WO2017096735A1 - 一种纳米碳多功能饮料及其制备方法 - Google Patents

一种纳米碳多功能饮料及其制备方法 Download PDF

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WO2017096735A1
WO2017096735A1 PCT/CN2016/078247 CN2016078247W WO2017096735A1 WO 2017096735 A1 WO2017096735 A1 WO 2017096735A1 CN 2016078247 W CN2016078247 W CN 2016078247W WO 2017096735 A1 WO2017096735 A1 WO 2017096735A1
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carbon
nanocarbon
nano carbon
water
nano
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陈国�
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四川百草通科新材料科技有限公司
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/44—Elemental carbon, e.g. charcoal, carbon black

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  • the invention belongs to the field of food technology, and in particular relates to a nano carbon multifunctional beverage and a preparation method thereof.
  • the object of the present invention is to solve the above problems and to provide a nanocarbon multifunctional beverage which can relieve or even cure a gastrointestinal disease.
  • Another object of the present invention is to provide a method for preparing the above nanocarbon multifunctional beverage.
  • the technical solution of the present invention is: a nano carbon multifunctional beverage, wherein the raw material comprises nano carbon and water, and is prepared by grinding, compounding and sterilizing processes, wherein the nano carbon content is 1 ⁇ g to 100000 ⁇ g. /ml.
  • the raw material further comprises a surfactant having a surfactant content of from 0 g to 1 g/ml.
  • the surfactant comprises one or more of an anionic surfactant, a cationic surfactant, and an ionic surfactant.
  • the nanocarbon comprises one or more of activated carbon, carbon black, carbon nanotubes, microcrystalline carbon, carbon aerogel, graphene.
  • the water is one or more of deionized water, distilled water, mineral water or purified water.
  • Nano carbon particles have good chemical stability, large specific surface area and good surface activity. Therefore, after entering the human body, nano carbon can effectively adsorb residual pesticides, fungicides, heavy metals and dioxins in the digestive tract and human body. As well as a variety of pathogenic bacteria and their toxins, it can also absorb harmful substances such as creatinine and uric acid, and also has a bactericidal and antibacterial effect.
  • Surfactants are used to improve the storage stability of the nanocarbon dispersion.
  • the invention provides a method for preparing a nano carbon multifunctional beverage, wherein the raw material comprises nano carbon and water, the nano carbon is added into water and ground to obtain a nano carbon slurry, and then the nano carbon slurry is prepared and mixed into water, and the sterilization process can be performed.
  • the nano carbon content is from 1 ⁇ g to 100,000 ⁇ g/ml.
  • the method specifically comprises the following steps:
  • S22 sterilizing the nano carbon dispersion obtained by S21, and filling the nano carbon multifunctional beverage product by filling.
  • the method further comprises the steps of:
  • a surfactant is added to the nanocarbon dispersion obtained in S21, and the surfactant is added in an amount of from 0 g to 1 g/ml.
  • the sterilization in the steps S11 and S21 is performed by steam sterilization.
  • the sterilization process is carried out in addition to the raw materials, the equipment and the nano carbon dispersion obtained in the step S21, and the finished beverage product after the filling can be integrally sterilized, so that the sterilization effect is more ideal.
  • the invention has the beneficial effects that the nano carbon multifunctional beverage provided by the invention can effectively adsorb residual pesticides, bactericides, heavy metals, dioxins and various pathogenic bacteria in the digestive tract and human body due to the nano carbon raw material. Its toxins, wastes that damage human health or cause diseases, etc., can also adsorb harmful substances such as creatinine and uric acid, and have the effect of cleaning up the gastrointestinal waste.
