JPH11313618A - Mineral (zinc) formulation for livestock gentle to stomach and its production - Google Patents
Mineral (zinc) formulation for livestock gentle to stomach and its productionInfo
- Publication number
- JPH11313618A JPH11313618A JP10162722A JP16272298A JPH11313618A JP H11313618 A JPH11313618 A JP H11313618A JP 10162722 A JP10162722 A JP 10162722A JP 16272298 A JP16272298 A JP 16272298A JP H11313618 A JPH11313618 A JP H11313618A
- Authority
- JP
- Japan
- Prior art keywords
- zinc
- chicken
- tablet
- starch
- coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Fodder In General (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
【０００１】［産業上の利用分野］本発明は、胃にやさ
しい家畜用ミネラル（亜鉛）製剤及びその製造法に関す
る。[0001] The present invention relates to a stomach-friendly veterinary mineral (zinc) preparation and a method for producing the same.
【０００２】［従来の技術］亜鉛は生物の生命維持に欠
かすことのできない必須無機元素の一つで、家畜の飼育
にも重要で、成長の促進や鶏肉・鶏卵の亜鉛の含量を増
加させるために飼料には必ず添加している。そして、亜
鉛は通常炭酸亜鉛、酸化亜鉛、硫酸亜鉛などの亜鉛化合
物が添加されている。[Prior art] Zinc is one of the essential inorganic elements indispensable for maintaining the life of living organisms. Zinc is also important for raising livestock and promotes growth and increases the zinc content of chicken and chicken eggs. Is always added to the feed. Zinc is usually added with zinc compounds such as zinc carbonate, zinc oxide and zinc sulfate.
【０００３】細胞の新陳代謝が盛んになると、亜鉛の消
費も盛んになり、特に産卵鶏は最低５ｍｇ／一日以上の
亜鉛が必要となっている。また、飼料に栄養素を多く添
加すれば鶏卵の方へも多く栄養素が移行し高栄養価の卵
を生産することができるので、亜鉛の場合も飼料に５ｍ
ｇ以上の亜鉛を含有している炭酸亜鉛、酸化亜鉛、硫酸
亜鉛などを添加することが盛んに実行されている。[0003] As the metabolism of cells becomes active, the consumption of zinc becomes active. In particular, laying hens require at least 5 mg of zinc per day. Also, if a large amount of nutrients are added to the feed, a large amount of nutrients can be transferred to the hen's egg to produce eggs with high nutritional value.
Addition of zinc carbonate, zinc oxide, zinc sulfate, etc., containing more than g of zinc has been actively performed.
【０００４】ところが、炭酸亜鉛、酸化亜鉛などは胃内
に入ると胃液中の塩酸と反応して、塩化亜鉛に変化す
る。この塩化亜鉛や硫酸亜鉛は生理作用が激しい物質で
局所粘膜を刺激したり、腐食したりするので、薬品とし
ては劇薬に指定されている。したがって、鶏の飼料に多
量の炭酸亜鉛、酸化亜鉛、硫酸亜鉛を添加すると鶏の体
調に大きな影響を与えることになる。However, when zinc carbonate, zinc oxide, etc. enter the stomach, they react with hydrochloric acid in gastric juice and change into zinc chloride. Zinc chloride and zinc sulfate are highly physiologic substances, and irritate and corrode local mucous membranes. Therefore, adding a large amount of zinc carbonate, zinc oxide, or zinc sulfate to chicken feed has a great effect on the physical condition of the chicken.
【０００５】この大量添加についてはＳｃｏｔｔとＣｒ
ｅｇａｒが２％亜鉛（酸化亜鉛）添加飼料を５〜１３日
間与えると、産卵を停止し、強制換羽の代りの強制休産
ができることを１９７６年に発表している。このことは
塩化亜鉛の激しい生理作用と亜鉛の添加料の上限を示唆
している。[0005] Regarding this large addition, Scott and Cr
In 1976, Egar announced that when fed 2% zinc (zinc oxide) supplemented feed for 5 to 13 days, spawning was stopped and forced leave of labor could be replaced with forced molt. This suggests the severe physiological effects of zinc chloride and the upper limit of zinc additives.
