WO2008071610A3 - Verfahren zur herstellung von katalysatoren und deren verwendung für die gasphasenoxidation von olefinen - Google Patents

Verfahren zur herstellung von katalysatoren und deren verwendung für die gasphasenoxidation von olefinen Download PDF

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Publication number
WO2008071610A3
WO2008071610A3 PCT/EP2007/063380 EP2007063380W WO2008071610A3 WO 2008071610 A3 WO2008071610 A3 WO 2008071610A3 EP 2007063380 W EP2007063380 W EP 2007063380W WO 2008071610 A3 WO2008071610 A3 WO 2008071610A3
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WO
WIPO (PCT)
Prior art keywords
olefins
gas phase
phase oxidation
producing catalysts
catalysts
Prior art date
Application number
PCT/EP2007/063380
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English (en)
French (fr)
Other versions
WO2008071610A2 (de
Inventor
Roland Heidenreich
Hans-Juergen Eberle
Johann Weis
Original Assignee
Wacker Chemie Ag
Roland Heidenreich
Hans-Juergen Eberle
Johann Weis
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wacker Chemie Ag, Roland Heidenreich, Hans-Juergen Eberle, Johann Weis filed Critical Wacker Chemie Ag
Priority to KR1020097011102A priority Critical patent/KR101124090B1/ko
Priority to EP07847868A priority patent/EP2106292A2/de
Priority to US12/518,520 priority patent/US8410014B2/en
Priority to CN2007800438404A priority patent/CN101541422B/zh
Priority to JP2009540720A priority patent/JP5087635B2/ja
Publication of WO2008071610A2 publication Critical patent/WO2008071610A2/de
Publication of WO2008071610A3 publication Critical patent/WO2008071610A3/de

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/48—Silver or gold
    • B01J23/52—Gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/58—Platinum group metals with alkali- or alkaline earth metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/60—Platinum group metals with zinc, cadmium or mercury
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0036—Grinding
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
    • C07C67/05—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds with oxidation
    • C07C67/055—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds with oxidation in the presence of platinum group metals or their compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/638—Pore volume more than 1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0205—Impregnation in several steps

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Die Erfindung betrifft ein Verfahren zur Herstellung von Katalysatoren auf stabilen, hochreinen Formkörpern aus pyrogenen Metalloxiden ohne Zusatz von Bindemitteln und deren Verwendung bei der Gasphasenoxidation von Olefinen.
PCT/EP2007/063380 2006-12-13 2007-12-06 Verfahren zur herstellung von katalysatoren und deren verwendung für die gasphasenoxidation von olefinen WO2008071610A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
KR1020097011102A KR101124090B1 (ko) 2006-12-13 2007-12-06 촉매의 제조 방법 및 올레핀의 기상 산화를 위한 이의 용도
EP07847868A EP2106292A2 (de) 2006-12-13 2007-12-06 Verfahren zur herstellung von katalysatoren und deren verwendung für die gasphasenoxidation von olefinen
US12/518,520 US8410014B2 (en) 2006-12-13 2007-12-06 Method for producing catalysts and their use for the gas phase oxidation of olefins
CN2007800438404A CN101541422B (zh) 2006-12-13 2007-12-06 制备催化剂的方法及其用于烯烃气相氧化的用途
JP2009540720A JP5087635B2 (ja) 2006-12-13 2007-12-06 触媒の製造方法及び触媒のオレフィン気相酸化のための使用

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102006058800A DE102006058800A1 (de) 2006-12-13 2006-12-13 Verfahren zur Herstellung von Katalysatoren und deren Verwendung für die Gasphasenoxidation von Olefinen
DE102006058800.2 2006-12-13

Publications (2)

Publication Number Publication Date
WO2008071610A2 WO2008071610A2 (de) 2008-06-19
WO2008071610A3 true WO2008071610A3 (de) 2008-09-12

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2007/063380 WO2008071610A2 (de) 2006-12-13 2007-12-06 Verfahren zur herstellung von katalysatoren und deren verwendung für die gasphasenoxidation von olefinen

Country Status (10)

Country Link
US (1) US8410014B2 (de)
EP (1) EP2106292A2 (de)
JP (1) JP5087635B2 (de)
KR (1) KR101124090B1 (de)
CN (1) CN101541422B (de)
DE (1) DE102006058800A1 (de)
RU (1) RU2447939C2 (de)
SA (1) SA07280669B1 (de)
SG (1) SG177197A1 (de)
WO (1) WO2008071610A2 (de)

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DE102011018532A1 (de) * 2011-04-26 2012-10-31 Süd-Chemie AG Basische Katalysatorträgerkörper mit niedriger Oberfläche
DE102011081786A1 (de) 2011-08-30 2013-02-28 Wacker Chemie Ag Verfahren zur Acetoxylierung von Olefinen in der Gasphase
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EP2106292A2 (de) 2009-10-07
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CN101541422B (zh) 2012-12-12
WO2008071610A2 (de) 2008-06-19
US20100022796A1 (en) 2010-01-28
SG177197A1 (en) 2012-01-30
US8410014B2 (en) 2013-04-02
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