WO2012133289A1 - Produit de tabac de type à aspiration mais sans combustion - Google Patents
Produit de tabac de type à aspiration mais sans combustion Download PDFInfo
- Publication number
- WO2012133289A1 WO2012133289A1 PCT/JP2012/057726 JP2012057726W WO2012133289A1 WO 2012133289 A1 WO2012133289 A1 WO 2012133289A1 JP 2012057726 W JP2012057726 W JP 2012057726W WO 2012133289 A1 WO2012133289 A1 WO 2012133289A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- tobacco
- stabilizer
- less
- tobacco product
- suction type
- Prior art date
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F42/00—Simulated smoking devices other than electrically operated; Component parts thereof; Manufacture or testing thereof
- A24F42/20—Devices without heating means
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/20—Devices using solid inhalable precursors
Definitions
- the present invention relates to a non-combustion suction type tobacco product that eliminates the generation of smoke associated with ignition.
- This type of non-combustion suction type tobacco product includes a hollow suction holder and a packing of tobacco particles obtained by granulating the tobacco raw material and having a ventilation resistance of about 40 to about 80 mmHg.
- a ventilation resistance of about 40 to about 80 mmHg.
- the amount of nicotine released from tobacco particles decreases relatively rapidly as the number of puffs increases. This means that as the number of puffs increases, the nicotine sucked by the user changes greatly. This not only gives the user a sense of incongruity when using the suction, but also allows the user to use a usable period (the number of puffs). ) Feels shorter (less) than expected.
- the present invention has been made based on the above-mentioned circumstances, and the object of the present invention is to stabilize the delivery amount of nicotine, which is one of tobacco-specific components, over a long period of time, greatly increasing the number of puffs satisfied by the user. It is to provide a non-combustion suction type tobacco product that can be increased.
- This non-combustion suction type tobacco product stabilizes the tobacco granules obtained by cutting or crushing tobacco raw materials and the delivery of nicotine from the granules. At least one stabilizer that has a solubility parameter distance with nicotine of 17 or less and a vapor pressure at 25 ° C. of 1 mmHg or less.
- the stabilizer is selected from propylene glycol, benzyl alcohol, or a compound having an ester group, which includes medium chain fatty acid triglycerides, citric acid triesters (triethyl citrate, tributyl citrate, etc.), benzyl benzoate and lauric acid. Selected from ethyl acid.
- the stabilizer preferably has a characteristic that the distance between solubility parameters is 12 or less and the vapor pressure at 25 ° C. is 0.1 mmHg or less.
- the tobacco particulates can further include an additive composed of at least one of a carbonate and a bicarbonate generally used in snuff products such as snus.
- the non-combustion suction type tobacco product may further include a heating source for heating the tobacco particulates.
- the stabilizer has a characteristic that the distance between the solubility parameters is 17 or less and the vapor pressure becomes 1 mmHg or less at the heating temperature of the tobacco granular material.
- the content of the stabilizer is preferably 5 to 20% by weight based on the dry matter weight of the source. In this case, if the content of the stabilizer is less than 5% by weight, the required stabilization of nicotine cannot be obtained. Conversely, if the content of the stabilizer is more than 20% by weight, the stabilizer becomes granular.
- the agglomerates are agglomerated, making it difficult to handle tobacco granules, that is, to produce them.
- the non-combustion suction type tobacco product of the present invention contains a stabilizer in the tobacco granules, the amount of nicotine, which is one of the components unique to tobacco released from the tobacco granules, can be stabilized over a long period of time. Can be made.
- the non-combustion suction type tobacco product 1 of one embodiment shown in FIG. 1 includes an axis A, an upstream member 2, a tobacco cartridge 6, a downstream member 10, and a mouthpiece member 12 aligned along the axis A.
- These members 2, 6, 10, 12 are integrally coupled by a plurality of connecting bolts / nuts 14.
- the upstream member 2 is a 1 mm thick sheet made of stainless steel, and includes an opening region 16 in the central region.
- the opening region 16 has an opening ratio of 23%.
- the opening region 16 is formed by small holes having a diameter of 1 mm that are uniformly distributed.
- the cigarette cartridge 6 includes a frame member 18 made of stainless steel and having a thickness of 2 mm.
- the frame member 18 has an opening having an inner diameter of 26 mm at the center thereof.
- Tobacco granules 20 are accommodated in the openings, and the tobacco granules 20 have air permeability.
