RU99124399A - MULTI-PHASE FILLER CONTAINING CARBON AND WAYS OF ITS PRODUCTION - Google Patents
MULTI-PHASE FILLER CONTAINING CARBON AND WAYS OF ITS PRODUCTIONInfo
- Publication number
- RU99124399A RU99124399A RU99124399/12A RU99124399A RU99124399A RU 99124399 A RU99124399 A RU 99124399A RU 99124399/12 A RU99124399/12 A RU 99124399/12A RU 99124399 A RU99124399 A RU 99124399A RU 99124399 A RU99124399 A RU 99124399A
- Authority
- RU
- Russia
- Prior art keywords
- filler
- feedstock
- silicon
- carbon
- carbon black
- Prior art date
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims 88
- 239000000945 filler Substances 0.000 title claims 71
- 229910052799 carbon Inorganic materials 0.000 title claims 36
- 239000000203 mixture Substances 0.000 claims 48
- 239000006229 carbon black Substances 0.000 claims 31
- 239000002994 raw material Substances 0.000 claims 22
- 239000004071 soot Substances 0.000 claims 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 19
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 18
- 229910052710 silicon Inorganic materials 0.000 claims 18
- 239000010703 silicon Substances 0.000 claims 18
- 239000000126 substance Substances 0.000 claims 15
- 229910052751 metal Inorganic materials 0.000 claims 13
- 239000002184 metal Substances 0.000 claims 13
- 239000002210 silicon-based material Substances 0.000 claims 12
- 150000001875 compounds Chemical class 0.000 claims 10
- 239000003085 diluting agent Substances 0.000 claims 10
- 229920001971 elastomer Polymers 0.000 claims 9
- 239000000377 silicon dioxide Substances 0.000 claims 9
- 150000003377 silicon compounds Chemical class 0.000 claims 8
- 239000000806 elastomer Substances 0.000 claims 7
- 238000005299 abrasion Methods 0.000 claims 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 4
- 125000000962 organic group Chemical group 0.000 claims 4
- 238000005096 rolling process Methods 0.000 claims 4
- 235000012239 silicon dioxide Nutrition 0.000 claims 4
- 229920001577 copolymer Polymers 0.000 claims 3
- -1 ethylene, propylene Chemical group 0.000 claims 3
- 229920003048 styrene butadiene rubber Polymers 0.000 claims 3
- 239000002174 Styrene-butadiene Substances 0.000 claims 2
- 239000011230 binding agent Substances 0.000 claims 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 claims 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- 239000002245 particle Substances 0.000 claims 2
- 239000005060 rubber Substances 0.000 claims 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- SDJHPPZKZZWAKF-UHFFFAOYSA-N 2,3-dimethylbuta-1,3-diene Chemical compound CC(=C)C(C)=C SDJHPPZKZZWAKF-UHFFFAOYSA-N 0.000 claims 1
- VHOQXEIFYTTXJU-UHFFFAOYSA-N 2-methylbuta-1,3-diene;2-methylprop-1-ene Chemical compound CC(C)=C.CC(=C)C=C VHOQXEIFYTTXJU-UHFFFAOYSA-N 0.000 claims 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N Cesium Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
- 229920000181 Ethylene propylene rubber Polymers 0.000 claims 1
- 240000008528 Hevea brasiliensis Species 0.000 claims 1
- QEFYFXOXNSNQGX-UHFFFAOYSA-N Neodymium Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 claims 1
- 229910052779 Neodymium Inorganic materials 0.000 claims 1
- 239000005062 Polybutadiene Substances 0.000 claims 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminum Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 230000000111 anti-oxidant Effects 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 claims 1
- 239000003963 antioxidant agent Substances 0.000 claims 1
- 229910052788 barium Inorganic materials 0.000 claims 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium(0) Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims 1
- 239000007767 bonding agent Substances 0.000 claims 1
- 150000001639 boron compounds Chemical class 0.000 claims 1
- NTXGQCSETZTARF-UHFFFAOYSA-N buta-1,3-diene;prop-2-enenitrile Chemical compound C=CC=C.C=CC#N NTXGQCSETZTARF-UHFFFAOYSA-N 0.000 claims 1
- KAKZBPTYRLMSJV-UHFFFAOYSA-N butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims 1
- 229920005549 butyl rubber Polymers 0.000 claims 1
- 229910052792 caesium Inorganic materials 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
- 239000011651 chromium Substances 0.000 claims 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 1
- 229910052803 cobalt Inorganic materials 0.000 claims 1
- 239000010941 cobalt Substances 0.000 claims 1
- 150000001993 dienes Chemical class 0.000 claims 1
