LU505449B1 - Sucrose decoloring method and system - Google Patents

Sucrose decoloring method and system Download PDF

Info

Publication number: LU505449B1
Authority: LU; Luxembourg
Prior art keywords: section; anion resin; resin column; regeneration; column
Prior art date: 2022-03-10

Application number

LU505449A

Other languages

English (en)

Other versions

LU505449A1 (en

Inventor

Shengchang Wang

Tianti Zhang

Jianguo Gao

Xin Su

Haijing Tang

Original Assignee

Oushangyuan Process & Equipment Intelligent Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2022-03-10

Filing date

2023-02-15

Publication date

2024-03-11

2023-02-15 Application filed by Oushangyuan Process & Equipment Intelligent Co filed Critical Oushangyuan Process & Equipment Intelligent Co

2023-12-11 Publication of LU505449A1 publication Critical patent/LU505449A1/en

2024-03-11 Application granted granted Critical

2024-03-11 Publication of LU505449B1 publication Critical patent/LU505449B1/en

Links

238000000034 method Methods 0.000 title claims abstract description 163
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title claims abstract description 58
229930006000 Sucrose Natural products 0.000 title claims abstract description 58
239000005720 sucrose Substances 0.000 title claims abstract description 58
239000011347 resin Substances 0.000 claims abstract description 313
229920005989 resin Polymers 0.000 claims abstract description 313
230000008569 process Effects 0.000 claims abstract description 146
230000008929 regeneration Effects 0.000 claims abstract description 99
238000011069 regeneration method Methods 0.000 claims abstract description 99
235000009508 confectionery Nutrition 0.000 claims abstract description 67
238000011001 backwashing Methods 0.000 claims abstract description 57
150000001450 anions Chemical class 0.000 claims description 108
238000004042 decolorization Methods 0.000 claims description 101
-1 acrylic anion Chemical class 0.000 claims description 99
239000000243 solution Substances 0.000 claims description 47
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 33
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 22
239000011780 sodium chloride Substances 0.000 claims description 11
239000011259 mixed solution Substances 0.000 claims description 10
230000001172 regenerating effect Effects 0.000 claims description 2
230000000630 rising effect Effects 0.000 claims 1
230000000694 effects Effects 0.000 abstract description 6
230000003247 decreasing effect Effects 0.000 abstract 1
230000000052 comparative effect Effects 0.000 description 26
239000000463 material Substances 0.000 description 9
FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 8
229910001415 sodium ion Inorganic materials 0.000 description 8
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
239000012267 brine Substances 0.000 description 6
239000000049 pigment Substances 0.000 description 6
HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 6
239000002351 wastewater Substances 0.000 description 6
239000003795 chemical substances by application Substances 0.000 description 5
238000001514 detection method Methods 0.000 description 5
238000010586 diagram Methods 0.000 description 5
238000006386 neutralization reaction Methods 0.000 description 5
238000011084 recovery Methods 0.000 description 5
230000009467 reduction Effects 0.000 description 5
238000001179 sorption measurement Methods 0.000 description 4
238000004065 wastewater treatment Methods 0.000 description 4
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
239000007788 liquid Substances 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
229920006395 saturated elastomer Polymers 0.000 description 3
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
238000007667 floating Methods 0.000 description 2
235000011389 fruit/vegetable juice Nutrition 0.000 description 2
150000002500 ions Chemical group 0.000 description 2
238000005374 membrane filtration Methods 0.000 description 2
239000012452 mother liquor Substances 0.000 description 2
238000012360 testing method Methods 0.000 description 2
239000002699 waste material Substances 0.000 description 2
DEXFNLNNUZKHNO-UHFFFAOYSA-N 6-[3-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperidin-1-yl]-3-oxopropyl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1CCN(CC1)C(CCC1=CC2=C(NC(O2)=O)C=C1)=O DEXFNLNNUZKHNO-UHFFFAOYSA-N 0.000 description 1
239000004925 Acrylic resin Substances 0.000 description 1
229920000178 Acrylic resin Polymers 0.000 description 1
238000013494 PH determination Methods 0.000 description 1
240000000111 Saccharum officinarum Species 0.000 description 1
235000007201 Saccharum officinarum Nutrition 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000003957 anion exchange resin Substances 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
230000008859 change Effects 0.000 description 1
239000013078 crystal Substances 0.000 description 1
125000004122 cyclic group Chemical group 0.000 description 1
238000007599 discharging Methods 0.000 description 1
238000010828 elution Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
238000010309 melting process Methods 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012545 processing Methods 0.000 description 1
239000000047 product Substances 0.000 description 1
238000000746 purification Methods 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000007670 refining Methods 0.000 description 1
150000003839 salts Chemical class 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/146—Purification of sugar juices using ion-exchange materials using only anionic ion-exchange material
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
- B01J49/57—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for anionic exchangers
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/60—Cleaning or rinsing ion-exchange beds
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Treatment Of Water By Ion Exchange (AREA)
Saccharide Compounds (AREA)

LU505449A 2022-03-10 2023-02-15 Sucrose decoloring method and system LU505449B1 (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
CN202210240595.2A CN114606348A (zh)	2022-03-10	2022-03-10	一种蔗糖脱色的方法及***
CN202210745626.XA CN114807456B (zh)	2022-03-10	2022-06-29	一种蔗糖脱色的方法及***

Publications (2)

