MX365785B - Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion. - Google Patents

Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion.

Info

Publication number
MX365785B
MX365785B MX2015008597A MX2015008597A MX365785B MX 365785 B MX365785 B MX 365785B MX 2015008597 A MX2015008597 A MX 2015008597A MX 2015008597 A MX2015008597 A MX 2015008597A MX 365785 B MX365785 B MX 365785B
Authority
MX
Mexico
Prior art keywords
carboxylic acid
concentration
solution containing
evaporation
purifying
Prior art date
Application number
MX2015008597A
Other languages
English (en)
Other versions
MX2015008597A (es
Inventor
Gehrke Helmut
Schulze Joachim
Ghanegaonkar Shashank
Kleiber Michael
Gnabs Ulrike
Gawenda Marcel
Original Assignee
Thyssenkrupp Ind Solutions Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thyssenkrupp Ind Solutions Ag filed Critical Thyssenkrupp Ind Solutions Ag
Publication of MX2015008597A publication Critical patent/MX2015008597A/es
Publication of MX365785B publication Critical patent/MX365785B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/02—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor with moving adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025—Reverse osmosis; Hyperfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/02—Specific process operations before starting the membrane separation process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Analytical Chemistry (AREA)
  • Nanotechnology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

La invención se refiere a un procedimiento y un dispositivo para la separación y purificación de ácidos carboxílicos de caldos de fermentación que contienen sales amonio de ácidos carboxílicos, comprendiendo el procedimiento las siguientes etapas, a) una separación de biomasa y de solidos eventualmente presentes a partir del caldo de fermentación, b) preparación de una disolución que contiene el ácido carboxílico deseado y de otra disolución que contiene sales de amonio, llevándose a cabo una cromatografía en el lecho móvil simulado (SMB), c) una purificación fina de la disolución que contiene el ácido carboxílico deseado de la etapa b) del procedimiento, d) una concentración de la disolución purificada de ácido carboxílico de la etapa c) del procedimiento, e) cristalización de la disolución concentrada de ácido carboxílico de la etapa d) del procedimiento, f) una concentración de la disolución adicional que contiene sales de amonio de la etapa b) del procedimiento, caracterizado porque en las etapas d) y f) del procedimiento en la concentración se lleva a cabo una combinación a base de ósmosis inversa y vaporización, y el vapor de la vaporización de la etapa f) del procedimiento se conduce a la vaporización de la etapa d) del procedimiento.
MX2015008597A 2013-01-03 2013-12-20 Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion. MX365785B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102013000027.0A DE102013000027A1 (de) 2013-01-03 2013-01-03 Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen
PCT/EP2013/003892 WO2014106532A2 (de) 2013-01-03 2013-12-20 Verfahren zur aufreinigung von carbonsäuren aus fermentationsbrühen

Publications (2)

Publication Number Publication Date
MX2015008597A MX2015008597A (es) 2016-01-15
MX365785B true MX365785B (es) 2019-06-05

Family

ID=50101851

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015008597A MX365785B (es) 2013-01-03 2013-12-20 Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion.

Country Status (10)

Country Link
US (1) US9422220B2 (es)
EP (1) EP2941412B1 (es)
CN (1) CN105073703A (es)
BR (1) BR112015015931B1 (es)
DE (1) DE102013000027A1 (es)
HU (1) HUE042352T2 (es)
MX (1) MX365785B (es)
MY (1) MY185170A (es)
PL (1) PL2941412T3 (es)
WO (1) WO2014106532A2 (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102014213637A1 (de) * 2014-07-14 2016-01-14 Thyssenkrupp Ag Verfahren und Vorrichtung zur Aufkonzentration und Kristallisation von fermentierbaren Carbonsäuren
FR3028864B1 (fr) 2014-11-26 2018-05-18 Roquette Freres Procede de recuperation de cristaux d'acide succinique avec mise en œuvre de tensioactifs au cours de la cristallisation, cristaux obtenus et leurs utilisations
CN111909030A (zh) * 2014-12-02 2020-11-10 法国罗盖特公司 由发酵培养液使用纳滤纯化回收的母液来制造琥珀酸的方法
DE102015216815A1 (de) 2015-09-02 2017-03-02 Thyssenkrupp Ag Verfahren und Anlage zur Gewinnung einer in einem Fermentationsprozess hergestellten Carbonsäure
DE102016119938A1 (de) 2016-10-19 2018-04-19 Thyssenkrupp Ag Reinigung und Konzentrierung von Carbonsäuren aus Fermentationsprozessen
CN110498740A (zh) * 2019-09-18 2019-11-26 重庆医药高等专科学校 一种生产3-羟基丙酸的方法
EP3822356A1 (en) * 2019-11-18 2021-05-19 Corvay Bioproducts GmbH Method for the production of a dicarboxylic acid
CN111635302B (zh) * 2020-07-08 2021-06-15 江南大学 一种多柱连续色谱除盐以纯化羟基乙酸的方法
IT202000017368A1 (it) 2020-07-16 2022-01-16 Radici Chimica S P A Purificazione di acidi dicarbossilici alifatici prodotti mediante processi biotecnologici
CN113185397B (zh) * 2021-04-09 2023-12-01 安徽丰原集团有限公司 一种从发酵液中回收苹果酸的方法
WO2022258732A1 (en) * 2021-06-09 2022-12-15 Avantium Knowledge Centre B.V. Process and system for the recovery of glyoxylic acid
WO2024097329A1 (en) * 2022-11-02 2024-05-10 Amalgamated Research Llc Smb separator for organic acid purification using a strong acid cation resin

