for 1 hour becomes -5% by volume or less within 4 hours, the amount of air blown from the tuyere is reduced by 5%, and further. When the amount of change in the average value of the porosity for 1 hour became -5% by volume or less within 2 hours, the amount of air blown from the tuyere was reduced by 5%. As a control of the coke ratio, when the amount of change in the average value of the void ratio for 1 hour is -10% by volume or less within 4 hours and the coke ratio is 360 kg / t-pig or less, coke is used.
- the ratio was increased to 380 kg / t-pig, and when the coke ratio was greater than 360 kg / t-pig and less than 400 kg / t-pig, the coke ratio was increased to 400 kg / t-pig. When the coke ratio was 400 kg / t-pig or more, the coke ratio was not increased any more.
- the porosity from the tuyere When the airflow from the tuyere is reduced and the porosity is higher than the porosity when the airflow is reduced after 4 hours have passed since the airflow was reduced, the porosity from the tuyere is increased. The air volume was returned to the one before the air volume was reduced. Further, when the porosity increased from the porosity when the coke ratio was increased after 4 hours had passed after the coke ratio was increased, the coke ratio was returned to the coke ratio before the coke ratio was increased.
- Example 2 In order to confirm the effect of the blast furnace operation method of Example 2, the control of the air volume and the coke ratio was applied for two months before applying the control of the air volume and the coke ratio (Comparative Example 2) in the same blast furnace. In the latter two months (Example 2), the relationship between the coke ratio and the upper pressure loss was investigated.
- FIG. 8 is a graph showing the relationship between the coke ratio and the upper pressure loss.
- the horizontal axis of FIG. 8 is the coke ratio (kg / t-pig), and the vertical axis is the upper pressure loss (kPa).
- the average strength DI (150/15) of coke during the period of Comparative Example 2 was 83.0, the average particle size was 44.0 mm, and the average porosity was 48.3%.
- the average strength DI (150/15) of coke during the period of Example 2 was 82.9, the average particle size was 43.8 mm, and the average porosity was 48.2%. As described above, the average properties of coke were almost the same between the period of Comparative Example 2 and the period of Example 2.
- the porosity was determined based on the blast furnace operating method of Example 2, and the relationship between the upper pressure loss and the coke ratio when the air flow rate and the coke ratio were adjusted based on the porosity was shown.
- the approximate straight line of the plot of Example 2 was lower than the approximate straight line of the plot of Comparative Example 2 in which the porosity and the coke ratio were not adjusted. From this result, it was confirmed that the increase in the upper pressure loss can be suppressed by applying the blast furnace operation method of Example 2.
