TWI455976B - 遮光型水溶性樹脂組成物 - Google Patents
遮光型水溶性樹脂組成物 Download PDFInfo
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- TWI455976B TWI455976B TW097121155A TW97121155A TWI455976B TW I455976 B TWI455976 B TW I455976B TW 097121155 A TW097121155 A TW 097121155A TW 97121155 A TW97121155 A TW 97121155A TW I455976 B TWI455976 B TW I455976B
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- dyes
- water
- protective film
- soluble resin
- organic semiconductor
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- 239000011342 resin composition Substances 0.000 title claims 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims 4
- 239000010408 film Substances 0.000 claims 25
- 239000000975 dye Substances 0.000 claims 21
- 230000001681 protective effect Effects 0.000 claims 17
- 239000004065 semiconductor Substances 0.000 claims 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 4
- 239000011347 resin Substances 0.000 claims 4
- 229920005989 resin Polymers 0.000 claims 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- -1 acetylene glycols Chemical class 0.000 claims 3
- 150000001298 alcohols Chemical class 0.000 claims 3
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims 3
- 239000011229 interlayer Substances 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 claims 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 2
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 claims 2
- 239000000987 azo dye Substances 0.000 claims 2
- LZCLXQDLBQLTDK-UHFFFAOYSA-N ethyl 2-hydroxypropanoate Chemical compound CCOC(=O)C(C)O LZCLXQDLBQLTDK-UHFFFAOYSA-N 0.000 claims 2
- XLLIQLLCWZCATF-UHFFFAOYSA-N ethylene glycol monomethyl ether acetate Natural products COCCOC(C)=O XLLIQLLCWZCATF-UHFFFAOYSA-N 0.000 claims 2
- CATSNJVOTSVZJV-UHFFFAOYSA-N heptan-2-one Chemical compound CCCCCC(C)=O CATSNJVOTSVZJV-UHFFFAOYSA-N 0.000 claims 2
- 150000002596 lactones Chemical class 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- JOLQKTGDSGKSKJ-UHFFFAOYSA-N 1-ethoxypropan-2-ol Chemical compound CCOCC(C)O JOLQKTGDSGKSKJ-UHFFFAOYSA-N 0.000 claims 1
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 claims 1
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 claims 1
- SVONRAPFKPVNKG-UHFFFAOYSA-N 2-ethoxyethyl acetate Chemical compound CCOCCOC(C)=O SVONRAPFKPVNKG-UHFFFAOYSA-N 0.000 claims 1
- BCHZICNRHXRCHY-UHFFFAOYSA-N 2h-oxazine Chemical compound N1OC=CC=C1 BCHZICNRHXRCHY-UHFFFAOYSA-N 0.000 claims 1
- LPEKGGXMPWTOCB-UHFFFAOYSA-N 8beta-(2,3-epoxy-2-methylbutyryloxy)-14-acetoxytithifolin Natural products COC(=O)C(C)O LPEKGGXMPWTOCB-UHFFFAOYSA-N 0.000 claims 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- 239000004372 Polyvinyl alcohol Substances 0.000 claims 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims 1
- 229920002125 Sokalan® Polymers 0.000 claims 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 1
- KVXNKFYSHAUJIA-UHFFFAOYSA-N acetic acid;ethoxyethane Chemical compound CC(O)=O.CCOCC KVXNKFYSHAUJIA-UHFFFAOYSA-N 0.000 claims 1
- 239000000999 acridine dye Substances 0.000 claims 1
- 150000001335 aliphatic alkanes Chemical class 0.000 claims 1
