JPH10141341A - High strength bolt excellent in delayed fracture - Google Patents

High strength bolt excellent in delayed fracture

Info

Publication number
JPH10141341A
JPH10141341A JP30169596A JP30169596A JPH10141341A JP H10141341 A JPH10141341 A JP H10141341A JP 30169596 A JP30169596 A JP 30169596A JP 30169596 A JP30169596 A JP 30169596A JP H10141341 A JPH10141341 A JP H10141341A
Authority
JP
Japan
Prior art keywords
delayed fracture
strength
bolt
hardness
surface hardness
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP30169596A
Other languages
Japanese (ja)
Inventor
Tetsuo Shiragami
哲夫 白神
Tatsuo Maeda
龍男 前田
Tomoyuki Yokota
智之 横田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Engineering Corp
Original Assignee
NKK Corp
Nippon Kokan Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NKK Corp, Nippon Kokan Ltd filed Critical NKK Corp
Priority to JP30169596A priority Critical patent/JPH10141341A/en
Publication of JPH10141341A publication Critical patent/JPH10141341A/en
Pending legal-status Critical Current

Links

Abstract

PROBLEM TO BE SOLVED: To improve a delayed fracture characteristic by making those of inner hardness, surface hardness and decarburizating depth satisfy the specific range, in case of a bolt using such steel as containing more than the specified amount of carbon. SOLUTION: Carbon C is necessary to secure tensile strength by means of quench-hardening and tempering processes, supposing that it is less than 0.3%, the desired tensile strength is not secured, it should be more than 0.3%. In addition, if surface hardness is more than HV250, delayed fracture sensibility becomes heightened so that its should be set to be less than HV250. In addition, supposing that decarburizing depth is less than 0.1mm, there is no effect to check the delayed fracture even if the surface hardness is low. Likewise, if it exceeds 0.3mm, variations are apt to come out in strength at the bolt body. Therefore, the decarburizing depth should be more than 1mm but less than 0.3mm. With this constitution, in such a high strength bolt as being more than 1420N/mm<2> , an improvement in a delayed fracture characteristic due to decarburization is made so as to be securable.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、遅れ破壊特性に優
れた高強度ボルトに関する。
[0001] The present invention relates to a high-strength bolt excellent in delayed fracture characteristics.

【0002】[0002]

【従来の技術】高強度ボルトはJIS B 1186 「摩擦接合
用高力六角ボルト・六角ナット・平座金のセット」やJI
S B 1051 「鋼製のボルト・小ねじの機械的性質」で強
度が規格化されているが、遅れ破壊が問題となるため、
1200N/mm2 級までの強度となっている。一方
で、自動車の軽量化や建築物の高層化に対応し、更なる
高強度化が要望されているが、1200N/mm2 以上
の強度の鋼は未だ確立されていない。遅れ破壊の起点は
表面であり、表面を軟化し、遅れ破壊感受性に優れた鋼
あるいはボルトを造る考え方がある。軟化法では一般的
に脱炭が考えられるが、この思想で出されたものとし
て、特開昭61-79015号公報、特開昭61-82014号公報及び
特開昭62-267420 号公報がある。
[Prior art] High-strength bolts are JIS B 1186 "Set of high-strength hexagon bolts, hexagon nuts and flat washers for friction welding" and JI
SB 1051 The strength is standardized in “Mechanical properties of steel bolts and small screws”, but delayed fracture is a problem.
And it has a strength of up to 1200N / mm 2 class. On the other hand, in order to cope with the reduction in the weight of automobiles and the height of buildings, further strengthening is demanded, but steel having a strength of 1200 N / mm 2 or more has not yet been established. The starting point of delayed fracture is the surface, and there is a concept of softening the surface and producing steel or bolt having excellent delayed fracture sensitivity. In the softening method, decarburization is generally considered, and as a result of this idea, there are JP-A-61-79015, JP-A-61-82014 and JP-A-62-267420. .

【0003】[0003]

【発明が解決しようとする課題】しかしながら、特開昭
61-79015号公報では脱炭を用いるとは言っても、表面硬
さがHV295〜383と比較的高い上、脱炭深さの規
定がなく、遅れ破壊の完全な防止は難しい。特開昭61-8
2014号公報も表面硬さがHV250〜350と比較的高
く、脱炭深さを規定しているものの0.01〜0.1m
mと浅いため、遅れ破壊の完全な防止は難しい。特開昭
62-267420 号公報は高Si添加鋼を用い、直接焼入れし
たものであり、ボルトへの適用は難しい。本発明の目的
は、上記した問題点を解決し、遅れ破壊特性に優れた引
張強さ:1420N/mm2 超えの高強度ボルトを提供
することにある。
SUMMARY OF THE INVENTION However, Japanese Patent Application Laid-Open
In Japanese Patent Application Laid-Open No. 61-79015, although decarburization is used, the surface hardness is relatively high at HV 295 to 383, and the decarburization depth is not specified, so that it is difficult to completely prevent delayed fracture. JP-A-61-8
No. 2014 also has a relatively high surface hardness of HV250 to 350 and defines the decarburization depth, but it is 0.01 to 0.1 m.
m, it is difficult to completely prevent delayed fracture. JP
JP-A-62-267420 uses high Si-added steel and is directly quenched, and is difficult to apply to bolts. An object of the present invention is to solve the above-mentioned problems and to provide a high-strength bolt excellent in delayed fracture characteristics and having a tensile strength of more than 1420 N / mm 2 .

