WO2008052426A1 - Comprimé sucré à base de xylitol et son procédé de préparation - Google Patents
Comprimé sucré à base de xylitol et son procédé de préparation Download PDFInfo
- Publication number
- WO2008052426A1 WO2008052426A1 PCT/CN2007/003026 CN2007003026W WO2008052426A1 WO 2008052426 A1 WO2008052426 A1 WO 2008052426A1 CN 2007003026 W CN2007003026 W CN 2007003026W WO 2008052426 A1 WO2008052426 A1 WO 2008052426A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- xylitol
- sugar
- extract
- taste
- fragrance
- Prior art date
Links
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 title claims abstract description 212
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 title claims abstract description 212
- 239000000811 xylitol Substances 0.000 title claims abstract description 212
- 235000010447 xylitol Nutrition 0.000 title claims abstract description 212
- 229960002675 xylitol Drugs 0.000 title claims abstract description 212
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 title claims abstract description 209
- 235000009508 confectionery Nutrition 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title abstract description 6
- 235000000346 sugar Nutrition 0.000 claims abstract description 150
- 239000000843 powder Substances 0.000 claims abstract description 19
- 238000002156 mixing Methods 0.000 claims abstract description 18
- 239000004615 ingredient Substances 0.000 claims abstract description 15
- 235000015097 nutrients Nutrition 0.000 claims abstract description 13
- 229930003231 vitamin Natural products 0.000 claims abstract description 11
- 235000013343 vitamin Nutrition 0.000 claims abstract description 11
- 239000011782 vitamin Substances 0.000 claims abstract description 11
- 229940088594 vitamin Drugs 0.000 claims abstract description 11
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims abstract description 10
- 150000001413 amino acids Chemical class 0.000 claims abstract description 9
- 235000018927 edible plant Nutrition 0.000 claims abstract description 9
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 8
- 239000011707 mineral Substances 0.000 claims abstract description 8
- 235000010755 mineral Nutrition 0.000 claims abstract description 8
- 239000008158 vegetable oil Substances 0.000 claims abstract description 7
- 239000010775 animal oil Substances 0.000 claims abstract description 5
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 5
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 5
- 229960003080 taurine Drugs 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 80
- 239000000284 extract Substances 0.000 claims description 65
- 235000019640 taste Nutrition 0.000 claims description 59
- 244000269722 Thea sinensis Species 0.000 claims description 58
- 235000013616 tea Nutrition 0.000 claims description 52
- 239000003205 fragrance Substances 0.000 claims description 51
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 47
- 235000013824 polyphenols Nutrition 0.000 claims description 47
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 45
- 239000013078 crystal Substances 0.000 claims description 40
- 239000000796 flavoring agent Substances 0.000 claims description 34
- 239000007937 lozenge Substances 0.000 claims description 30
- 238000003756 stirring Methods 0.000 claims description 24
- 235000013355 food flavoring agent Nutrition 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 19
- 229940069765 bean extract Drugs 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 16
- 240000004922 Vigna radiata Species 0.000 claims description 15
- 235000010721 Vigna radiata var radiata Nutrition 0.000 claims description 15
- 235000011469 Vigna radiata var sublobata Nutrition 0.000 claims description 15
- 235000019634 flavors Nutrition 0.000 claims description 14
- 150000005846 sugar alcohols Chemical class 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 13
- 235000006468 Thea sinensis Nutrition 0.000 claims description 12
- 239000000419 plant extract Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 240000002853 Nelumbo nucifera Species 0.000 claims description 11
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims description 11
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims description 11
- 239000000049 pigment Substances 0.000 claims description 11
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 230000009286 beneficial effect Effects 0.000 claims description 7
- 235000020688 green tea extract Nutrition 0.000 claims description 7
- 229940094952 green tea extract Drugs 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 238000000465 moulding Methods 0.000 claims description 7
- 241000185686 Apocynum venetum Species 0.000 claims description 6
- 240000008397 Ganoderma lucidum Species 0.000 claims description 6
- 235000001637 Ganoderma lucidum Nutrition 0.000 claims description 6
- 241000241413 Propolis Species 0.000 claims description 6
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 6
- 244000299790 Rheum rhabarbarum Species 0.000 claims description 6
