JPS55119185A - Manufacture of alpha-phenylglycine - Google Patents
Manufacture of alpha-phenylglycineInfo
- Publication number
- JPS55119185A JPS55119185A JP2665879A JP2665879A JPS55119185A JP S55119185 A JPS55119185 A JP S55119185A JP 2665879 A JP2665879 A JP 2665879A JP 2665879 A JP2665879 A JP 2665879A JP S55119185 A JPS55119185 A JP S55119185A
- Authority
- JP
- Japan
- Prior art keywords
- compartment
- alpha
- cathode
- anode
- resorting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
PURPOSE: To obtain alpha-phenylglycine easily without resorting to complicated processes of conventional methods by reducing electrolytically benzonitrile and CO2 in the cathode compartment in the presence of aluminum chloride and HCl , using an electrolytic cell with a cation exchange membrane.
CONSTITUTION: Benzonitrile and CO2 in the cathode compartment of an electrolytic cell consisting of a cathode, a cathode compartment, an anode, an anode compartment, a cation exchange diaphragm for separation, etc., are reduced electrolytically under a proper eleloctrolysis condition using an approx. 0.1W4N aluminum chloride solution and HCl where an aprotic polar organic solvent containing a quaternary ammonium salt of p-toluenesulfonic acid as a supporting electrolyte is used in the anode compartment. Thus, alpha-phenyl-glycine which is useful as an intermediate for medicines etc. can be easily obtained without resorting to complicated processes by a method entirely different from conventional methods, as shown in the formula.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2665879A JPS55119185A (en) | 1979-03-09 | 1979-03-09 | Manufacture of alpha-phenylglycine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2665879A JPS55119185A (en) | 1979-03-09 | 1979-03-09 | Manufacture of alpha-phenylglycine |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS55119185A true JPS55119185A (en) | 1980-09-12 |
Family
ID=12199516
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2665879A Pending JPS55119185A (en) | 1979-03-09 | 1979-03-09 | Manufacture of alpha-phenylglycine |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS55119185A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013500294A (en) * | 2009-07-29 | 2013-01-07 | シーメンス アクティエンゲゼルシャフト | Method for producing radiolabeled carboxylate |
-
1979
- 1979-03-09 JP JP2665879A patent/JPS55119185A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013500294A (en) * | 2009-07-29 | 2013-01-07 | シーメンス アクティエンゲゼルシャフト | Method for producing radiolabeled carboxylate |
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