- the tobacco cartridge 6 further includes breathable nonwoven fabrics 4, 8 that sandwich the frame member 18 of the tobacco cartridge 6, and the tobacco particulates 20 fall off from the frame member 18. To prevent.
- the tobacco granular material 20 will be described later.
- the downstream member 10 is a 1 mm thick sheet made of stainless steel like the upstream member 2, and has an opening 22 having an inner diameter of 18 mm in the central region.
- the mouthpiece member 12 is formed of Teflon (trademark) and includes a mouth end 24. The mouth end 24 protrudes from the face of the mouth member 12 opposite to the downstream member 10 and has an inner diameter of 6 mm.
- the opening of the mouthpiece member 12 located on the downstream member 10 side has an inner diameter of 20 mm.
- the external air flows from the opening region 16 of the upstream member 2 to the nonwoven fabric 4, the tobacco granular material 20, the nonwoven fabric 8, and the downstream. It flows into the user's mouth through the opening 22 of the member 10 and the mouthpiece member 12.
- the air passes through the tobacco granule 20
- the nicotine released from the tobacco granule 20 is included in the air, and thus the user sucks in air containing nicotine.
- the tobacco granule 20 is made from a granule obtained by chopping or pulverizing a tobacco raw material made of domestically produced Burley leaf tobacco, followed by humidification and heat treatment, and, for example, at least one of carbonate and bicarbonate.
- the granular material is contained in an amount of 300 mg by dry matter weight.
- the mixture contains 12% by weight of additives based on the dry matter weight of the tobacco raw material, and nicotine, one of the tobacco-specific components contained in the granules, is 2.3% of the dry matter weight. %, And the volatile component contained in the granular material is adjusted to be 12% by weight of the weight of the granular material.
- the content of nicotine was 200 mg ⁇ 2.5 mg granule added with 7.5 ml of 11 wt% sodium hydroxide aqueous solution and 10 ml of hexane, and shaken at room temperature for 60 minutes while shielding light with aluminum foil.
- the hexane phase was obtained by analyzing with a gas chromatograph mass spectrometer.
- the content of the volatile component is determined from the weight reduction of the granular material after 200 mg ⁇ 2 mg of the granular material is dried at 80 ° C. for 3 hours. Further, the dry matter weight is represented by a value obtained by subtracting the amount of the volatile component obtained as described above from the weight of the granular material.
- the tobacco granule 20 includes, in addition to the above-mentioned mixture, at least one stabilizer that stabilizes the delivery amount of the nicotine to the user, and this stabilizer has a solubility parameter with nicotine.
- the distance is 17 or less, preferably 12 or less, and the vapor pressure at 25 ° C. is 1 mmHg or less, preferably 0.1 mmHg or less.
- the distance between solubility parameters is an index indicating the solubility of a solute in a solvent, and is generally represented by Ra (MPa 1/2 ), and Ra is obtained from the following equation.
- Ra [4 * ( ⁇ d, 2- ⁇ d, 1) ⁇ 2 + ( ⁇ p, 2- ⁇ p, 1) ⁇ 2 + ( ⁇ h, 2- ⁇ h, 1) ⁇ 2] ⁇ (1/2)
- ⁇ d, ⁇ p, and ⁇ h are defined as follows.
- ⁇ d Dispersion force of solubility parameter
- ⁇ p Dipolar interaction of solubility parameter
- ⁇ h Hydrogen bond of solubility parameter
- the stabilizer is selected from propylene glycol, benzyl alcohol, or a compound having an ester group, and as the compound, medium chain fatty acid triglyceride, citric acid triester (triethyl citrate, tributyl citrate, etc.), benzylbenzoate And ethyl laurate.
- Table 1 shows the solubility parameter distance Ra of the stabilizer and the vapor pressure at 25 ° C. together with glycerin (A).
- the stabilizer C is a medium-chain fatty acid triglyceride mainly composed of caprylic acid triglyceride, specifically, Coconut MT manufactured by Kao Corporation.
- the distance Ra between the solubility parameters in Table 1 is a calculation result using Molecular Modeling Pro Version 6.01.
- the measuring device shown in FIG. 2 is used. This measuring device is specific to the tobacco supplied from the tobacco product 1 to the user when the user sucks the tobacco product 1 described above. Measure the amount of nicotine delivered.
- the measuring apparatus includes an impinger 26 containing 20 ml of ethanol.
- an impinger 26 containing 20 ml of ethanol.