【０００６】［発明が解決しようとする課題］養鶏業者
は鶏に給与する飼料に炭酸亜鉛や酸化亜鉛を添加して、
鶏の成長を促進し、また亜鉛を高度に含有する鶏卵を生
産するため、炭酸亜鉛や酸化亜鉛の添加量をできるだけ
多くしたいと思っているが、塩化亜鉛の副作用のために
その量はあまり多くできないのが現状となっている。[Problems to be Solved by the Invention] Poultry farmers add zinc carbonate or zinc oxide to feeds fed to chickens,
We want to add as much zinc carbonate and zinc oxide as possible to promote chicken growth and produce high-enriched chicken eggs, but the amount is too high due to the side effects of zinc chloride. It is not possible at present.
【０００７】本発明は鶏に給与する亜鉛の量を多くして
も鶏の体に障害を及ぼさず、しかも通常の亜鉛化合物の
給与に比べて亜鉛の吸収がよく、鶏の成長や鶏肉・鶏卵
の亜鉛の含量を高める製剤とその製造法を提供すること
を目的としている。According to the present invention, even if the amount of zinc supplied to a chicken is increased, the body of the chicken is not damaged, and the absorption of zinc is better than that of a normal zinc compound, and the growth of chicken, chicken meat and eggs It is an object of the present invention to provide a preparation for increasing the zinc content of a liposome and a method for producing the same.
【０００８】［課題を解決するための手段］上記目的を
達成するために、つぎの順序に従って製造をおこなう。
酸化亜鉛・炭酸亜鉛・クエン酸亜鉛・酒石酸亜鉛などの
亜鉛化合物１種類〜数種類とメチオニン・トリプトファ
ン・シスチン・スレオニンなどの必須アミノ酸１種類〜
数種類を混合したものに、デンプンや小麦粉などの賦形
剤適量を加えてからデンプンや小麦粉などの糊料を添加
し、顆粒または錠剤を製する。亜鉛化合物とアミノ酸の
配合比は酸化亜鉛１／２グラム当量・炭酸亜鉛１／２グ
ラム当量・クエン酸亜鉛１／３グラム当量・酒石酸亜鉛
１／２グラム当量に対してメチオニン１グラム当量・ト
リプトファン１グラム当量・シスチン１／２グラム当量
・スレオニン１グラム当量以上とする。[Means for Solving the Problems] In order to achieve the above object, manufacturing is performed in the following order.
One type of zinc compound such as zinc oxide, zinc carbonate, zinc citrate, zinc tartrate, etc. and several types of essential amino acids, such as methionine, tryptophan, cystine, threonine, etc.
An appropriate amount of excipient such as starch or flour is added to a mixture of several types, and then a paste such as starch or flour is added to produce granules or tablets. The mixing ratio of the zinc compound to the amino acid is 1/2 gram equivalent of zinc oxide, 1/2 gram equivalent of zinc carbonate, 1/3 gram equivalent of zinc citrate, 1/2 gram equivalent of zinc tartrate, 1 gram equivalent of methionine, and 1 tryptophan. Gram equivalent, cystine 1/2 gram equivalent, threonine 1 gram equivalent or more.
【０００９】製剤の亜鉛・アミノ酸の含量は家畜に給与
する一日量を決め、剤形の大きさと量が、家畜が飼料を
摂取するのに最も好適なものとなるように賦形剤の量を
加減する。[0009] The zinc and amino acid content of the formulation determines the daily dose to be fed to the livestock, and the amount of excipients should be such that the size and amount of the dosage form is most suitable for the livestock to feed. To adjust.
【００１０】次に亜鉛化合物とアミノ酸からなる顆粒や
錠剤にアルギン酸ナトリウム水溶液やカルボキシメチー
ルセルロースナトリウム水溶液などによって表面に０．
０５ｍｍ以上の厚さの腸溶性皮膜をコーティングしてか
ら、さらにこれらの水溶液で表面を湿潤してから牡蛎殻
粉末を適当量塗してから乾燥して製する。Next, a granule or tablet comprising a zinc compound and an amino acid is coated on the surface with an aqueous sodium alginate solution or an aqueous sodium carboxymethyl cellulose solution.