- Particle size distribution measuring device 10 Particle size distribution measuring device 12 Imaging device 14 Lighting device 16 Arithmetic logic unit 20 Coke 22 Hopper 24 Sieve 26 Conveyor 30 Blast furnace
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Abstract
Description
(1)炉下部に設けられた羽口から送風して高炉を操業する高炉操業方法であって、前記高炉へ搬送されるコークスの粒度分布を逐次測定し、前記粒度分布から求められる指標に応じて送風量およびコークス比の少なくとも一方を調整する、高炉操業方法。
(2)前記送風量を調整する場合であって、前記指標の一定時間での変化量に対して第1の閾値を予め設定し、前記第1の閾値が正の値の場合は、前記指標の一定時間での変化量が予め設定された第1の閾値以上である場合に前記送風量を減少させ、前記第1の閾値が負の値の場合は、前記指標の一定時間での変化量が予め設定された第1の閾値以下である場合に前記送風量を減少させる、(1)に記載の高炉操業方法。
(3)前記コークス比を調整する場合であって、前記指標の一定時間での変化量に対して第2の閾値を予め設定し、前記第2の閾値が正の値の場合は、前記指標の一定時間での変化量が予め設定された第2の閾値以上である場合に前記コークス比を高め、前記第2の閾値が負の値の場合は、前記指標の一定時間での変化量が予め設定された第2の閾値以下である場合に前記コークス比を高める、(1)に記載の高炉操業方法。
(4)前記指標の一定時間での変化量に対して第1の閾値と、前記第1の閾値の絶対値よりも大きい絶対値の第2の閾値を予め設定し、前記第1の閾値および前記第2の閾値が正の値の場合は、前記指標の一定時間での変化量が前記第1の閾値以上かつ前記第2の閾値未満となった場合に前記送風量を減少させ、前記指標の一定時間での変化量が前記第2の閾値以上となった場合に前記コークス比を高め、前記第1の閾値および前記第2の閾値が負の値の場合は、前記指標の一定時間での変化量が前記第1の閾値以下かつ前記第2の閾値よりも大きい場合に前記送風量を減少させ、前記指標の一定時間での変化量が前記第2の閾値以下となった場合に前記コークス比を高める、(1)に記載の高炉操業方法。
(5)前記指標は前記コークスに含まれる粒径5mm以下のコークス粉の粉率である、(1)から(4)のいずれか1つに記載の高炉操業方法。
(6)前記指標はコークス充填層の空隙率である、(1)から(4)のいずれか1つに記載の高炉操業方法。
12 撮像装置
14 照明装置
16 演算装置
20 コークス
22 ホッパ
24 篩
26 コンベア
30 高炉
Claims (6)
- 炉下部に設けられた羽口から送風して高炉を操業する高炉操業方法であって、
前記高炉へ搬送されるコークスの粒度分布を逐次測定し、
前記粒度分布から求められる指標に応じて送風量およびコークス比の少なくとも一方を調整する、高炉操業方法。 - 前記送風量を調整する場合であって、
前記指標の一定時間での変化量に対して第1の閾値を予め設定し、
前記第1の閾値が正の値の場合は、前記指標の一定時間での変化量が予め設定された第1の閾値以上である場合に前記送風量を減少させ、
前記第1の閾値が負の値の場合は、前記指標の一定時間での変化量が予め設定された第1の閾値以下である場合に前記送風量を減少させる、請求項1に記載の高炉操業方法。 - 前記コークス比を調整する場合であって、
前記指標の一定時間での変化量に対して第2の閾値を予め設定し、
前記第2の閾値が正の値の場合は、前記指標の一定時間での変化量が予め設定された第2の閾値以上である場合に前記コークス比を高め、
前記第2の閾値が負の値の場合は、前記指標の一定時間での変化量が予め設定された第2の閾値以下である場合に前記コークス比を高める、請求項1に記載の高炉操業方法。 - 前記指標の一定時間での変化量に対して第1の閾値と、前記第1の閾値の絶対値よりも大きい絶対値の第2の閾値を予め設定し、
前記第1の閾値および前記第2の閾値が正の値の場合は、
前記指標の一定時間での変化量が前記第1の閾値以上かつ前記第2の閾値未満となった場合に前記送風量を減少させ、
前記指標の一定時間での変化量が前記第2の閾値以上となった場合に前記コークス比を高め、
前記第1の閾値および前記第2の閾値が負の値の場合は、
前記指標の一定時間での変化量が前記第1の閾値以下かつ前記第2の閾値よりも大きい場合に前記送風量を減少させ、
前記指標の一定時間での変化量が前記第2の閾値以下となった場合に前記コークス比を高める、請求項1に記載の高炉操業方法。 - 前記指標は前記コークスに含まれる粒径5mm以下のコークス粉の粉率である、請求項1から請求項4のいずれか一項に記載の高炉操業方法。
- 前記指標はコークス充填層の空隙率である、請求項1から請求項4のいずれか一項に記載の高炉操業方法。
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- 2020-10-19 WO PCT/JP2020/039288 patent/WO2021085221A1/ja unknown
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- 2020-10-19 EP EP20882125.6A patent/EP4029953B1/en active Active
- 2020-10-19 JP JP2021522106A patent/JP7074259B2/ja active Active
- 2020-10-29 TW TW109137528A patent/TWI783285B/zh active
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US20220380859A1 (en) | 2022-12-01 |
EP4029953B1 (en) | 2023-09-20 |
CN114599802A (zh) | 2022-06-07 |
BR112022007841A2 (pt) | 2022-07-05 |
TWI783285B (zh) | 2022-11-11 |
EP4029953A4 (en) | 2022-11-16 |
JP7074259B2 (ja) | 2022-05-24 |
KR20220066146A (ko) | 2022-05-23 |
EP4029953A1 (en) | 2022-07-20 |
JPWO2021085221A1 (ja) | 2021-11-25 |
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CN114599802B (zh) | 2024-03-29 |
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