LU505449B1 - Sucrose decoloring method and system - Google Patents
Sucrose decoloring method and system Download PDFInfo
- Publication number
- LU505449B1 LU505449B1 LU505449A LU505449A LU505449B1 LU 505449 B1 LU505449 B1 LU 505449B1 LU 505449 A LU505449 A LU 505449A LU 505449 A LU505449 A LU 505449A LU 505449 B1 LU505449 B1 LU 505449B1
- Authority
- LU
- Luxembourg
- Prior art keywords
- section
- anion resin
- resin column
- regeneration
- column
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 163
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title claims abstract description 58
- 229930006000 Sucrose Natural products 0.000 title claims abstract description 58
- 239000005720 sucrose Substances 0.000 title claims abstract description 58
- 239000011347 resin Substances 0.000 claims abstract description 313
- 229920005989 resin Polymers 0.000 claims abstract description 313
- 230000008569 process Effects 0.000 claims abstract description 146
- 230000008929 regeneration Effects 0.000 claims abstract description 99
- 238000011069 regeneration method Methods 0.000 claims abstract description 99
- 235000009508 confectionery Nutrition 0.000 claims abstract description 67
- 238000011001 backwashing Methods 0.000 claims abstract description 57
- 150000001450 anions Chemical class 0.000 claims description 108
- 238000004042 decolorization Methods 0.000 claims description 101
- -1 acrylic anion Chemical class 0.000 claims description 99
- 239000000243 solution Substances 0.000 claims description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 33
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 22
- 239000011780 sodium chloride Substances 0.000 claims description 11
- 239000011259 mixed solution Substances 0.000 claims description 10
- 230000001172 regenerating effect Effects 0.000 claims description 2
- 230000000630 rising effect Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 26
- 239000000463 material Substances 0.000 description 9
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 8
- 229910001415 sodium ion Inorganic materials 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000012267 brine Substances 0.000 description 6
- 239000000049 pigment Substances 0.000 description 6
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 6
- 239000002351 wastewater Substances 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000001514 detection method Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 238000006386 neutralization reaction Methods 0.000 description 5
- 238000011084 recovery Methods 0.000 description 5
- 230000009467 reduction Effects 0.000 description 5
- 238000001179 sorption measurement Methods 0.000 description 4
- 238000004065 wastewater treatment Methods 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000007667 floating Methods 0.000 description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 2
- 150000002500 ions Chemical group 0.000 description 2
- 238000005374 membrane filtration Methods 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- DEXFNLNNUZKHNO-UHFFFAOYSA-N 6-[3-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperidin-1-yl]-3-oxopropyl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1CCN(CC1)C(CCC1=CC2=C(NC(O2)=O)C=C1)=O DEXFNLNNUZKHNO-UHFFFAOYSA-N 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 238000013494 PH determination Methods 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000003957 anion exchange resin Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/146—Purification of sugar juices using ion-exchange materials using only anionic ion-exchange material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
- B01J49/57—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for anionic exchangers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/60—Cleaning or rinsing ion-exchange beds
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatment Of Water By Ion Exchange (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202210240595.2A CN114606348A (zh) | 2022-03-10 | 2022-03-10 | 一种蔗糖脱色的方法及*** |
CN202210745626.XA CN114807456B (zh) | 2022-03-10 | 2022-06-29 | 一种蔗糖脱色的方法及*** |
Publications (2)
Publication Number | Publication Date |
---|---|
LU505449A1 LU505449A1 (en) | 2023-12-11 |
LU505449B1 true LU505449B1 (en) | 2024-03-11 |
Family
ID=81863518
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
LU505449A LU505449B1 (en) | 2022-03-10 | 2023-02-15 | Sucrose decoloring method and system |
Country Status (3)
Country | Link |
---|---|
CN (2) | CN114606348A (zh) |
LU (1) | LU505449B1 (zh) |
WO (1) | WO2023169166A1 (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114606348A (zh) * | 2022-03-10 | 2022-06-10 | 欧尚元(天津)有限公司 | 一种蔗糖脱色的方法及*** |
CN117583038B (zh) * | 2024-01-18 | 2024-04-12 | 欧尚元智能装备有限公司 | 一种蔗糖脱钙方法及*** |
CN117599860B (zh) * | 2024-01-23 | 2024-03-26 | 欧尚元智能装备有限公司 | 一种头孢脱色***及工艺 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100401916C (zh) * | 2006-03-15 | 2008-07-16 | 浙江大学 | 一种菊芋浸提液的脱色方法 |
CN102031315B (zh) * | 2010-11-30 | 2013-08-07 | 华南理工大学 | 制糖脱色脱钙树脂的再生方法及再生废液的回用方法 |
JP6283235B2 (ja) * | 2014-02-25 | 2018-02-21 | オルガノ株式会社 | 蔗糖溶液の精製方法および精製装置 |
CN209138051U (zh) * | 2018-11-13 | 2019-07-23 | 赛普特环保技术(厦门)有限公司 | 一种用于木糖除杂的移动树脂柱*** |
CN109225355B (zh) * | 2018-11-13 | 2023-11-14 | 赛普特环保技术(厦门)有限公司 | 一种脱除无机盐的连续离子交换工艺及所采用的*** |
CN111254230B (zh) * | 2020-03-04 | 2022-04-12 | 德兰梅勒(北京)分离技术股份有限公司 | 一种精致糖脱色处理装置及脱色、反洗、再生和清洗工艺 |
CN112062796B (zh) * | 2020-10-30 | 2022-02-22 | 石药集团圣雪葡萄糖有限责任公司 | 一种基于连续离子交换装置的阿卡波糖连续脱盐中和生产方法 |
CN112619713A (zh) * | 2020-12-30 | 2021-04-09 | 保龄宝生物股份有限公司 | 一种生产功能性低聚糖的离子交换***及其使用方法 |
CN114606348A (zh) * | 2022-03-10 | 2022-06-10 | 欧尚元(天津)有限公司 | 一种蔗糖脱色的方法及*** |
-
2022
- 2022-03-10 CN CN202210240595.2A patent/CN114606348A/zh active Pending
- 2022-06-29 CN CN202210745626.XA patent/CN114807456B/zh active Active
-
2023
- 2023-02-15 WO PCT/CN2023/076190 patent/WO2023169166A1/zh unknown
- 2023-02-15 LU LU505449A patent/LU505449B1/en active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
CN114606348A (zh) | 2022-06-10 |
CN114807456A (zh) | 2022-07-29 |
WO2023169166A1 (zh) | 2023-09-14 |
CN114807456B (zh) | 2023-01-13 |
LU505449A1 (en) | 2023-12-11 |
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Legal Events
Date | Code | Title | Description |
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FG | Patent granted |
Effective date: 20240311 |