KR860007956A - 2-형태 실리콘 유제 조성물 및 실리콘 유화방법 - Google Patents

2-형태 실리콘 유제 조성물 및 실리콘 유화방법 Download PDF

Info

Publication number
KR860007956A
KR860007956A KR1019860002493A KR860002493A KR860007956A KR 860007956 A KR860007956 A KR 860007956A KR 1019860002493 A KR1019860002493 A KR 1019860002493A KR 860002493 A KR860002493 A KR 860002493A KR 860007956 A KR860007956 A KR 860007956A
Authority
KR
South Korea
Prior art keywords
weight
parts
polydimethyl siloxane
polydimethylsiloxane
viscosity
Prior art date
Application number
KR1019860002493A
Other languages
English (en)
Other versions
KR930006262B1 (ko
Inventor
나룰라 디파크
Original Assignee
다우 코닝 코포레이션
앨빈 어네스트 베이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 다우 코닝 코포레이션, 앨빈 어네스트 베이 filed Critical 다우 코닝 코포레이션
Publication of KR860007956A publication Critical patent/KR860007956A/ko
Application granted granted Critical
Publication of KR930006262B1 publication Critical patent/KR930006262B1/ko

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2383/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2383/04—Polysiloxanes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
    • Y10S516/922—Colloid systems having specified particle size, range, or distribution, e.g. bimodal particle distribution
    • Y10S516/923—Emulsion

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Colloid Chemistry (AREA)
  • Lubricants (AREA)
  • Paints Or Removers (AREA)
  • Cosmetics (AREA)

Abstract

내용 없음

Description

2-형태 실리콘 유제 조성물 및 실리콘 유화방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (8)

  1. (1) 주로 (A) 점도가 25℃에서 50Pa.s(pascal-seconds)까지이고, 주로 (i)점도가 25℃에서 30Pa.s이상인 1 내지 100중량부의 비휘발성 폴리디메틸 실옥산 부분 및 (ii) 0내지 99중량부의 휘발성 폴리디메틸 실옥산 부분으로 이루어진 100중량부의 폴리디메틸 실옥산액 및 (B) 제 1계면활성제 밀리몰당 1 내지 5밀리몰의, HLB수가 7 내지 9인 비이온성 제2계면활성제로 이루어진 성분들을 충분히 혼합시키고 :
    (Ⅱ) 주로(C) HLB수가 13 내지 15인 3 밀리몰 이상의 비이온성 제1계면활성제 및 (D) 유제-형성량의 물로 이루어진 성분들과 (Ⅰ)의 혼합물을 충분히 혼합시켜 미가공 수-중-실리콘 유체를 생성시키고 :
    (Ⅲ) 미가공 유제를, 실리콘의 평균 입자 크기를 약 2μ 미만까지 감소시키기에 충분한 시간동안, 유제의 온도를 약 1 내지40℃로 유지시키면서, 저 전달 발생장치로 분쇄시킴을 특징으로 하는 유화방법.
  2. 제1항에 있어서 상기 저 전단 발생 장치가 원심분리펌프이고, 수-중-실리콘 유체를 상기 펌프에 반복하여 통과시키는 방법.
  3. 제1항에 있어서, 상기 저 전달 발생 장치가 간격이 0.04인치 이상으로 고정된 콜로이드 밀(mill)이고 수-중-실리콘 유제를 이 간격에 반복하여 통과시키는데, 각각 이 간격을 통과하기 전 수-중-실리콘 유제의 온도를 20내지 30℃로 조절하는 방법.
  4. 제1항에 있어서, 폴리디메틸실옥산액(A)가 주로(i) 점도가 25℃에서 30Pa.s 이상인 1내지 75중량부의 비휘발성 폴리디메틸실옥산 부분 및 (ii) 25내지 99 중량부의 휘발성 폴리디메틸실옥산 부분으로 이루어진 2-형태의 방법.
  5. 제4항에 있어서, 2-형태 폴리디메틸실옥산액(A)가 주로 (i) 점도가 25℃에서 10Kpa.s 이상인 10내지 20중량부의 비휘발성 폴리디메틸실옥산 부분 및 (ii) 분자당 4 또는 5실리콘 원자를 갖는 시클로폴리디 메틸실옥산 중에서 선택된 80 내지 90중량부의 휘발성 폴리디메틸실옥산 부분으로 이루어진 방법.
  6. 주로(A) 점도가 25℃에서 50Pa.s까지이고, 주로 (i) 점도가 25℃에서 30Pa.s이상인 1내지 75중량부의 비휘발성 폴리디메틸 실옥산 부분 및 (ii) 25내지 99중량부의 휘발성 폴리디메틸 실옥산 부분으로 이루어진 100중량부의 2-형태 폴리디메틸 실옥산액 성분. (B) 제1계면활성제 밀리몰당 1내지 5밀리몰의, HLB가 7 내지 9인 비이온성 제2계면활성제. (C) HLB수가 13 내지 15인 3밀리몰 이상의 비이온성 제1계면활성제 및 (D) 유제-형성량의 물로 이루어진, 2-형태 수-중-실리콘 유제 조성물.
  7. 제6항에 있어서, 폴리디메틸 실옥산액(A)이 주로 (i) 점도가 25℃에서 10KPa.s 이상인 10내지 20중량부의 비휘발성 폴리디메틸 실옥산 부분 및 (ii) 분자당 4 또는 실리콘 원자를 갖는 시클로폴리디메틸실옥산 중에서 선택된 80내지 90중량부의 휘발성 폴리디메틸실옥산 부분으로 이루어진 조성물.
  8. 제1항의 방법으로 제조한 수-중-실리콘 유제 조성물.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019860002493A 1985-04-02 1986-04-02 2-형태 실리콘 유제 조성물 및 실리콘 유화방법 KR930006262B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US718985 1985-04-02
US06/718,985 US4874547A (en) 1985-04-02 1985-04-02 Bi-modal silicone emulsions, silicone emulsification process and emulsions therefrom
US718,985 1985-04-02