- 235000009411 Rheum rhabarbarum Nutrition 0.000 claims description 6
- 229940069521 aloe extract Drugs 0.000 claims description 6
- 235000020279 black tea Nutrition 0.000 claims description 6
- 125000000524 functional group Chemical group 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 235000020333 oolong tea Nutrition 0.000 claims description 6
- 229940069949 propolis Drugs 0.000 claims description 6
- 235000003687 soy isoflavones Nutrition 0.000 claims description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 6
- 241000208688 Eucommia Species 0.000 claims description 5
- 241001289529 Fallopia multiflora Species 0.000 claims description 5
- 239000003925 fat Substances 0.000 claims description 5
- 235000020717 hawthorn extract Nutrition 0.000 claims description 5
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 4
- 241000427159 Achyranthes Species 0.000 claims description 4
- 244000144730 Amygdalus persica Species 0.000 claims description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- 235000015197 apple juice Nutrition 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 238000005352 clarification Methods 0.000 claims description 4
- 235000013948 strawberry juice Nutrition 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- 238000004040 coloring Methods 0.000 claims description 3
- 235000019197 fats Nutrition 0.000 claims description 3
- 235000009569 green tea Nutrition 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 235000018102 proteins Nutrition 0.000 claims description 3
- 238000009923 sugaring Methods 0.000 claims description 3
- 150000008163 sugars Chemical class 0.000 claims description 3
- 239000002023 wood Substances 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- 241000282412 Homo Species 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- 240000005809 Prunus persica Species 0.000 claims description 2
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 2
- 229930003451 Vitamin B1 Natural products 0.000 claims description 2
- 229930003316 Vitamin D Natural products 0.000 claims description 2
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 claims description 2
- 229930003427 Vitamin E Natural products 0.000 claims description 2
- 229930003448 Vitamin K Natural products 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- -1 color Substances 0.000 claims description 2
- 235000015203 fruit juice Nutrition 0.000 claims description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- SHUZOJHMOBOZST-UHFFFAOYSA-N phylloquinone Natural products CC(C)CCCCC(C)CCC(C)CCCC(=CCC1=C(C)C(=O)c2ccccc2C1=O)C SHUZOJHMOBOZST-UHFFFAOYSA-N 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 229910052711 selenium Inorganic materials 0.000 claims description 2
- 239000011669 selenium Substances 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 229960003495 thiamine Drugs 0.000 claims description 2
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 claims description 2
- 235000010374 vitamin B1 Nutrition 0.000 claims description 2
- 239000011691 vitamin B1 Substances 0.000 claims description 2
- 235000019166 vitamin D Nutrition 0.000 claims description 2
- 239000011710 vitamin D Substances 0.000 claims description 2
- 150000003710 vitamin D derivatives Chemical class 0.000 claims description 2
- 235000019165 vitamin E Nutrition 0.000 claims description 2
- 229940046009 vitamin E Drugs 0.000 claims description 2
- 239000011709 vitamin E Substances 0.000 claims description 2
- 235000019168 vitamin K Nutrition 0.000 claims description 2
- 239000011712 vitamin K Substances 0.000 claims description 2
- 150000003721 vitamin K derivatives Chemical class 0.000 claims description 2
- 229940046008 vitamin d Drugs 0.000 claims description 2
- 229940046010 vitamin k Drugs 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims 1
- 241000205407 Polygonum Species 0.000 claims 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims 1
- 244000013123 dwarf bean Species 0.000 claims 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims 1
- 235000019155 vitamin A Nutrition 0.000 claims 1
- 239000011719 vitamin A Substances 0.000 claims 1
- 229940045997 vitamin a Drugs 0.000 claims 1
- 238000005266 casting Methods 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 3
- 150000003722 vitamin derivatives Chemical class 0.000 abstract description 3
- 239000000758 substrate Substances 0.000 abstract 2
- 235000013311 vegetables Nutrition 0.000 abstract 1
- 239000000047 product Substances 0.000 description 15
- 239000002245 particle Substances 0.000 description 4
- 235000005979 Citrus limon Nutrition 0.000 description 3
- 244000131522 Citrus pyriformis Species 0.000 description 3
- 229930006000 Sucrose Natural products 0.000 description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 3
- 235000019658 bitter taste Nutrition 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000000845 maltitol Substances 0.000 description 3
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 description 3
- 235000010449 maltitol Nutrition 0.000 description 3