  • the nano carbon multifunctional beverage also has a bactericidal and antibacterial effect, and the action principle of the nano carbon is a physical action, and has no toxic and side effects to the human body.
  • the preparation method of the nano carbon multifunctional beverage provided by the invention is simple, operability and easy to standardize, and is worthy of being promoted in the industry.
  • FIG. 1 is a schematic view showing the steps of a method for preparing a nanocarbon multifunctional beverage according to the present invention.
  • a schematic diagram of a method for preparing a nano carbon multifunctional beverage according to the present invention includes the following steps:
  • Step S1 Preparation of nano carbon slurry:
  • S22 sterilizing the nano carbon dispersion obtained by S21, and filling the nano carbon multifunctional beverage product by filling;
  • the detection of the absorbance in step S13 is the initial inspection of the nano-carbon content, and the preparation of the nano-carbon slurry by the added nano-carbon content is strictly calculated, and the initial inspection of the step may not be performed.
  • the sampling of the particle size, the carbon content, the heavy metal content and the bacterial content in step S23 is to ensure the quality of the product, and whether it is carried out or not is not the key to preparing the nanocarbon multifunctional beverage of the present invention and the preparation method thereof.
  • S22 The nano carbon dispersion obtained by S21 is steam sterilized, and the steam temperature is 121 ° C for 30 minutes, and the nano carbon multifunctional beverage is finished by filling.
  • S22 steam sterilization of the nano carbon dispersion obtained in S21, steam temperature 121 ° C, time 30 minutes, filling system Get the finished nano-carbon multi-functional beverage.
  • S22 The nano carbon dispersion obtained by S21 is steam sterilized, and the steam temperature is 121 ° C for 30 minutes, and the nano carbon multifunctional beverage is finished by filling.
  • nanocarbon multifunctional beverage prepared in the above Examples 1 to 3 was tested for particle size, carbon content, absorbance, heavy metal content and bacterial content, and the results are shown in the following table:
  • nanocarbon multifunctional beverage prepared in the above Examples 1 to 3 was subjected to an antibacterial experiment according to the standard "QB/T 2591-2003 antibacterial plastic - antibacterial property test method and antibacterial effect", using the experimental strain: Escherichia coli, golden yellow Staphylococcus and Helicobacter pylori, the results are shown in the table below:
  • the clinical experiment was carried out on the nano-carbon multifunctional beverage prepared in Example 3.
  • the cases were: habitual enteritis, gastric acid (gastritis) and bad breath. Each case was 100 people, and the age was evenly distributed between 20 and 60 years old. People, for three consecutive months Drink the nano-carbon multi-functional beverage of the present invention, 10 ml / support, three times a day, once a month, the results are as follows:
  • the nano carbon multifunctional beverage provided by the invention contains nano carbon raw materials, can effectively adsorb residual pesticides, bactericides, heavy metals, dioxins, various pathogenic bacteria and toxins thereof in the digestive tract and human body, and damage human health. Or pathogenic waste, etc., can also adsorb harmful substances such as creatinine, uric acid, and have the effect of cleaning up the gastrointestinal waste.
  • the nano carbon multifunctional beverage also has a bactericidal antibacterial effect. It can be intuitively seen from the above antibacterial experiment and the result of the case experiment that the nanocarbon multifunctional beverage provided by the invention has good antibacterial effect and has an effective healing ability against gastrointestinal diseases.
  • nanocarbon The principle of action of nanocarbon is physical, so the nanocarbon multifunctional beverage has no toxic side effects on the human body. Further, the preparation method of the nano carbon multifunctional beverage provided by the invention is simple, operability, easy to standardize, and is worthy of being promoted in the industry.