Publications (2)

Publication Number Publication Date
KR860007956A true KR860007956A (ko) 1986-11-10
KR930006262B1 KR930006262B1 (ko) 1993-07-09

Family

ID=24888351

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019860002493A KR930006262B1 (ko) 1985-04-02 1986-04-02 2-형태 실리콘 유제 조성물 및 실리콘 유화방법

Country Status (9)

Country Link
US (1) US4874547A (ko)
EP (1) EP0200009B1 (ko)
JP (1) JPH0659401B2 (ko)
KR (1) KR930006262B1 (ko)
AU (1) AU579461B2 (ko)
BR (1) BR8601443A (ko)
CA (1) CA1260794A (ko)
DE (1) DE3677248D1 (ko)
MX (1) MX165179B (ko)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE34584E (en) 1984-11-09 1994-04-12 The Procter & Gamble Company Shampoo compositions
CA1260795A (en) * 1985-04-02 1989-09-26 Dipak Narula Emulsification process and emulsions therefrom
JPS63130512A (ja) * 1986-11-18 1988-06-02 Toray Silicone Co Ltd 化粧料
JPS6443342A (en) * 1987-08-07 1989-02-15 Shiseido Co Ltd Emulsifying compound
US5130122A (en) * 1989-01-27 1992-07-14 Medicontrol Corporation Oral cavity and dental microemulsion products
JPH0745332B2 (ja) * 1989-04-27 1995-05-17 アサヒビール株式会社 ガラス容器の擦り傷遮蔽剤、擦り傷が遮蔽されたガラス容器およびガラス容器の擦り傷遮蔽方法
EP0432951B2 (en) * 1989-12-04 2004-06-30 Unilever Plc Hair treatment composition
CA2043282A1 (en) * 1990-06-07 1991-12-08 Ronald P. Gee Process for making polysiloxane emulsions
US5371139A (en) * 1991-06-21 1994-12-06 Dow Corning Toray Silicone Co., Ltd. Silicone rubber microsuspension and method for its preparation
ATE120952T1 (de) * 1991-07-18 1995-04-15 Procter & Gamble Flüssige deodorantzusammensetzungen.
DE4142387A1 (de) * 1991-12-20 1993-06-24 Wacker Chemie Gmbh Pflegemittel fuer harte oberflaechen
US5302658A (en) * 1992-07-14 1994-04-12 Dow Corning Corporation Method of manufacturing silicone emulsions
DE4309971A1 (de) * 1993-03-26 1994-09-29 Bayer Ag Imprägnierungsemulsion für mineralische Baustoffe
US5421865A (en) * 1993-10-29 1995-06-06 United Technologies Corporation Water based silicone coating compositions
FR2717731B1 (fr) * 1994-03-24 1996-05-15 Chryso Sa Concentré pour émulsion de démoulage des liants hydrauliques, émulsion de démoulage et utilisation.
US5746810A (en) * 1995-11-30 1998-05-05 Toyo Ink Manufacturing Co., Ltd. Aqueous emulsion of alkylalkoxysilane, process for the production thereof, and use thereof
FR2747321B1 (fr) * 1996-04-16 1998-07-10 Centre Nat Rech Scient Procede de preparation d'une emulsion
US5882387A (en) * 1996-08-26 1999-03-16 Wacker Silicones Corporation Polish composition
US5844007A (en) * 1996-10-21 1998-12-01 No Touch North America Lustering and protecting agent for rubber, vinyl, and the like
US5856402A (en) * 1996-12-30 1999-01-05 General Electric Company Process for the synthesis of multi-modal aqueous dispersions of polysiloxanes
DE10326188A1 (de) * 2003-06-06 2004-11-18 Schering Ag Wässrige Emulsion, enthaltend ein Organopolysiloxan und ein nichtionisches Tensid, Verfahren zu ihrer Herstellung sowie Verwendung der Emulsion
US7528209B2 (en) * 2004-10-29 2009-05-05 Shin-Etsu Chemical Co., Ltd. Curable silicone release composition and sheet having a releasability using the same
WO2007088417A1 (en) * 2006-02-03 2007-08-09 Wockhardt Limited Silicone oil-in-water emulsions-formulation, production and use