- 229940035436 maltitol Drugs 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 239000005720 sucrose Substances 0.000 description 3
- 241000722949 Apocynum Species 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- SERLAGPUMNYUCK-DCUALPFSSA-N 1-O-alpha-D-glucopyranosyl-D-mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O SERLAGPUMNYUCK-DCUALPFSSA-N 0.000 description 1
- 241000283690 Bos taurus Species 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 241001464837 Viridiplantae Species 0.000 description 1
- 235000019631 acid taste sensations Nutrition 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- HEBKCHPVOIAQTA-NGQZWQHPSA-N d-xylitol Chemical compound OC[C@H](O)C(O)[C@H](O)CO HEBKCHPVOIAQTA-NGQZWQHPSA-N 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000000905 isomalt Substances 0.000 description 1
- 235000010439 isomalt Nutrition 0.000 description 1
- HPIGCVXMBGOWTF-UHFFFAOYSA-N isomaltol Natural products CC(=O)C=1OC=CC=1O HPIGCVXMBGOWTF-UHFFFAOYSA-N 0.000 description 1
- 210000003127 knee Anatomy 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 235000011888 snacks Nutrition 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/0056—Mouth soluble or dispersible forms; Suckable, eatable, chewable coherent forms; Forms rapidly disintegrating in the mouth; Lozenges; Lollipops; Bite capsules; Baked products; Baits or other oral forms for animals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
- A23G3/368—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins containing vitamins, antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/38—Sucrose-free products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Definitions
- the invention belongs to a lozenge, in particular to a xylitol confectionery lozenge and a preparation method thereof. - Background technique
- Low-energy confectionery has become the hotspot and development focus of today's international confectionery market. The market potential is huge and there is a trend to replace traditional cane candy.
- Low-energy confectionery is mainly based on xylitol.
- the candy made from xylitol is cooler and cooler than other "non-sucrose" candy. Its sweet taste is pure and has no bad aftertaste. Due to its special molecular structure, Maillard browning reaction does not occur.
- the saccharide body is stable in color, can withstand the high temperature during cooking, and is not easily decomposed.
- Xylitol has good storage properties and does not absorb moisture and moisture even when exposed to the atmosphere, prolonging the shelf life of its products.
- xylitol is not easily fermented by the oral bacterium of the sputum, inhibiting the growth of bacteria in the oral cavity, preventing the energy in the food from multiplying and producing harmful acid, and effectively preventing the occurrence of tooth decay.
- the object of the present invention is to provide a xylitol confectionery lozenge containing a medicine or edible plant powder, a medicine or edible plant extract, a vitamin, a protein, a mineral, and a fat. Functional ingredients such as sugar, vegetable oil or animal oil, amino acids, taurine and other nutrients beneficial to the human body.
- the base is 100% xylitol and has a good taste.
- Another object of the present invention is to provide a method for preparing two kinds of xylitol confectionery lozenges, wherein a preparation method comprises mixing functional components in xylitol melt to ensure xylitol and functional components Mixing and hooking; Another method of preparation, first prepare xylitol aqueous solution, then add functional components, often press sugar or vacuum sugar to ensure that xylitol and functional components are evenly mixed.
- the xylitol crystal structure is uniform in the products made by the two methods, the taste is pure, and the taste is good; the specific flavoring agent is selected, and the pH value of the candy is determined, which can be eliminated.
- the unpleasant taste of the general functional components the proper pouring temperature is found to ensure that the sugar liquid can be molded and industrialized.
- the present invention also explores the range of amounts of functional components added.
- the technical solution of the present invention is as follows:
- a xylitol confectionery lozenge characterized by comprising xylitol, a functional component and a toning, aroma and an odorant, the functional component comprising at least one or more of the following: Edible plant powder, medicinal or edible plant extracts, vitamins, proteins, minerals, fats, sugars, other sugar alcohols other than xylitol, vegetable oils or animal oils, amino acids, taurine and other nutrients beneficial to the human body.
- the xylitol confectionery lozenge characterized in that the weight ratio of each component is - xylitol 90-100
- the xylitol confectionery lozenge characterized in that the weight ratio of each component is - xylitol 95-98
- Toning, fragrance, 'flavoring amount Toning, fragrance, 'flavoring amount.