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
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  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Non-Alcoholic Beverages (AREA)
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Abstract

一种纳米碳饮料，原料包括纳米碳和水，经研磨、调配、灭菌工艺后制成，其中纳米碳含量为1μg～100000μg/ml。该饮料的制备方法是，将纳米碳加入水中经过研磨制得纳米碳浆料，再取纳米碳浆料调配入水中，经灭菌即可。该饮料能有效地清理胃肠道垃圾，还能吸附肌酐、尿酸等有害物质，同时具有杀菌抗菌作用。

Description

一种纳米碳多功能饮料及其制备方法 技术领域
本发明属于食品技术领域，具体涉及一种纳米碳多功能饮料及其制备方法。
背景技术
饮料属于人们生活不可或缺的食品。随之人们对食品多样化要求的提升，单一用于解渴的饮料已经满足不了市场的需求，于是各式各样的饮料层出不穷，从不同可感到不同颜色，再到不同功能。从功能饮料分析，现在市场有用于补充体力的能量饮品，如红牛、东鹏特饮及K可人参等品牌，也有用于补充维生素的蔬菜水果饮料，还有用于补充蛋白质的动植物奶制品饮料。上述功能饮料主要强调补充营养，但是在现有的物质生活水平下，人们摄入的食物中已经可提供足够的营养于人体，甚至出现营养过剩的现象。市场上还有一类清理型饮料，如肠茶清，但是此类清理型饮料其清理作用仅限于吸附，功效十分有限。
发明内容
本发明的目的是解决上述问题，提供一种对胃肠道疾病起到缓解乃至治愈作用的纳米碳多功能饮料。
本发明的另一目的在于提供一种上述纳米碳多功能饮料的制备方法。
为解决上述技术问题，本发明的技术方案是：一种纳米碳多功能饮料，其原料包括纳米碳和水，经研磨、调配、灭菌工艺后制备而成，其中纳米碳含量为1μg～100000μg/ml。
优选地，所述原料还包括表面活性剂，所述表面活性剂含量为0g～1g/ml。
优选地，所述表面活性剂包括阴离子表面活性剂、阳离子表面活性剂和离子表面活性剂中的一种或多种。
优选地，所述纳米碳包括活性炭、炭黑、纳米碳管、微晶碳、碳气凝胶、石墨烯中一种或多种。
优选地，所述水为去离子水、蒸馏水、矿物质水或净化水中的一种或多种。
纳米碳粒子，具有良好的化学稳定性、较大的比表面积以及良好的表面活性，因此，纳米碳进入人体后，能有效地吸附消化道及人体内残留农药、杀菌剂、重金属、二噁英以及各种致病菌及其毒素，还能吸附肌酐和尿酸等有害物质，同时还具有杀菌抗菌作用。
表面活性剂用于提高纳米碳分散液的存储稳定性。
本发明提供的纳米碳多功能饮料的制备方法，原料包括纳米碳和水，将纳米碳加入水中经过研磨制得纳米碳浆料，再取纳米碳浆料调配入水中，经灭菌工艺即可，纳米碳含量为1μg～100000μg/ml。
优选地，该方法具体包括以下步骤：
S1：纳米碳浆料制备：
S11：对原料、仪器设备进行清洗灭菌处理；
S12：取纳米碳加入水中，球磨2～12小时后，将所得浆体再进行砂磨2～12小时，制得50～170nm的纳米碳浆料；
S2：饮料制备：
S21：取S1中所得纳米碳浆料加入水中，搅拌至液体均一稳定，制得纳米碳含量为1μg～100000μg/ml的纳米碳分散液；
S22：对S21所得纳米碳分散液进行灭菌，灌装制得纳米碳多功能饮料成品。
优选地，该方法还包括步骤：
S211：在S21所得纳米碳分散液中添加表面活性剂，表面活性剂添加量为0g～1g/ml。
优选地，所述步骤S11、S21中灭菌采用蒸汽灭菌法。
值得说明的是，本发明中，灭菌工艺除了针对原料、仪器设备以及步骤S21所得纳米碳分散液进行，还可对灌装后所得饮料成品进整体灭菌，以使灭菌效果更加理想。
本发明的有益效果是：本发明提供的纳米碳多功能饮料，由于含有纳米碳原料，能有效地吸附消化道及人体内的残留农药、杀菌剂、重金属、二噁英、各种致病菌及其毒素、有损害人体健康或致病的废物等，还能吸附肌酐、尿酸等有害物质，具有清理胃肠道垃圾作用。该纳米碳多功能饮料还具有杀菌抗菌作用，且纳米碳的作用原理为物理作用，对人体完全无毒副作用。本发明提供的纳米碳多功能饮料的制备方法，简单可操作性强，易于标准化，值得在业内推广。
附图说明
图1是本发明纳米碳多功能饮料的制备方法步骤示意图。
具体实施方式
为了使本发明的目的、技术方案和优点更加清楚，以下结合具体实施例和附图，对本发明作进一步的详细说明。
如图1所示，本发明的纳米碳多功能饮料的制备方法步骤示意图，包括以下步骤：
步骤S1：纳米碳浆料制备：
S11：对原料、仪器设备进行清洗灭菌处理；
S12：取纳米碳加入水中，球磨2～12小时后，将所得浆体再进行砂磨2～12小时，制得50～170nm的纳米碳浆料；