- a Kinoshita gas absorption cleaning bottle (standard type 50 ml) manufactured by Kinoshita Rika Kogyo Co., Ltd. was used for the impinger 26.
- the impinger 26 has filter particles (100 to 200 ⁇ m) inside thereof, and has a suction pipe 28 and a delivery pipe 30 respectively led out from the inside.
- the tobacco product 1 to be verified can be connected to the suction pipe 28, while the delivery pipe 30 is connected to a suction pump 36 via an electromagnetic valve 32 and a mass flow controller (MFC) 34. Further, a valve controller (VC) 38 is electrically connected to the electromagnetic valve 32, and this valve controller 38 controls the opening / closing operation of the electromagnetic valve 32.
- MFC mass flow controller
- the solenoid valve 32 can repeat one suction cycle in which the impinger 26 is released to the atmosphere for 11 seconds after the suction pump 36 and the impinger 26 are connected for 4 seconds.
- the flow rate of the mass flow controller 34 is set to 3300 cc / min.
- a tobacco product of a first comparative example in which the tobacco granule 20 does not contain glycerin (A) or stabilizers B to H and a comparative example 2 in which the tobacco granule 20 contains glycerin (A)
- Tobacco products and tobacco products of Examples each containing stabilizers B to H in tobacco granules 20 were prepared.
- the contents of glycerin (A) and stabilizers B to F are each 15% by weight (45 mg) with respect to the dry matter weight of the tobacco granules 20. Then, after connecting one of the tobacco products of Comparative Examples 1 and 2 and the Example to the suction tube 28 of the impinger 26, the above suction cycle was repeated 50 times in an environment of room temperature 22 ° C. and humidity 60%, Nicotine delivered from the tobacco product was collected in ethanol in Impinger 26.
- the ethanol from which the nicotine was collected was taken out from the impinger 26, the taken-out ethanol was analyzed with a gas chromatograph mass spectrometer, and tobacco-specific nicotine per one suction cycle (1 puff) from the tobacco product was measured.
- the collection and analysis measurements described above were repeated until the total number of aspiration cycles reached a predetermined number of times, thereby completing the measurement process for one tobacco product. Such a measurement process is carried out for each tobacco product, and the measurement results are shown in FIGS.
- the tobacco products of the examples containing the stabilizers G and H are different in the following points when compared with other examples.
- nicotine contained in the granules was 1.6% by weight of the dry weight of the tobacco raw material, and the volatile components contained in the granules were 10% by weight of the granules.
- the tobacco products of the examples containing stabilizers B to H are lower in the amount of nicotine delivered with the increase in the number of puffs than the tobacco products of comparative example 1 (without stabilizer). It can be seen that the stabilizers B to H are effective in stabilizing the delivery amount of nicotine over a long period of time.
- the decrease in the amount of nicotine delivered with the increase in the number of puffs was not significantly changed compared to the tobacco product of Comparative Example 1 (without stabilizer). It is not effective in stabilizing the delivery amount.
- the amount of nicotine delivered is lower than that of the tobacco product of Comparative Example 1 regardless of the number of puffs. This is because the trapping effect of nicotine by the stabilizer F (benzyl alcohol) is higher than that of the other stabilizers B to E, G and H. Therefore, when the stabilizer F is used, if the content of the stabilizer F is made lower than the contents of the stabilizers B to E, G, H, the tobacco product containing the stabilizer F is the tobacco of other examples. It is thought that nicotine can be delivered in the same way as the product. This point will become clear from the description of the measurement results in FIG.
- the nicotine delivery amount tends to increase as the number of puffs increases.
- the vapor at 25 ° C in the case of a stabilizer having a solubility parameter distance Ra of 12 or less, such as the stabilizer F, the vapor at 25 ° C.
- the pressure is considered to be too high, and therefore it is desirable to select a stabilizer with a vapor pressure at 25 ° C. of 0.1 mmHg or less.
- the content of the stabilizers B to H may be 5 wt% to 20 wt%. I understand that. Here, if the content is less than 5% by weight, a desired stabilizing effect cannot be obtained with respect to the delivery amount of nicotine. Conversely, if the content is more than 20% by weight, the stabilizer causes the tobacco granule 20 to be formed. Condensation makes handling of the tobacco granulate 20, ie its manufacture difficult.
- the tobacco products containing the stabilizer F can be used as stabilizers B to E, G, It is expected that a similar amount of nicotine delivered by tobacco products containing H can be generated.