- 239000000839 emulsion Substances 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 125000000524 functional group Chemical group 0.000 claims 1
- 229920001519 homopolymer Polymers 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- VQTUBCCKSQIDNK-UHFFFAOYSA-N isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 1
- 239000011733 molybdenum Substances 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 239000000178 monomer Substances 0.000 claims 1
- 229920001194 natural rubber Polymers 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 229920002857 polybutadiene Polymers 0.000 claims 1
- 229920001195 polyisoprene Polymers 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 230000003014 reinforcing Effects 0.000 claims 1
- 229910052714 tellurium Inorganic materials 0.000 claims 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims 1
- 229910052718 tin Inorganic materials 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N tin hydride Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium(0) Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 1
- 239000003039 volatile agent Substances 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
Claims (93)
a) введение первого исходного сырья в первую ступень многоступенчатого реактора;
b) введение, по меньшей мере, одного из других видов исходного сырья в упомянутый многоступенчатый реактор в месте после упомянутой первой ступени, в котором, по меньшей мере, один из видов исходного сырья содержит смесь расщепляемых или летучих соединений, содержащих кремний, и углеродного сырья для получения сажи;
c) действие упомянутого реактора при температуре, достаточной для разложения упомянутого содержащего кремний соединения и для пиролиза упомянутого углеродного сырья для получения сажи, для образования упомянутого наполнителя;
d) извлечение упомянутого наполнителя.1. A method of obtaining a filler containing a carbon phase and a phase containing silicon substances, comprising the steps of:
a) introducing the first feedstock into the first stage of a multi-stage reactor;
b) introducing at least one of the other types of feedstock into said multi-stage reactor at a location after said first step, in which at least one of the feedstocks comprises a mixture of fissionable or volatile compounds containing silicon and carbon feed to obtain soot;
c) operating said reactor at a temperature sufficient to decompose said silicon-containing compound and to pyrolyze said carbon raw material to produce carbon black, to form said filler;
d) recovering said filler.
a) введение первого исходного сырья в первую ступень многоступенчатого реактора;
b) введение, по меньшей мере, одного из других видов исходного сырья в упомянутый многоступенчатый реактор в месте после упомянутой первой ступени, в котором
по меньшей мере, одно исходное сырья содержит углеродное сырье для получения сажи;
по меньшей мере, одно исходное сырье содержит, по меньшей мере, одно расщепляемое или летучее соединение, содержащее металл;
и, необязательно, по меньшей мере, одно исходное сырье, кроме того, содержит расщепляемое или летучее содержащее кремний соединение;
c) действие упомянутого реактора при температуре, достаточной для разложения или испарения упомянутого содержащего металл соединения, для пиролиза упомянутого углеродного сырья для получения сажи и для разложения или испарения упомянутого содержащего кремний соединения, если оно присутствует, для образования наполнителя;
d) извлечение упомянутого наполнителя.25. A method of producing a filler containing a carbon phase, a phase of a metal-containing substance and, optionally, a phase of a silicon-containing substance, said method comprising the steps of:
a) introducing the first feedstock into the first stage of a multi-stage reactor;
b) introducing at least one of the other types of feedstock into said multi-stage reactor at a location after said first stage, in which
at least one feedstock contains carbon raw materials for carbon black;
at least one feedstock contains at least one cleavable or volatile metal-containing compound;
and optionally at least one feedstock further comprises a cleavable or volatile silicon-containing compound;
c) operating said reactor at a temperature sufficient to decompose or vaporize said metal-containing compound, to pyrolyze said carbon raw material to produce carbon black, and to decompose or vaporize said silicon-containing compound, if present, to form a filler;
d) recovering said filler.