WO2012119068A2 (en) 2011-03-03 2012-09-07 Dow Corning Corporation Bi-modal emulsions
BR112013022310A2 (pt) * 2011-03-03 2019-09-24 Dow Corning emulsões bimodais
EP2690177B1 (en) 2012-07-24 2014-12-03 Technische Universität Dresden Protein with recombinase activity for site-specific DNA-recombination
KR20150086284A (ko) * 2012-11-21 2015-07-27 다우 코닝 코포레이션 이중모드 에멀젼을 포함하는 화장품 조성물
CN107046802A (zh) * 2014-12-03 2017-08-15 道康宁公司 双峰乳液
US9605229B2 (en) * 2014-12-19 2017-03-28 Bathium Canada Inc. Lubricant for lamination of lithium sheets into lithium thin films
US11602582B2 (en) * 2018-04-10 2023-03-14 Chemsil Silicones, Inc. Intimate care lubricant compositions and methods for making same
US20220325209A1 (en) * 2021-04-01 2022-10-13 W.M. Barr & Company, Inc. Water-in-silicone emulsion based liquid cleaner

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2697674A (en) * 1954-12-21 Method for cleaning paint brushes
US2702276A (en) * 1951-04-10 1955-02-15 Du Pont Water-dispersible emulsions of polysiloxanes
US2891920A (en) * 1955-01-26 1959-06-23 Dow Corning Polymerization of organopolysiloxanes in aqueous emulsion
NL204267A (ko) * 1955-02-07
GB1024024A (en) * 1963-04-08 1966-03-30 Dow Corning Improvements in or relating to polymerising or co-polymerising organosilicon compounds
NL124881C (ko) * 1964-05-18
US3634285A (en) * 1969-03-24 1972-01-11 Stauffer Wacker Silicone Corp Silicone release emulsion
US3635834A (en) * 1969-12-22 1972-01-18 Squibb & Sons Inc Process for preparing semisolid emulsions
US3925242A (en) * 1970-06-17 1975-12-09 Rhone Poulenc Sa Process for reducing foaming of liquids susceptible to foaming
US3795538A (en) * 1971-10-01 1974-03-05 Midland Silicones Ltd Process for lubricating organic and inorganic fibers
JPS512688A (ja) * 1974-06-27 1976-01-10 Nippon Unicar Co Ltd Shirikoonshohoemarujon
US4005044A (en) * 1975-06-20 1977-01-25 General Electric Company Method of making aqueous antifoam compositions
JPS5236920A (en) * 1975-09-19 1977-03-22 Nippon Hoso Kyokai <Nhk> Color framing unit for electronic editing
US4009117A (en) * 1975-11-05 1977-02-22 Sun Oil Company Of Pennsylvania Method of making invert water-in-oil emulsion
US4177177A (en) * 1976-03-26 1979-12-04 El Aasser Mohamed S Polymer emulsification process
DE2730923C3 (de) * 1977-07-08 1981-10-22 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von wäßrigen feindispersen, lagerstabilen Polysiloxanolemulsionen
GB2079300B (en) * 1980-07-01 1984-04-26 Gen Electric Transparent silicone emulsions
JPS5757063A (en) * 1980-09-24 1982-04-06 Hashimoto Corp Automatic answering telephone set with tape for remote hearing reproduced in high speed
FI68330C (fi) * 1981-04-29 1985-08-12 Radiographic Screen Oy Roentgenkollimator
JPS587335A (ja) * 1981-07-07 1983-01-17 Achilles Corp リボンデイングフオ−ムの製造方法
US4509981A (en) * 1983-06-13 1985-04-09 Sws Silicones Corporation Coating compositions
US4501619A (en) * 1983-11-14 1985-02-26 Dow Corning Corporation Aqueous emulsions of carboxyl-containing silicone fluids and a method for their preparation
CA1260795A (en) * 1985-04-02 1989-09-26 Dipak Narula Emulsification process and emulsions therefrom
CA1272136A (en) * 1985-04-02 1990-07-31 Grish Chandra Substantive skin care compositions comprising a polydiorganosiloxane