An enteric film having a thickness of at least 05 mm is coated, the surface is further wetted with these aqueous solutions, an appropriate amount of oyster husk powder is applied, and then the product is dried.
【００１１】［作用］酸化亜鉛、炭酸亜鉛、クエン酸亜
鉛、酒石酸亜鉛などの亜鉛化合物はそのまま経口給与す
ると胃中で胃酸と反応して塩化亜鉛となる。そしてこの
塩化亜鉛が胃の粘膜を刺激したり、腐食することになる
が、本発明では顆粒や錠剤の表面には酸に不溶のアルギ
ン酸ナトリウムやカルボキシメチールセルロースナトリ
ウムの皮膜があるので亜鉛化合物は胃酸の影響をうけな
いで腸へ送られる。そして腸液のアルカリ性の作用を受
けて剤皮がとけて顆粒、錠剤が溶解する。[Action] When zinc compounds such as zinc oxide, zinc carbonate, zinc citrate and zinc tartrate are orally fed as they are, they react with stomach acid in the stomach to form zinc chloride. And this zinc chloride will irritate and corrode the stomach mucous membrane, but in the present invention, the surface of granules and tablets has a film of sodium alginate and sodium carboxymethyl cellulose which are insoluble in acid, so the zinc compound is It is sent to the intestine without being affected by stomach acid. Then, the skin is melted by the alkaline action of the intestinal juice, and the granules and tablets are dissolved.
【００１２】顆粒や錠剤の表面に牡蛎殻粉末を塗してお
くのは、鶏の飼料摂取性を高めるためである。The reason why oyster shell powder is applied to the surfaces of granules and tablets is to enhance the feed intake of chickens.
【００１３】腸管における亜鉛の吸収はキレート化合物
の状態になっているときによく吸収される。アミノ酸の
なかではシスチンの亜鉛キレートがもっともよく吸収さ
れるといわれている。[0013] The absorption of zinc in the intestinal tract is well absorbed when it is in the form of a chelating compound. It is said that zinc chelates of cystine are best absorbed among amino acids.
【００１４】亜鉛は通常、胃酸などの酸には溶けるが、
弱アルカリ性液（腸液）には不溶であるが、研究の結
果、クエン酸亜鉛や酒石酸亜鉛は腸液（ＰＨ５．６〜
８）にもよく溶け、沈殿を生じない良好なキレート化合
物であることが分かった。いずれの亜鉛化合物も腸管に
おいてアミノ酸の働きによって吸収されるが、クエン酸
亜鉛と酒石酸亜鉛はより吸収がよいことが分かつた。Zinc is usually soluble in acids such as stomach acid,
Although insoluble in weakly alkaline fluids (intestinal fluid), studies have shown that zinc citrate and zinc tartrate are insoluble in intestinal fluids (PH 5.6-
8) It was found that the compound was a good chelate compound which dissolved well in 8) and did not cause precipitation. All zinc compounds are absorbed by the action of amino acids in the intestinal tract, but it has been found that zinc citrate and zinc tartrate absorb better.
【００１５】［実施例］クエン酸亜鉛５７５ｇとシスチ
ン６３７ｇに４７８０ｇのデンプンを加え混合してか
ら、５％デンプン糊適量を加え造粒してから打錠する。
次に錠剤に５％アルギン酸ナトリウム水溶液で常法によ
って皮層厚０．０５ｍｍ以上の皮膜で錠剤を被覆する。
さらに５％アルギン酸ナトリウム水溶液で錠剤を湿潤し
てから、牡蛎殻粉末適量を塗すことを２〜３回繰返して
から乾燥して製品とする。[Example] 4780 g of starch is added to 575 g of zinc citrate and 637 g of cystine, mixed, and then an appropriate amount of 5% starch paste is added and granulated, followed by tableting.
Next, the tablet is coated with a 5% aqueous solution of sodium alginate with a coating having a skin thickness of 0.05 mm or more by a conventional method.