S13：检测吸光度；
S2：饮料制备：
S21：取S1中所得纳米碳浆料加入水中，搅拌至液体均一稳定，制得纳米碳含量为1μg～100000μg/ml的纳米碳分散液；
S22：对S21所得纳米碳分散液进行灭菌，灌装制得纳米碳多功能饮料成品；
S23：抽样检测粒径、碳含量、重金属含量以及细菌含量；
S24：包装入库。
值得说明的是，步骤S13吸光度的检测，是对纳米碳含量的初检，严格按照经计算而因添加的纳米碳含量进行纳米碳浆料制备，也可不进行该步骤的初检。步骤S23中抽样检测粒径、碳含量、重金属含量以及细菌含量，是为了保证产品的品质，其是否进行与否，并不是制备本发明纳米碳多功能饮料及其制备方法的关键所在。
实施例1
S11：对原料、仪器设备进行清洗灭菌处理；
S12：量取碳气凝胶1㎏，加入100㎏去离子水中，球磨2小时，球磨转速为200r/min，将球磨后的浆体再进行砂磨2～12小时，砂磨转速800r/min，制得170nm的纳米碳气凝胶浆料；
S13：检测吸光度；
S2：饮料制备：
S21：取S1中所得纳米碳气凝胶浆料1㎏，加入500L超纯水中，边滴加边搅拌，直至液体均一稳定，制得纳米碳含量为50μg/ml的纳米碳分散液；
S22：对S21所得纳米碳分散液进行蒸汽灭菌，蒸汽温度121℃，时间30分钟，灌装制得纳米碳多功能饮料成品。
S23：抽样检测粒径、碳含量、重金属含量以及细菌含量；
S24：包装入库。
实施例2
S11：对原料、仪器设备进行清洗灭菌处理；
S12：量取碳气凝胶1㎏，加入100㎏去离子水中，球磨6小时，球磨转速为200r/min，将球磨后的浆体再进行砂磨6小时，砂磨转速800r/min，制得70nm的纳米碳气凝胶浆料；
S13：检测吸光度；
S2：饮料制备：
S21：取S1中所得纳米碳气凝胶浆料1㎏，加入500L超纯水中，边滴加边搅拌，直至液体均一稳定，制得纳米碳含量为50μg/ml的纳米碳分散液；
S22：对S21所得纳米碳分散液进行蒸汽灭菌，蒸汽温度121℃，时间30分钟，灌装制 得纳米碳多功能饮料成品。
S23：抽样检测粒径、碳含量、重金属含量以及细菌含量；
S24：包装入库。
实施例3
S11：对原料、仪器设备进行清洗灭菌处理；
S12：量取碳气凝胶1㎏，加入100㎏去离子水中，球磨12小时，球磨转速为200r/min，将球磨后的浆体再进行砂磨12小时，砂磨转速800r/min，制得50nm的纳米碳气凝胶浆料；
S13：检测吸光度；
S2：饮料制备：
S21：取S1中所得纳米碳气凝胶浆料1㎏，加入500L超纯水中，边滴加边搅拌，直至液体均一稳定，制得纳米碳含量为50μg/ml的纳米碳分散液；
S22：对S21所得纳米碳分散液进行蒸汽灭菌，蒸汽温度121℃，时间30分钟，灌装制得纳米碳多功能饮料成品。
S23：抽样检测粒径、碳含量、重金属含量以及细菌含量；
S24：包装入库。
对上述实施例1～3所制得的纳米碳多功能饮料，进行粒度、碳含量、吸光度、重金属含量以及细菌含量的检测，结果见下表：
  粒度(nm) 碳含量(μg/ml) 吸光度 铅镉汞砷总量 细菌总量
实施例1 170 50 1.04A 未检出 未检出
实施例2 70 50 1.01A 未检出 未检出
实施例3 55 50 0.97A 未检出 未检出
对上述实施例1～3所制得的纳米碳多功能饮料，按照标准《QB/T 2591-2003抗菌塑料-抗菌性能试验方法和抗菌效果》进行抗菌实验，采用实验菌株：大肠杆菌、金黄色葡萄球菌和幽门螺旋杆菌，结果见下表：
Figure PCTCN2016078247-appb-000001
对实施例3制得的纳米碳多功能饮料进行临床实验，采用病例：习惯性肠炎、胃酸(胃炎)和口臭，每个病例100人，年龄均匀分布于20～60岁之间，男女分别50人，连续三月 饮用本发明的纳米碳多功能饮料，10ml/支，每天三只，每月检查一次，结果见下表：
Figure PCTCN2016078247-appb-000002
本发明提供的纳米碳多功能饮料，含有纳米碳原料，能有效地吸附消化道及人体内的残留农药、杀菌剂、重金属、二噁英、各种致病菌及其毒素、有损害人体健康或致病的废物等，还能吸附肌酐、尿酸等有害物质，具有清理胃肠道垃圾作用。该纳米碳多功能饮料还具有杀菌抗菌作用。由上述抗菌实验以及病例实验结果可直观得知，本发明提供的纳米碳多功能饮料，具有良好的抗菌效果，同时对胃肠疾病具有有效的治愈能力。纳米碳的作用原理为物理作用，因此该纳米碳多功能饮料对人体完全无毒副作用。进一步的，本发明提供的纳米碳多功能饮料的制备方法，简单可操作性强，易于标准化，值得在业内推广。
本领域的普通技术人员将会意识到，这里所述的实施例是为了帮助读者理解本发明的原理，应被理解为本发明的保护范围并不局限于这样的特别陈述和实施例。本领域的普通技术人员可以根据本发明公开的这些技术启示做出各种不脱离本发明实质的其它各种具体变形和组合，这些变形和组合仍然在本发明的保护范围内。