Family Cites Families (18)

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Publication number Priority date Publication date Assignee Title
DE3328093A1 (de) 1983-08-04 1985-02-21 Hoechst Ag, 6230 Frankfurt Isolierung von durch fermentation erzeugten carbonsaeuren
US5168055A (en) 1986-06-11 1992-12-01 Rathin Datta Fermentation and purification process for succinic acid
US5143834A (en) 1986-06-11 1992-09-01 Glassner David A Process for the production and purification of succinic acid
US5034105A (en) 1989-07-27 1991-07-23 Michigan Biotechnology Institute Carboxylic acid purification and crystallization process
EP0603321A1 (en) 1991-09-13 1994-06-29 Purdue Research Foundation Fermentation process for producing lactic acid
BE1011197A3 (fr) 1997-06-06 1999-06-01 Brussels Biotech En Abrege Bb Procede de purification d'acide lactique.
US5958744A (en) 1997-08-18 1999-09-28 Applied Carbochemicals Succinic acid production and purification
US6229046B1 (en) 1997-10-14 2001-05-08 Cargill, Incorported Lactic acid processing methods arrangements and products
US6034269A (en) * 1998-08-03 2000-03-07 E. I. Du Pont De Nemours And Company Process for producing pure carboxylic acids
US6291708B1 (en) 1999-04-28 2001-09-18 A.E. Staley Manufacturing Co. Process for production of organic acids and esters thereof
DE19939630C2 (de) 1999-08-20 2001-07-12 Mg Technologies Ag Verfahren zum Feinreinigen einer wässrigen Lösung, die eine fermentativ hergestellte organische Säure enthält
US7381386B2 (en) * 2003-06-05 2008-06-03 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
DE102004026152A1 (de) 2004-05-28 2005-12-15 Basf Ag Fermentative Herstellung von Feinchemikalien
WO2006124633A1 (en) 2005-05-13 2006-11-23 Cargill, Incorporated Production of lactic acid
DE102007045701B3 (de) 2007-09-24 2009-05-14 Uhde Gmbh Gewinnung von Milchsäure durch Fermentation und Extraktion mit Aminen
DE102009019248A1 (de) 2009-04-30 2010-11-04 Uhde Gmbh Isolierung von organischen Säuren aus Fermenterbrühe mit Hilfe chromatographischer Methoden
KR20120099154A (ko) * 2009-12-31 2012-09-06 미리안트 코포레이션 암모늄 숙신산염을 함유하고 있는 발효 배지로부터의 숙신산의 정제
DE102010025167A1 (de) * 2010-06-25 2011-12-29 Uhde Gmbh Verfahren zur Abtrennung, Gewinnung und Reinigung von Bernsteinsäure

Also Published As

Publication number Publication date
BR112015015931A2 (pt) 2017-07-11
MX2015008597A (es) 2016-01-15
DE102013000027A1 (de) 2014-07-03
EP2941412A2 (de) 2015-11-11
HUE042352T2 (hu) 2019-06-28
US9422220B2 (en) 2016-08-23
PL2941412T3 (pl) 2019-04-30
US20150344397A1 (en) 2015-12-03
EP2941412B1 (de) 2018-10-24
BR112015015931B1 (pt) 2020-10-20
WO2014106532A2 (de) 2014-07-10
WO2014106532A3 (de) 2014-09-12
CN105073703A (zh) 2015-11-18
MY185170A (en) 2021-04-30

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