Also Published As

Publication number Publication date
MX165179B (es) 1992-10-30
EP0200009A2 (en) 1986-11-05
AU5551986A (en) 1986-10-09
EP0200009B1 (en) 1991-01-30
BR8601443A (pt) 1986-12-09
AU579461B2 (en) 1988-11-24
CA1260794A (en) 1989-09-26
DE3677248D1 (de) 1991-03-07
KR930006262B1 (ko) 1993-07-09
JPS61230734A (ja) 1986-10-15
EP0200009A3 (en) 1988-05-25
US4874547A (en) 1989-10-17
JPH0659401B2 (ja) 1994-08-10

Similar Documents

Publication Publication Date Title
KR860007956A (ko) 2-형태 실리콘 유제 조성물 및 실리콘 유화방법
US4476282A (en) Method of producing finely divided, stable oil-in-water emulsions of organopolysiloxanes
KR950000132A (ko) 실리콘을 함유하는 수중유적형 유화액
US5814411A (en) Water-repellent wallboard
US4532132A (en) Skin care formulations comprising a water-in-mineral oil emulsion and siloxane compositions therefor
DE3564584D1 (en) Aqueous-emulsion compositions for the non-adhering and hydrofugal treatment of cellulosic materials
AU2002224879A1 (en) Process for making silicone emulsions
KR880000519A (ko) 유연재료 피복용 중첨가 유기폴리실록산 조성물의 보관시 안정한 수화 에멀션
US5221339A (en) Heat-conductive silicone oil compound
US5977191A (en) Method for controlling foam
KR870002225A (ko) 실세스키옥산 유탁액의 제조방법
KR950003392A (ko) 오르가노폴리실록산의 수용성분산제
KR900009039A (ko) 발한억제 조성물
DE69012277T2 (de) Silikon-Entschäumer-Zusammensetzung.
GB1600222A (en) Anti-foam silicone composition
KR930021726A (ko) 아미노실리콘을 기재로 한 가교결합조성물
KR900016417A (ko) 부가 경화성 실리콘 감압 접착제
EP0270898B1 (en) Foam control process for highly acidic aqueous systems
KR860003290A (ko) 실리콘 탄성발포체
KR860006513A (ko) 개량된 내연소성 거품으로 전환될 수 있는 유기폴리 실록산 조성물
EP0366133A3 (de) Verfahren zur Herstellung wässriger Emulsionen von hochmolekularen Organopolysiloxanen
KR880009093A (ko) 부식방지용 경화성 실리콘 조성물
GB1261637A (en) Improvements in flame retardant organopolysiloxane elastomer compositions
GB1191289A (en) Method of Emulsifying Highly Viscous Organopolysiloxane Oils in Water
KR900016333A (ko) 실리콘 발포 소재

Legal Events

Date Code Title Description
A201 Request for examination
G160 Decision to publish patent application
E701 Decision to grant or registration of patent right
GRNT Written decision to grant
FPAY Annual fee payment

Payment date: 20000708

Year of fee payment: 8

LAPS Lapse due to unpaid annual fee