Publication Number	Publication Date
LU505449A1 LU505449A1 (en)	2023-12-11
LU505449B1 true LU505449B1 (en)	2024-03-11

Family

ID=81863518

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU505449A LU505449B1 (en)	2022-03-10	2023-02-15	Sucrose decoloring method and system

Country Status (3)

Country	Link
CN (2)	CN114606348A (zh)
LU (1)	LU505449B1 (zh)
WO (1)	WO2023169166A1 (zh)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN114606348A (zh) *	2022-03-10	2022-06-10	欧尚元(天津)有限公司	一种蔗糖脱色的方法及***
CN117583038B (zh) *	2024-01-18	2024-04-12	欧尚元智能装备有限公司	一种蔗糖脱钙方法及***
CN117599860B (zh) *	2024-01-23	2024-03-26	欧尚元智能装备有限公司	一种头孢脱色***及工艺

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN100401916C (zh) *	2006-03-15	2008-07-16	浙江大学	一种菊芋浸提液的脱色方法
CN102031315B (zh) *	2010-11-30	2013-08-07	华南理工大学	制糖脱色脱钙树脂的再生方法及再生废液的回用方法
JP6283235B2 (ja) *	2014-02-25	2018-02-21	オルガノ株式会社	蔗糖溶液の精製方法および精製装置
CN209138051U (zh) *	2018-11-13	2019-07-23	赛普特环保技术(厦门)有限公司	一种用于木糖除杂的移动树脂柱***
CN109225355B (zh) *	2018-11-13	2023-11-14	赛普特环保技术(厦门)有限公司	一种脱除无机盐的连续离子交换工艺及所采用的***
CN111254230B (zh) *	2020-03-04	2022-04-12	德兰梅勒（北京）分离技术股份有限公司	一种精致糖脱色处理装置及脱色、反洗、再生和清洗工艺
CN112062796B (zh) *	2020-10-30	2022-02-22	石药集团圣雪葡萄糖有限责任公司	一种基于连续离子交换装置的阿卡波糖连续脱盐中和生产方法
CN112619713A (zh) *	2020-12-30	2021-04-09	保龄宝生物股份有限公司	一种生产功能性低聚糖的离子交换***及其使用方法
CN114606348A (zh) *	2022-03-10	2022-06-10	欧尚元(天津)有限公司	一种蔗糖脱色的方法及***

2022
- 2022-03-10 CN CN202210240595.2A patent/CN114606348A/zh active Pending
- 2022-06-29 CN CN202210745626.XA patent/CN114807456B/zh active Active
2023
- 2023-02-15 WO PCT/CN2023/076190 patent/WO2023169166A1/zh unknown
- 2023-02-15 LU LU505449A patent/LU505449B1/en active IP Right Grant

Also Published As

Publication number	Publication date
CN114606348A (zh)	2022-06-10
CN114807456A (zh)	2022-07-29
WO2023169166A1 (zh)	2023-09-14
CN114807456B (zh)	2023-01-13
LU505449A1 (en)	2023-12-11

Legal Events

Date	Code	Title	Description
2024-04-03	FG	Patent granted	Effective date: 20240311

Publication	Publication Date	Title
LU505449B1 (en)	2024-03-11	Sucrose decoloring method and system
US4968353A (en)	1990-11-06	Method for refining sugar liquor
EP2552562B1 (en)	2014-10-08	Separation process
CN112593017A (zh)	2021-04-02	一种用于甜菜制糖糖分高效分离方法
JP6265750B2 (ja)	2018-01-24	蔗糖溶液の精製方法および精製装置
CN103896762B (zh)	2016-02-10	一种含柠檬酸溶液的纯化方法
US5032686A (en)	1991-07-16	Method for the recovery of citric acid from a liquor containing the same
KR20010062380A (ko)	2001-07-07	혼상식(混床式) 당액 정제장치 및 그의 재생법
CN114699801B (zh)	2022-09-20	一种用于红乳酸纯化的阀阵式连续离交***
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CN114606349A (zh)	2022-06-10	一种甜菜糖稀汁软化方法
US2926110A (en)	1960-02-23	Process for the purification of beet sugar juice by means of ion exchange resins
WO2019111490A1 (ja)	2019-06-13	糖液の精製方法及び糖液精製装置
CN100361724C (zh)	2008-01-16	一种n-乙酰乙酰替苯胺生产废水的处理方法
JPH0577400B2 (zh)	1993-10-26
JPH01244000A (ja)	1989-09-28	甜菜糖液を処理する方法
CN114702379B (zh)	2022-09-20	一种红乳酸纯化方法
CN219156794U (zh)	2023-06-09	一种苹果酸除杂酸纯化的装置
CN112410474B (zh)	2023-09-15	一种精炼糖离子交换脱色节水工艺
JP2005295916A (ja)	2005-10-27	糖含有溶液の精製方法
US20220098684A1 (en)	2022-03-31	Method for Bleaching Sugar With Effluent Recycling
CN107417514A (zh)	2017-12-01	一种从柠檬酸液中纯化柠檬酸的方法
CN114272960A (zh)	2022-04-05	一种阀阵式多单元连续离交提纯木糖的方法及装置
JPH0227999A (ja)	1990-01-30	糖液の清浄方法
CN114260028A (zh)	2022-04-01	一种谷氨酸钠料液脱色的方法和装置