- the xylitol confectionery lozenge characterized in that the plant extract is selected from one or more of the following: green tea extract, black tea extract, oolong tea extract, jasmine tea extract, tea Polyphenols, mung bean extract, rhubarb extract, lotus leaf extract, aloe extract, soy isoflavones, propolis, ganoderma lucidum, hawthorn extract, Polygonum multiflorum extract, lotus leaf extract, peach kernel extract, Eucommia extract, cattle Knee extract, apocynum extract, fruit juice; the vitamins are vitamin 4, vitamin B1, B2, B6, B12, vitamins (:, vitamin D, vitamin E, vitamin K, the amino acids are 20 kinds of human body The desired amino acid, the mineral is potassium, sodium, calcium, zinc, iron, selenium, the vegetable oil is not full And fatty acids, the nutrients beneficial to the human body are other functional factors not mentioned.
- the plant extract is selected from one or more of the following: green tea extract, black tea extract,
- the xylitol confectionery lozenge is characterized in that the weight ratio of the components is: (1) xylitol 90-99.5 green tea 0.01-2 green tea extract 0.1-5, tea Phenol 0.01-1, mung bean extract 0.1-2, color, fragrance, taste
- the xylitol confectionery lozenge characterized in that the flavoring agent is citric acid.
- a method for preparing a xylitol confectionery lozenge comprising the steps of:
- the pouring step is: adding xylitol seed crystals to the sugar liquid or stirring and stirring with a stirrer to produce a seed crystal, and the xylitol sugar liquid is cooled to a temperature of 8 (TC to 92 ° C) to start pouring.
- the pouring step adding xylitol seed crystals to the sugar liquid or stirring the sugar liquid with a stirrer to produce a seed crystal, and the xylitol sugar liquid is cooled to a temperature of 85 ° C to 90 ° C, and then poured.
- the chemical sugar and the functional component are mixed in the following manner:
- the above functional group may be dispensed into an aqueous solution or pulverized into a powder to be added;
- the xylitol sugar solution after mixing the functional components has a final water content of not more than 2%.
- the present invention also provides another method for preparing a xylitol confectionery lozenge, which comprises the following steps:
- the vacuum sugar is: the obtained sugar liquid is put into a vacuum sugar machine for vacuum sugaring, the degree of vacuum is -0.60 ⁇ - 0. 090Mpa, the sugar temperature is 110-160 ° C and higher than the wood The boiling point of the sugar alcohol liquid, after the end of the sugar, the sugar liquid is driven into the ingredient tank;
- the xylitol sugar liquid is completely melted and clarified, the remaining functional components are added, and the mixture is uniformly mixed; the xylitol sugar liquid mixed with the functional component has a final water content of not more than 2 %;
- the pouring step is: adding xylitol seed crystals to the sugar liquid or stirring and stirring with a stirrer to produce a seed crystal, and the xylitol sugar liquid is cooled to a temperature of 80 ° C to 92 ° C to start pouring.
- the pouring step adding xylitol seed crystals to the sugar liquid or stirring the sugar liquid with a stirrer to produce a seed crystal, and the xylitol sugar liquid is cooled to a temperature of 85 ° C to 90 ° C and poured.
- the particle size is 150 - 1000 mesh.
- the xylitol has a purity of 98.5% or more.
- the toner of the present invention is a pigment, the flavoring agent is a flavor, and the flavoring agent is preferably citric acid.
- the amount of the flavoring agent is 0. 2-1. 5%.
- the amount of the flavoring agent is 0. 2-1. 5%.
- the present invention simultaneously adds a part of functional components which are either non-heat-sensitive components or belong to components having a large water content.
- the remaining functional components added during the compounding step are generally heat sensitive components, or components having a lower water content.
- the basic principle of the production process of the present invention is to change the fine crystal of the sugar alcohol into a coarse crystal.
- the xylitol which is basically used in the actual production of the invention is of pharmaceutical grade, and the purity of xylitol is above 98.5%, such wood Sugar alcohol is a high-purity xylitol.
- the high-purity xylitol powder is mixed with functional components such as plant extracts or other nutrients, and then thawed and recrystallized, which is equivalent to evenly adding in the pure crystal of xylitol.
- the impurities are recrystallized to become coarse crystals.
- the homogeneity of the taste of the product becomes a prominent problem after the xylitol is mixed with the functional component.