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims 1
- 239000001000 anthraquinone dye Substances 0.000 claims 1
- 150000004056 anthraquinones Chemical class 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims 1
- 125000005626 carbonium group Chemical group 0.000 claims 1
- 229940125898 compound 5 Drugs 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims 1
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical compound C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 claims 1
- ODQWQRRAPPTVAG-GZTJUZNOSA-N doxepin Chemical compound C1OC2=CC=CC=C2C(=C/CCN(C)C)/C2=CC=CC=C21 ODQWQRRAPPTVAG-GZTJUZNOSA-N 0.000 claims 1
- 229940116333 ethyl lactate Drugs 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 229940057867 methyl lactate Drugs 0.000 claims 1
- 239000001005 nitro dye Substances 0.000 claims 1
- 239000001006 nitroso dye Substances 0.000 claims 1
- 239000001007 phthalocyanine dye Substances 0.000 claims 1
- 229920000083 poly(allylamine) Polymers 0.000 claims 1
- 239000004584 polyacrylic acid Substances 0.000 claims 1
- 229920002451 polyvinyl alcohol Polymers 0.000 claims 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 1
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 239000001008 quinone-imine dye Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 239000001016 thiazine dye Substances 0.000 claims 1
- 239000001017 thiazole dye Substances 0.000 claims 1
- 239000010409 thin film Substances 0.000 claims 1
- JOUDBUYBGJYFFP-FOCLMDBBSA-N thioindigo Chemical compound S\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2S1 JOUDBUYBGJYFFP-FOCLMDBBSA-N 0.000 claims 1
- AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 claims 1
- 239000001018 xanthene dye Substances 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
- C08L101/12—Compositions of unspecified macromolecular compounds characterised by physical features, e.g. anisotropy, viscosity or electrical conductivity
- C08L101/14—Compositions of unspecified macromolecular compounds characterised by physical features, e.g. anisotropy, viscosity or electrical conductivity the macromolecular compounds being water soluble or water swellable, e.g. aqueous gels
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L29/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
- C08L29/02—Homopolymers or copolymers of unsaturated alcohols
- C08L29/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L39/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions of derivatives of such polymers
- C08L39/04—Homopolymers or copolymers of monomers containing heterocyclic rings having nitrogen as ring member
- C08L39/06—Homopolymers or copolymers of N-vinyl-pyrrolidones
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/1333—Constructional arrangements; Manufacturing methods
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L29/00—Semiconductor devices specially adapted for rectifying, amplifying, oscillating or switching and having potential barriers; Capacitors or resistors having potential barriers, e.g. a PN-junction depletion layer or carrier concentration layer; Details of semiconductor bodies or of electrodes thereof ; Multistep manufacturing processes therefor