Further, the tablet is moistened with a 5% aqueous sodium alginate solution, and the application of an appropriate amount of oyster shell powder is repeated two or three times, followed by drying to obtain a product.
【００１６】［発明による効果］ 腸溶性剤皮を採用したので亜鉛化合物は胃内において
生理的に障害を及ぼす塩化亜鉛に変化することなく、腸
内へ移行する。したがって亜鉛の障害を懸念する事な
く、亜鉛を十分に給与することができる。亜鉛化合物
とアミノ酸類を密接するように顆粒や錠剤に一緒に配合
することによつて、腸管における亜鉛に対するアミノ酸
のキレート作用が効率よく行われる。したがって亜鉛化
合物を飼料に配合して給与している従来の方法より吸収
がよい。亜鉛化合物の中でもクエン酸亜鉛、酒石酸亜
鉛はキレート作用がすぐれていて、酸化亜鉛や炭酸亜鉛
をアミノ酸に配合した場合よりも亜鉛の吸収率がよい。[Effects of the Invention] Since an enteric coating is employed, the zinc compound moves into the intestine without being changed to zinc chloride, which causes physiological damage in the stomach. Therefore, it is possible to supply zinc sufficiently without worrying about zinc disorders. By blending the zinc compound and the amino acids together in granules or tablets so as to be in close contact, the chelating action of the amino acids on zinc in the intestinal tract can be efficiently performed. Therefore, the absorption is better than the conventional method in which the zinc compound is added to the feed and fed. Among the zinc compounds, zinc citrate and zinc tartrate have excellent chelating effects, and have a higher zinc absorption rate than when zinc oxide or zinc carbonate is blended with amino acids.
─────────────────────────────────────────────────────
────────────────────────────────────────────────── ───
【手続補正書】[Procedure amendment]
【提出日】平成１０年１２月２８日[Submission date] December 28, 1998
【手続補正１】[Procedure amendment 1]
【補正対象書類名】明細書[Document name to be amended] Statement
【補正対象項目名】０００８[Correction target item name] 0008
【補正方法】変更[Correction method] Change
【補正内容】[Correction contents]
【０００８】［課題を解決するための手段］上記目的を
達成するために、つぎの順序に従って製造をおこなう。
酸化亜鉛・炭酸亜鉛・クエン酸亜鉛・酒石酸亜鉛などの
亜鉛化合物１種類〜数種類とメチオニン・トリプトファ
ン・シスチン・スレオニンなどの必須アミノ酸１種類〜
数種類を混合したものに、デンプンや小麦粉などの賦形
剤適量を加えてからデンプンや小麦粉などの糊料を添加
し、顆粒または錠剤を製する。亜鉛化合物とアミノ酸の
配合比は酸化亜鉛１／２モル・炭酸亜鉛１／２モル・ク
エン酸亜鉛１／３モル・酒石酸亜鉛１／２モルに対して
メチオニン１モル・トリプトファン１モル・シスチン１
／２モル・スレオニン１モル以上とする。[Means for Solving the Problems] In order to achieve the above object, manufacturing is performed in the following order.
One type of zinc compound such as zinc oxide, zinc carbonate, zinc citrate, zinc tartrate, etc. and several types of essential amino acids, such as methionine, tryptophan, cystine, threonine, etc.
An appropriate amount of excipient such as starch or flour is added to a mixture of several types, and then a paste such as starch or flour is added to produce granules or tablets. Zinc compound and compounding ratio of the amino acid methionine 1 mole Tryptophan 1 mole cystine 1 against the zinc oxide ½ mole of zinc carbonate 1/2 mole zinc citrate 1/3 mole zinc tartrate 1/2 mole
/ 2 mol threonine 1 mol or more.