- the non-combustion suction type tobacco product may include a heating source for heating the tobacco granules 20.
- the upstream member 2 of the tobacco product contains an electrical heater 40.
- the heater 40 heats the tobacco granular material 20 to a desired temperature via the upstream member 2, the nonwoven fabric 4 and the frame member 18 during use of the tobacco product.
- the stabilizer contained in the tobacco granule 20 has a vapor pressure of 1 mmHg or less at the heating temperature of the tobacco granule 20 and a solubility parameter distance Ra with nicotine of 17 or less. More preferably, the stabilizer is selected from among stabilizers having such characteristics that the vapor pressure is 0.1 mmHg or less and the distance Ra between the solubility parameters is 12 or less at the heating temperature of the tobacco granule 20.
- Table 2 shows the vapor pressures of glycerin (A) and the above-mentioned stabilizer at 25 ° C., 70 ° C. and 100 ° C., respectively.
- the stabilizer is not limited to the stabilizers B to H described above as long as the stabilizer has a characteristic in which the distance Ra between the dissolution parameters is 17 or less and the vapor pressure at 25 ° C. is 1 mmHg or less.
- B to H may be arbitrarily combined, and the structure of the tobacco product itself is not limited to that shown in FIG.
- the heating temperature illustrated in Table 2 is selected.
- the tobacco granular material 20 can be heated to an arbitrary temperature.
- the heating method of the tobacco granular material 20 is not limited to the method illustrated in FIG.
Abstract
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP12764151.2A EP2647299B1 (fr) | 2011-03-29 | 2012-03-26 | Produit de tabac de type à aspiration mais sans combustion |
JP2013507554A JP5489190B2 (ja) | 2011-03-29 | 2012-03-26 | 非燃焼吸引型たばこ製品 |
RU2013138739/12A RU2544152C1 (ru) | 2011-03-29 | 2012-03-26 | Несжигаемое табачное изделие вдыхательного типа |
CN201280008764.4A CN103369980B (zh) | 2011-03-29 | 2012-03-26 | 非燃烧吸引型烟制品 |
ES12764151T ES2735537T3 (es) | 2011-03-29 | 2012-03-26 | Producto de tabaco de tipo aspiración sin combustión |
US13/926,076 US20130284193A1 (en) | 2011-03-29 | 2013-06-25 | Non-combustion suction type tobacco product |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2011072481 | 2011-03-29 | ||
JP2011-072481 | 2011-03-29 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US13/926,076 Continuation US20130284193A1 (en) | 2011-03-29 | 2013-06-25 | Non-combustion suction type tobacco product |
Publications (1)
Publication Number | Publication Date |
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WO2012133289A1 true WO2012133289A1 (fr) | 2012-10-04 |
Family
ID=46931007
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2012/057726 WO2012133289A1 (fr) | 2011-03-29 | 2012-03-26 | Produit de tabac de type à aspiration mais sans combustion |
Country Status (8)
Country | Link |
---|---|
US (1) | US20130284193A1 (fr) |
EP (1) | EP2647299B1 (fr) |
JP (1) | JP5489190B2 (fr) |
CN (1) | CN103369980B (fr) |
ES (1) | ES2735537T3 (fr) |
RU (1) | RU2544152C1 (fr) |
TW (1) | TWI457082B (fr) |
WO (1) | WO2012133289A1 (fr) |
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CN103169157A (zh) * | 2013-04-01 | 2013-06-26 | 上海烟草集团有限责任公司 | 加热不燃烧的香烟装置 |
CN103190705A (zh) * | 2013-04-01 | 2013-07-10 | 上海烟草集团有限责任公司 | 用于加热不燃烧装置的烟草制品及其制备方法 |
WO2014104078A1 (fr) * | 2012-12-28 | 2014-07-03 | 日本たばこ産業株式会社 | Source de saveur pour produit de tabac du type à inhalation sans combustion, et produit de tabac du type à inhalation sans combustion |
CN104382223A (zh) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | 一种适用于配制果香型电子烟烟液的溶剂及其配制的烟液和电子烟 |