Claims (9)

  1. 一种纳米碳多功能饮料，其特征在于：其原料包括纳米碳和水，经研磨、调配、灭菌工艺后制备而成，其中纳米碳含量为1μg～100000μg/ml。
  2. 根据权利要求1所述的纳米碳多功能饮料，其特征在于：所述原料还包括表面活性剂，所述表面活性剂含量为0g～1g/ml。
  3. 根据权利要求2所述的纳米碳多功能饮料，其特征在于：所述表面活性剂包括阴离子表面活性剂、阳离子表面活性剂和离子表面活性剂中的一种或多种。
  4. 根据权利要求1所述的纳米碳多功能饮料，其特征在于：所述纳米碳包括活性炭、炭黑、纳米碳管、微晶碳、碳气凝胶、石墨烯单体/混合物的中一种或多种。
  5. 根据权利要求1所述的纳米碳多功能饮料，其特征在于：所述水为去离子水、蒸馏水、矿物质水或净化水中的一种或多种。
  6. 一种权利要求1～5任一所述的纳米碳多功能饮料的制备方法，其特征在于：原料包括纳米碳和水，将纳米碳加入水中经过研磨制得纳米碳浆料，再取纳米碳浆料调配入水中，经灭菌工艺即可，纳米碳含量为1μg～100000μg/ml。
  7. 根据权利要求6所述的纳米碳多功能饮料的制备方法，其特征在于：该方法具体包括以下步骤：
    S1：纳米碳浆料制备：
    S11：对原料、仪器设备进行清洗灭菌处理；
    S12：取纳米碳加入水中，球磨2～12小时后，将所得浆体再进行砂磨2～12小时，制得50～170nm的纳米碳浆料；
    S2：饮料制备：
    S21：取S1中所得纳米碳浆料加入水中，搅拌至液体均一稳定，制得纳米碳含量为1μg～100000μg/ml的纳米碳分散液；
    S22：对S21所得纳米碳分散液进行灭菌，灌装制得纳米碳多功能饮料成品。
  8. 根据权利要求7所述的纳米碳多功能饮料的制备方法，其特征在于：该方法还包括步骤：
    S211：在S21所得纳米碳分散液中添加表面活性剂，表面活性剂添加量为0g～1g/ml。
  9. 根据权利要求7所述的纳米碳多功能饮料的制备方法，其特征在于：所述步骤S11、S21中灭菌采用蒸汽灭菌法。
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