- the present invention controls the weight ratio of xylitol to the functional component, the addition form and the particle size of the functional component, Timing of addition: uniform mixing in the molten state of xylitol, organically combining functional components in the smallest unit of xylitol crystals, the product becomes a solid continuous phase, avoiding powder additives in xylitol solution
- the problem of uneven dispersion also avoids the phenomenon that liquid additives are easily agglomerated in solid xylitol particles; and the conditions of casting, in the casting step of the present invention, the preferred choice is: sugar liquid temperature 85-90° C, sugar liquid moisture 0.8-1.5%, so that the crystal particles in the product can be uniform in size, does not affect the taste.
- it is also required to make the casting temperature, mold temperature, cooling temperature and demoulding time uniform during the
- the content of xylitol in the final product ranges from 92 to 99.5%, while moisture and addition
- the functional components and the total content of the toning, aroma and taste agents are below 8%; the preferred composition is: xylitol 96-98%, moisture and added functional components and color, fragrance, taste
- the total content of the agent is below 4%.
- the preferred flavoring agent of the present invention is citric acid, because a general plant extract may have a bitter taste. After being added to xylitol, the mouthfeel is not good, and it is difficult for consumers to accept, and it is difficult to commercialize.
- the present invention has been repeatedly explored. Experiments, using citric acid as a flavoring agent, can well cover the sweetness of xylitol, and the bitter taste of plant extracts, and the palatability is greatly improved, which is favored by consumers. It has made it possible to commercialize functional components in xylitol, opening up a new field of xylitol health foods, enabling people to enjoy the sweetness of xylitol without the side effects of long-term consumption of ordinary sucrose.
- the existing manufacturers of isomalt and maltitol sugar products cannot only overcome the bitter taste of tea polyphenols, and the amount of tea polyphenol added in the product can only be a few ten thousandths, and the present invention passes the lemon.
- the acid taste, the amount of tea polyphenols can be more than one percent, so that people can absorb the nutrients of tea while eating xylitol sugar, which is good for human health.
- the pH of the xylitol sugar is generally 2.5-3.5.
- the pouring temperature of the present invention is 2 to 10 Torr lower than the pouring temperature of the single xylitol component depending on the added substance. Since the temperature of the casting is lowered, the added heat sensitive component is less damaged, the volatile component is relatively less lost, and the color, fragrance and taste of the product are better.
- the xylitol confectionery lozenge of the invention is a healthy snack food, which is based on xylitol and adds green Plant extracts such as tea extract, mung bean extract, and lotus leaf extract can be added with vitamins, minerals, and various functional factors and nutrients. Since xylitol has a natural sweetness comparable to sucrose, a candy made from xylitol has a pleasant sweetness, but xylitol itself does not have good nutritional value. It has 60% of the metabolism produces heat, and there is no other nutritional and health value other than it. Therefore, various plant extracts or other nutrients with nutrients or health functions are added to the xylitol confectionery lozenges, and then passed through the lemon.
- Plant extracts such as tea extract, mung bean extract, and lotus leaf extract
- Acid flavor, with fragrance and color treatment so that the product not only has a refreshing taste, rich natural plant aroma, sweet and pleasant, but also has low calorie, no sugar, no fat, fresh breath, anti-oxidation and other health care functions, and thus Meet the health and leisure trends of modern fast-paced society.
- Xylitol confectionery lozenges containing medicated or edible plant powders, medicated or edible plant extracts, vitamins, proteins, minerals, fats, sugars, vegetable oils or animal oils, amino acids, taurine and others beneficial to humans
- Functional components such as nutrients, 100% of the matrix is xylitol, and the taste is good.
- the invention mixes functional components in the xylitol melt, ensures that the xylitol and the functional components are uniformly mixed, the crystal structure is hooked, and the taste is pure; the specific flavoring agent is selected, and the pH value of the candy is determined, In addition to the unpleasant taste of the general functional components; the proper pouring temperature is found to ensure that the sugar liquid can be cast and molded to achieve industrial production.
- Citric acid 1. 25kg
- the xylitol, tea polyphenol, citric acid, and pigment in the above formula were weighed according to the prescribed amount, and mixed in a trough mixer, transferred to a sugar pot, and then added 0.5- 2% water.
- the steam was heated to slowly melt the mixture to a clear state and stirred. When the temperature reached 122 ⁇ , the steam was turned off.
- the prepared sugar liquid is placed in a small barrel in a batch, and seed crystals are added or stirred to produce a seed crystal, and the temperature of the sugar liquid is 85 ° C to 90 ° C, and poured.