WO2015046420A1 (fr) | 2013-09-30 | 2015-04-02 | 日本たばこ産業株式会社 | Inhalateur de saveur sans combustion |
US10034988B2 (en) | 2012-11-28 | 2018-07-31 | Fontem Holdings I B.V. | Methods and devices for compound delivery |
US10194693B2 (en) | 2013-09-20 | 2019-02-05 | Fontem Holdings 1 B.V. | Aerosol generating device |
JP2021507684A (ja) * | 2017-12-20 | 2021-02-25 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 油添加剤を含むエアロゾル発生基体 |
WO2022185434A1 (fr) * | 2021-03-03 | 2022-09-09 | 日本たばこ産業株式会社 | Inhalateur d'arôme de type à chauffage sans combustion, et cartouche |
US11712059B2 (en) | 2020-02-24 | 2023-08-01 | Nicoventures Trading Limited | Beaded tobacco material and related method of manufacture |
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US10244786B2 (en) * | 2013-10-03 | 2019-04-02 | Altria Client Services Llc | Tobacco lozenge |
CN105054281B (zh) * | 2015-07-21 | 2016-11-23 | 中国烟草总公司广东省公司 | 一种气雾型口香烟 |
US20180368472A1 (en) * | 2017-06-21 | 2018-12-27 | Altria Client Services Llc | Encapsulated ingredients for e-vaping devices and method of manufacturing thereof |
CN109171021B (zh) * | 2018-08-22 | 2021-08-27 | 青岛颐中科技有限公司 | 电子烟吸烟机的供料*** |
EP4338603A2 (fr) * | 2019-10-28 | 2024-03-20 | JT International S.A. | Composition contenant du tabac générant un aérosol comprenant un triglycéride à chaîne moyenne |
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2013
- 2013-06-25 US US13/926,076 patent/US20130284193A1/en not_active Abandoned
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Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
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US10034988B2 (en) | 2012-11-28 | 2018-07-31 | Fontem Holdings I B.V. | Methods and devices for compound delivery |
WO2014104078A1 (fr) * | 2012-12-28 | 2014-07-03 | 日本たばこ産業株式会社 | Source de saveur pour produit de tabac du type à inhalation sans combustion, et produit de tabac du type à inhalation sans combustion |
CN103190705A (zh) * | 2013-04-01 | 2013-07-10 | 上海烟草集团有限责任公司 | 用于加热不燃烧装置的烟草制品及其制备方法 |
CN103169157A (zh) * | 2013-04-01 | 2013-06-26 | 上海烟草集团有限责任公司 | 加热不燃烧的香烟装置 |
CN103169157B (zh) * | 2013-04-01 | 2015-05-20 | 上海烟草集团有限责任公司 | 加热不燃烧的香烟装置 |
CN103190705B (zh) * | 2013-04-01 | 2015-05-20 | 上海烟草集团有限责任公司 | 用于加热不燃烧装置的烟草制品及其制备方法 |
US10194693B2 (en) | 2013-09-20 | 2019-02-05 | Fontem Holdings 1 B.V. | Aerosol generating device |
WO2015046420A1 (fr) | 2013-09-30 | 2015-04-02 | 日本たばこ産業株式会社 | Inhalateur de saveur sans combustion |
CN104382223A (zh) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | 一种适用于配制果香型电子烟烟液的溶剂及其配制的烟液和电子烟 |
JP2021507684A (ja) * | 2017-12-20 | 2021-02-25 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 油添加剤を含むエアロゾル発生基体 |
JP7408547B2 (ja) | 2017-12-20 | 2024-01-05 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 油添加剤を含むエアロゾル発生基体 |
US11712059B2 (en) | 2020-02-24 | 2023-08-01 | Nicoventures Trading Limited | Beaded tobacco material and related method of manufacture |
WO2022185434A1 (fr) * | 2021-03-03 | 2022-09-09 | 日本たばこ産業株式会社 | Inhalateur d'arôme de type à chauffage sans combustion, et cartouche |
Also Published As
Publication number | Publication date |
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RU2544152C1 (ru) | 2015-03-10 |
RU2013138739A (ru) | 2015-02-27 |
TWI457082B (zh) | 2014-10-21 |
EP2647299B1 (fr) | 2019-05-15 |
JPWO2012133289A1 (ja) | 2014-07-28 |
EP2647299A1 (fr) | 2013-10-09 |
US20130284193A1 (en) | 2013-10-31 |
CN103369980B (zh) | 2016-04-06 |
CN103369980A (zh) | 2013-10-23 |
TW201244651A (en) | 2012-11-16 |
ES2735537T3 (es) | 2019-12-19 |
EP2647299A4 (fr) | 2015-06-10 |
JP5489190B2 (ja) | 2014-05-14 |
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