【手続補正２】[Procedure amendment 2]
【補正対象書類名】明細書[Document name to be amended] Statement
【補正対象項目名】００１５[Correction target item name] 0015
【補正方法】変更[Correction method] Change
【補正内容】[Correction contents]
【００１５】［実施例］クエン酸亜鉛５７５ｇとシスチ
ン７２５ｇに４７８０ｇのデンプンを加え混合してか
ら、５％デンプン糊適量を加え造粒してから打錠する。
次に錠剤に５％アルギン酸ナトリウム水溶液で常法によ
って皮層厚０．０５ｍｍ以上の皮膜で錠剤を被覆する。
さらに５％アルギン酸ナトリウム水溶液で錠剤を湿潤し
てから、牡蛎殻粉末適量を塗すことを２〜３回繰返して
から乾燥して製品とする。[Example] 575 g of zinc citrate and 725 g of cystine are mixed with 4780 g of starch, and then an appropriate amount of 5% starch paste is added and granulated, followed by tableting.
Next, the tablet is coated with a 5% aqueous solution of sodium alginate with a coating having a skin thickness of 0.05 mm or more by a conventional method.
Further, the tablet is moistened with a 5% aqueous sodium alginate solution, and the application of an appropriate amount of oyster shell powder is repeated two or three times, followed by drying to obtain a product.
───────────────────────────────────────────────────── フロントページの続き (71)出願人 598076731 井上 京子 東京都杉並区南荻窪１丁目42―10 (72)発明者 井上 義夫 徳島市下助任町２丁目37番地の２ (72)発明者 井上 裕子 徳島市下助任町２丁目37番地の２ (72)発明者 片山 久 徳島市下助任町２丁目37番地の２ (72)発明者 片山 智子 徳島市下助任町２丁目37番地の２ (72)発明者 井上 京子 東京都杉並区南荻窪１丁目42−10 ──────────────────────────────────────────────────続 き Continuing from the front page (71) Applicant 598076731 Kyoko Inoue 1-42-10 Minamiogikubo, Suginami-ku, Tokyo (72) Inventor Yoshio Inoue 2-37-2 Shimosukemincho, Tokushima-shi 2 (72) Inventor Yuko Inoue 2-72, Shimosuke-machi, Tokushima-shi (72) Inventor Hisa Katayama 2-37-2, Shimosuke-machi, Tokushima-shi (72) Inventor Tomoko Katayama 2-37-2, Shimosuke-machi, Tokushima-shi (72) Inventor Inoue Kyoko 1-42-10 Minamiogikubo, Suginami-ku, Tokyo
Claims (2)
石酸亜鉛などの亜鉛化合物１種類〜数種類とメチオニン
・トリプトファン・シスチン・スレオニンなどの必須ア
ミノ酸１種類〜数種類を混合したものに、デンプンや小
麦粉などの賦形剤適量を加えてからデンプンや小麦粉な
どの糊料を添加し、顆粒または錠剤を製し、この顆粒や
錠剤にアルギンナトリウム水溶液やカルボキシメチール
セルロースナトリウム水溶液などによって表面に０．０
５ｍｍ以上の厚さの腸溶性皮膜をコーティングしてか
ら、さらに、これらの水溶液で表面を湿潤してから牡蛎
殻粉末を適当量塗してから乾燥して製品とする。1. A mixture of one or more zinc compounds such as zinc oxide, zinc carbonate, zinc citrate, zinc tartrate and one or more essential amino acids such as methionine, tryptophan, cystine and threonine, and starch or flour. After adding an appropriate amount of excipients such as starch and glue such as starch or flour, granules or tablets are produced, and the surface of the granules or tablets is treated with an aqueous solution of alginine sodium or sodium carboxymethyl cellulose to give
After coating an enteric film having a thickness of 5 mm or more, the surface is wetted with these aqueous solutions, an appropriate amount of oyster shell powder is applied, and then dried to obtain a product.