a) углеродное сырье для получения сажи;
b) по меньшей мере, одно расщепляемое или летучее соединение, содержащее металл; и, необязательно,
c) расщепляемое или летучее содержащее кремний соединение;
и кроме того, такие виды сырья в совокупности включают по меньшей мере углеродное сырье для получения сажи и по меньшей мере одно расщепляемое или летучее соединение, содержащее металл.35. The method according A.25, comprising at least three stages, when the feedstock is introduced into the aforementioned multi-stage reactor, in which the feedstock at each stage includes at least one of:
a) carbon raw materials for carbon black;
b) at least one cleavable or volatile metal-containing compound; and optionally
c) a cleavable or volatile silicon-containing compound;
and further, such feedstocks together include at least carbon black for carbon black and at least one fissile or volatile metal-containing compound.
a) разностью между площадью BET (N2) поверхности и t-площадью поверхности приблизительно 2 - 100 м2/г;
b) разностью между площадью BET (N2) поверхности и t-площадью поверхности приблизительно 1 - 50 м2/г после обработки HF;
c) отношением приблизительно 0,1 - 10 на основании 1) разности площадей BET (N2 ) поверхности у наполнителя после обработки и перед обработкой HF к 2) содержанию кремния в весовых процентах в упомянутом наполнителе без обработки HF;
d) уменьшением средневзвешенного размера частиц наполнителя, измеренного с помощью дискового центрифугирующего фотоседиментометра (DCP), после обработки HF приблизительно 5 - 40% по сравнению со средневзвешенным размером частиц наполнителя без обработки HF;
e) содержанием золы двуокиси кремния в упомянутом наполнителе приблизительно 0,05 - 1% на основе веса упомянутого наполнителя после обработки HF и золы, полученной из содержащего кремний соединения;
f) площадью BET поверхности золы двуокиси кремния в упомянутом наполнителе приблизительно 200 - 700 м2/г.39. A filler comprising a carbon phase and a phase containing a silicon substance, characterized in that it has one of the following indicators:
a) the difference between the surface area BET (N 2 ) and the surface t-area of about 2-100 m 2 / g;
b) the difference between the BET (N 2 ) surface area and the t-surface area of approximately 1 to 50 m 2 / g after HF treatment;
c) a ratio of about 0.1 to 10 based on 1) the area difference BET (N 2 ) of the surface of the filler after treatment and before HF treatment to 2) the silicon percentage by weight in said filler without HF treatment;
d) a decrease in the weighted average particle size of the filler, measured using a disk centrifuging photosedimentometer (DCP), after processing HF from about 5 to 40% compared with the weighted average particle size of the filler without processing HF;
e) a silica ash content in said filler of about 0.05-1% based on the weight of said filler after treatment with HF and ash obtained from a silicon-containing compound;
f) a BET surface area of the silica ash in said filler of about 200 to 700 m 2 / g.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/837,493 | 1997-04-18 | ||
US08/837,493 US5904762A (en) | 1997-04-18 | 1997-04-18 | Method of making a multi-phase aggregate using a multi-stage process |
Publications (2)
Publication Number | Publication Date |
---|---|
RU99124399A true RU99124399A (en) | 2001-09-27 |
RU2220176C2 RU2220176C2 (en) | 2003-12-27 |
Family
ID=25274612
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU99124399/15A RU2220176C2 (en) | 1997-04-18 | 1998-04-17 | Multiphase carbon-containing filling agent and methods for its preparing |
Country Status (17)
Country | Link |
---|---|
US (6) | US5904762A (en) |
EP (1) | EP0975699B8 (en) |
JP (3) | JP4837810B2 (en) |
KR (1) | KR100527025B1 (en) |
CN (1) | CN100341955C (en) |
AU (1) | AU734675B2 (en) |
BR (1) | BR9814241B1 (en) |
CZ (1) | CZ302267B6 (en) |
DE (1) | DE69838448T2 (en) |
HU (1) | HU230169B1 (en) |
ID (1) | ID24202A (en) |
NZ (1) | NZ500369A (en) |
PL (1) | PL189823B1 (en) |
RU (1) | RU2220176C2 (en) |
SE (1) | SE525456C2 (en) |
TR (1) | TR199903300T2 (en) |
WO (1) | WO1998047971A1 (en) |
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