- H01L29/66—Types of semiconductor device ; Multistep manufacturing processes therefor
- H01L29/68—Types of semiconductor device ; Multistep manufacturing processes therefor controllable by only the electric current supplied, or only the electric potential applied, to an electrode which does not carry the current to be rectified, amplified or switched
- H01L29/76—Unipolar devices, e.g. field effect transistors
- H01L29/772—Field effect transistors
- H01L29/78—Field effect transistors with field effect produced by an insulated gate
- H01L29/786—Thin film transistors, i.e. transistors with a channel being at least partly a thin film
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- Thin Film Transistor (AREA)
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Claims (13)
- 一種有機半導體保護膜用水溶性樹脂組成物,該有機半導體保護膜係形成於有機半導體膜及層間絕緣膜之間,且該組成物包含:a)水溶性樹脂100重量份;b)水溶性染料化合物5至50重量份;及c)溶劑,其係i)水或ii)水及可溶解於水的有機溶劑之混合物,且其係被包含以使組成物總量中之固形物含量達3至60重量%。
- 如申請專利範圍第1項之有機半導體保護膜用水溶性樹脂組成物,係相對於水溶性樹脂100重量份更包含水溶性界面活性劑0.0001至2重量份。
- 如申請專利範圍第1項之有機半導體保護膜用水溶性樹脂組成物,其中該水溶性樹脂係選自於由聚乙烯醇、聚乙烯吡咯啶酮、聚丙烯酸、聚乙亞胺、聚環氧乙烷、聚乙烯胺、聚烯丙胺及其等之衍生物所組成之群之1種以上。
- 如申請專利範圍第1項之有機半導體保護膜用水溶性樹脂組成物,其中該水溶性樹脂具有1,000至300,000之聚苯乙烯換算重量平均分子量(Mw)。
- 如申請專利範圍第1項之有機半導體保護膜用水溶性樹脂組成物,其中該水溶性染料化合物係選自於由偶氮染料(Azo dyes)、重氮染料(Diazo dyes)、蒽醌染料(Anthraquinone dyes)、靛屬染料(Indigoid dyes)、靛藍系 染料(Indigo dyes)、硫靛系染料(Thioindigo dyes)、離子型染料(Carbonium dyes)、二苯甲烷系染料(Diphenylmethane dyes)、三苯甲烷系染料(Triphenylmethane dyes)、二苯并哌喃系染料(Xanthene dyes)、吖啶系染料(Acridine dyes)、酞青染料(Phthalocyanine dyes)、次甲基染料(Methine dyes)、聚次甲基系染料(Polymethine dyes)、次甲基偶氮系染料(Azomethine dyes)、噻唑染料(Thiazole dyes)、醌亞胺染料(Quinoneimine dyes)、吖嗪系染料(Azine dyes)、噁系染料(Oxazine dyes)、噻系染料(Thiazine dyes)、內酯染料(Lactone dyes)、胺酮染料(Amino Ketone dyes)、羥基酮染料(Hydroxy ketone dyes)、硝基染料(Nitro dyes)、亞硝基染料(Nitroso dyes)及喹啉染料(Quinoline dyes)所組成之群之1種以上。
- 如申請專利範圍第2項之有機半導體保護膜用水溶性樹脂組成物,其中該水溶性界面活性劑係選自於由乙炔醇、乙炔二醇、乙炔醇之聚乙氧基醇及乙炔二醇之聚乙氧基醇所組成之群之1種以上。
- 如申請專利範圍第1項之有機半導體保護膜用水溶性樹脂組成物,其中該有機溶劑係選自於由甲醇、乙醇、異丙醇、丙酮、甲基乙基酮、2-庚酮、環己酮、乙酸甲酯、乙酸乙酯、乙二醇一甲基醚、乙二醇一乙基醚、乙二醇一甲基醚乙酸酯、乙二醇一乙基醚乙酸酯、丙二醇一甲基醚、丙二醇一乙基醚、丙二醇一甲基醚乙酸酯、丙二 醇一乙基醚乙酸酯、乳酸甲酯、乳酸乙酯、甲苯、二甲苯、N,N-二甲基乙醯胺及N-甲基吡咯啶酮所組成之群之1種以上。
- 一種有機電性元件,係於有機半導體膜與層間絕緣膜間含有使申請專利範圍第1至7項中任一項之有機半導體保護膜用水溶性樹脂組成物硬化形成之保護膜者。
- 如申請專利範圍第8項之有機電性元件,其中該保護膜係將樹脂組成物塗佈於有機半導體膜上後,以80~150℃之溫度進行40~100分鐘之硬化而得者。
- 如申請專利範圍第8項之有機電性元件,其中該保護膜具有0.05至0.2微米之厚度。
- 如申請專利範圍第8項之有機電性元件,該有機電性元件係有機薄膜電晶體(OTFO,organic thin-film transistor)、具有可撓性之顯示器(flexible display)或有機電性發光元件(OLED,organic light-emitting device)。
- 一種有機電性元件之製造方法,包含一將申請專利範圍第1至7項中任一項之有機半導體保護膜用水溶性樹脂組成物塗佈於有機半導體膜上後,經硬化形成保護膜,並於前述保護膜上形成層間絕緣膜之步驟。
- 如申請專利範圍第12項之有機電性元件之製造方法,其中該保護膜係將前述有機半導體保護膜用水溶性樹脂組成物塗佈於有機半導體膜上後,以80~150℃之溫度進行40~100分鐘之硬化而得者。
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KR20070055699A KR101482652B1 (ko) | 2007-06-07 | 2007-06-07 | 유기반도체 보호막 조성물 |
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TW200909502A TW200909502A (en) | 2009-03-01 |
TWI455976B true TWI455976B (zh) | 2014-10-11 |
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JP (1) | JP5538689B2 (zh) |
KR (1) | KR101482652B1 (zh) |
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