にやさしい家畜用ミネラル（亜鉛）製剤。2. A stomach-friendly veterinary mineral (zinc) preparation produced by the method of claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10162722A JPH11313618A (en) | 1998-05-06 | 1998-05-06 | Mineral (zinc) formulation for livestock gentle to stomach and its production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10162722A JPH11313618A (en) | 1998-05-06 | 1998-05-06 | Mineral (zinc) formulation for livestock gentle to stomach and its production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH11313618A true JPH11313618A (en) | 1999-11-16 |
Family
ID=15760041
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10162722A Pending JPH11313618A (en) | 1998-05-06 | 1998-05-06 | Mineral (zinc) formulation for livestock gentle to stomach and its production |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH11313618A (en) |
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|---|---|---|---|---|
| WO2004080210A1 (en) * | 2003-03-14 | 2004-09-23 | Boehringer Ingelheim Danmark A/S | Compositions of dietary metals for support of the physiological intestinal development and prevention of diarrhoea |
| JP2012175977A (en) * | 2005-05-18 | 2012-09-13 | Dsm Ip Assets Bv | Composition for administering microorganism into intestine |
| CN102813082A (en) * | 2012-06-21 | 2012-12-12 | 曲湘勇 | Feeds for producing zinc-rich green-shell eggs and raising laying rate and effect determination method |
| US20140099426A1 (en) * | 2012-10-10 | 2014-04-10 | Pharmavite Llc | Natural coating formulas and composition for coating tablets |
| KR20180117874A (en) * | 2017-04-20 | 2018-10-30 | 강곤태 | The method of breeding poultry using the active ingredient containing zinc and the poultry eggs |
| CN108740371A (en) * | 2018-04-04 | 2018-11-06 | 广州智特奇生物科技股份有限公司 | Enteric capsulating material, using coated zinc oxide of the capsulating material and preparation method thereof |
| JP2019534046A (en) * | 2016-11-01 | 2019-11-28 | ジロニックス・アイピー・ホールディングス・ピーティーイー．リミテッド | Gamma-polyglutamic acid and zinc composition |
| CN115006363A (en) * | 2022-06-23 | 2022-09-06 | 上海信谊万象药业股份有限公司 | Oyster calcium carbonate chewable tablets and preparation method thereof |
| US11944640B2 (en) | 2016-11-01 | 2024-04-02 | Xylonix PTE. LTD. | Zinc-[gamma]-PGA compositions and methods for treating cancer |
-
1998
- 1998-05-06 JP JP10162722A patent/JPH11313618A/en active Pending
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| WO2004080210A1 (en) * | 2003-03-14 | 2004-09-23 | Boehringer Ingelheim Danmark A/S | Compositions of dietary metals for support of the physiological intestinal development and prevention of diarrhoea |
| JP2012175977A (en) * | 2005-05-18 | 2012-09-13 | Dsm Ip Assets Bv | Composition for administering microorganism into intestine |
| CN102813082A (en) * | 2012-06-21 | 2012-12-12 | 曲湘勇 | Feeds for producing zinc-rich green-shell eggs and raising laying rate and effect determination method |
| US20140099426A1 (en) * | 2012-10-10 | 2014-04-10 | Pharmavite Llc | Natural coating formulas and composition for coating tablets |
| WO2014059045A1 (en) * | 2012-10-10 | 2014-04-17 | Pharmavite Llc | Natural coating formulas and composition for coating tablets |
| JP2015533120A (en) * | 2012-10-10 | 2015-11-19 | ファーマバイト エルエルシー | Natural coating formulations and compositions for coating tablets |
| JP2019534046A (en) * | 2016-11-01 | 2019-11-28 | ジロニックス・アイピー・ホールディングス・ピーティーイー．リミテッド | Gamma-polyglutamic acid and zinc composition |
| US11944640B2 (en) | 2016-11-01 | 2024-04-02 | Xylonix PTE. LTD. | Zinc-[gamma]-PGA compositions and methods for treating cancer |
| KR20180117874A (en) * | 2017-04-20 | 2018-10-30 | 강곤태 | The method of breeding poultry using the active ingredient containing zinc and the poultry eggs |
| CN108740371A (en) * | 2018-04-04 | 2018-11-06 | 广州智特奇生物科技股份有限公司 | Enteric capsulating material, using coated zinc oxide of the capsulating material and preparation method thereof |
| CN108740371B (en) * | 2018-04-04 | 2021-07-30 | 广州智特奇生物科技股份有限公司 | Enteric coating material, zinc oxide coated by coating material and preparation method thereof |
| CN115006363A (en) * | 2022-06-23 | 2022-09-06 | 上海信谊万象药业股份有限公司 | Oyster calcium carbonate chewable tablets and preparation method thereof |
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