- Xylitol with a purity of 98.5% or more is weighed according to the formula, and the xylitol is completely melted and clarified (heated to %- ⁇ 22 ⁇ ) with functional components (except xylitol and toning, fragrance, and flavoring). All components are mixed and can be used in the following three ways: The following methods are used:
- the sugar liquid is filtered through an 80 mesh sieve and then driven into a storage tank, and the mixture is stirred to prepare a vacuum sugar.
- the liquid in the liquid storage tank is preheated by a preheater, and then pressed by a vacuum sugar machine. 2MPa,
- the steam pressure of the steam is 0. 2MPa
- the steam pressure of the preheater is 0. 3 ⁇ 0. 4MPa
- the steam pressure of the insulation is 0. 2MPa.
- the vacuum slowly rises to -0.65Mpa), when the temperature and vacuum of the sugar reach the set value (parameter: vacuum sugar temperature 145 ° C ⁇ 148 ° C, vacuum degree 0. 065 MPa), keep this temperature and The vacuum was cycled for 5 minutes.
- the prepared sugar liquid is placed in a small barrel in a batch, stirred until the temperature of the sugar liquid is 86 ° C ⁇ 88 O (reference value, observe the crystallization of the sugar liquid), set three temperature parameters and the pouring speed to start according to the regulations Specification pouring. If the sugar solution fails to cool down in time and does not guarantee the pouring requirement, a small amount of seed crystals may be added and the hook is stirred to promote crystallization. When paying attention, observe the time when the sugar liquid starts to crystallize after casting and the molding condition, and adjust the pouring temperature or speed parameter in time.
- Normal pressure sugar or vacuum sugar can be used.
- the vacuum sugar is: the obtained sugar liquid is put into a vacuum sugar machine for vacuum sugaring, the degree of vacuum is -0. 060 ⁇ - 0. 090Mpa, the sugar temperature is 110-160O and higher than xylitol The boiling point of the liquid, when the moisture of the sugar liquid does not exceed 2%, the sugar liquid is driven into the ingredient tank;
- the xylitol sugar liquid is completely melted and clarified and mixed with the remaining functional component powder;
- the xylitol sugar solution after mixing the functional components, the final water content is not more than 2%, preferably water The amount is 0. 8-1. 5%;
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Abstract
La présente invention concerne un comprimé sucré à base de xylitol et son procédé de préparation, lequel comprend l'utilisation de xylitol en tant que substrat, l'addition d'ingrédients fonctionnels tels qu'une poudre médicinale ou comestible, un extrait de plante médicinale ou comestible, une vitamine, une protéine, une substance minérale, une matière grasse, du sucre, une huile végétale ou animale, un acide aminé, de la taurine, d'autres aliments, etc. Le xylitol compris dans le substrat est du xylitol à 100 % en poids. On mélange le xylitol avec des ingrédients fonctionnels lorsque le xylitol est fondu et limpide et on le coule lorsque la température est chauffée dans une gamme de 85 à 90 °C de façon à obtenir le produit fini.
Applications Claiming Priority (4)
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CN200610097529A CN1957732B (zh) | 2006-11-03 | 2006-11-03 | 一种木糖醇硬糖及其制作方法 |
CN200610097529.5 | 2006-11-03 | ||
CNA2007101338000A CN101411378A (zh) | 2007-10-16 | 2007-10-16 | 一种木糖醇糖果类含片及其制作方法 |
CN200710133800.0 | 2007-10-16 |
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WO2008052426A1 true WO2008052426A1 (fr) | 2008-05-08 |
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PCT/CN2007/003026 WO2008052426A1 (fr) | 2006-11-03 | 2007-10-23 | Comprimé sucré à base de xylitol et son procédé de préparation |
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WO2009118589A3 (fr) * | 2008-03-24 | 2010-01-14 | Wockhardt Research Centre | Compositions orodispersibles de rhéine ou de diacéréine |
CN114468104A (zh) * | 2021-12-30 | 2022-05-13 | 潘哒鲁鲁(深圳)生物科技有限公司 | 具有特效调节胃肠作用的功能性糖果及其工业化生产方法 |
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WO2009118589A3 (fr) * | 2008-03-24 | 2010-01-14 | Wockhardt Research Centre | Compositions orodispersibles de rhéine ou de diacéréine |
CN114468104A (zh) * | 2021-12-30 | 2022-05-13 | 潘哒鲁鲁(深圳)生物科技有限公司 | 具有特效调节胃肠作用的功能性糖果及其工业化生产方法 |
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