【0004】[0004]

【課題を解決するための手段】前記課題を解決し目的を
達成するために、本発明は以下に示す手段を用いてい
る。 (1)本発明のボルトは、重量%(以下%は重量%を示
す)で、C>0.3%を含有する鋼を用いたボルトであ
って、内部硬さ:HV>430、表面硬さ:HV<25
0及び0.1mm<脱炭深さ≦0.3mmを満たすこと
を特徴とする引張強さ:1420N/mm2 超えの遅れ
破壊特性に優れた高強度ボルトである。
In order to solve the above problems and achieve the object, the present invention uses the following means. (1) The bolt of the present invention is a bolt using steel containing C> 0.3% by weight (hereinafter,% indicates weight%), and has an internal hardness: HV> 430 and a surface hardness. Sa: HV <25
It is a high-strength bolt excellent in delayed fracture characteristics with a tensile strength of more than 1420 N / mm 2 characterized by satisfying 0 and 0.1 mm <decarburization depth ≦ 0.3 mm.

【0005】[0005]

【発明の実施の形態】本発明者は、1420N/mm2
超えの高強度ボルトにおいて、脱炭による遅れ破壊特性
の向上を確実なものにするよう、鋭意研究を重ねた。そ
の結果、1420N/mm2 超えの高強度ボルトにおい
て、脱炭による遅れ破壊特性を確実に向上させるために
は、ボルトの内部硬さ、表面硬さ及び脱炭深さを最適化
することが有効であるという知見を得た。
DETAILED DESCRIPTION OF THE INVENTION The present inventors have, 1420N / mm 2
For high-strength bolts exceeding that, we have conducted intensive studies to ensure the improvement of delayed fracture characteristics by decarburization. As a result, the high-strength bolts exceeding 1420N / mm 2, in order to reliably improve the delayed fracture due to decarburization, the internal hardness of the bolt, effective to optimize the surface hardness and decarburization depth Was obtained.

【0006】この知見に基づき、本発明者は、高強度ボ
ルトの内部硬さ、表面硬さ及び脱炭深さを一定範囲内に
制限するようにして、遅れ破壊特性に優れた引張強さ:
1420N/mm2 超えの本発明の高強度ボルトを見出
し、本発明を完成させた。すなわち、本発明は鋼組成及
びボルトの内部硬さ、表面硬さ及び脱炭深さを下記範囲
に限定することにより、遅れ破壊特性に優れた引張強
さ:1420N/mm2 超えの高強度ボルトを提供する
ことができる。
[0006] Based on this finding, the present inventors have limited the internal hardness, surface hardness and decarburization depth of the high-strength bolt to certain ranges, and have a tensile strength excellent in delayed fracture characteristics:
A high-strength bolt of the present invention exceeding 1420 N / mm 2 was found, and the present invention was completed. That is, the present invention limits the steel composition and the internal hardness, surface hardness and decarburization depth of the bolt to the following ranges, thereby providing a tensile strength excellent in delayed fracture characteristics: a high-strength bolt exceeding 1420 N / mm 2. Can be provided.

【0007】以下に本発明の成分添加理由、成分限定理
由、ボルトの内部硬さ、表面硬さ及び脱炭深さの限定理
由について説明する。 (1)成分組成範囲 C>0.3% Cは焼入れ焼戻し処理により引張強度を確保するために
必要であり、0.3%以下では所望の引張強度が得られ
ない。従って、C量は0.3%超えである。
The reasons for adding the components of the present invention, the reasons for limiting the components, and the reasons for limiting the internal hardness, surface hardness and decarburization depth of the bolt will be described. (1) Component composition range C> 0.3% C is necessary to secure tensile strength by quenching and tempering, and if it is 0.3% or less, a desired tensile strength cannot be obtained. Therefore, the C amount exceeds 0.3%.

【0008】また、Si,P,S,は本発明の効果を阻
害しない範囲で、それぞれ0.5%、0.015%、
0.015%の混入は許容される。また、必要に応じて
Mn,Cr,Mo,Niを、それぞれ、<2%、<2
%、<0.5%、<2%添加することも可能である。 (2)ボルトの内部硬さ、表面硬さ及び脱炭深さの範囲 内部硬さ>HV430 内部硬さがHV430以下では所望の引張強度を確保で
きない。従って、HV430超えである。
Further, Si, P, S, are 0.5%, 0.015%, and 0.5%, respectively, within a range not to impair the effects of the present invention.
A mixing of 0.015% is acceptable. If necessary, Mn, Cr, Mo, and Ni may be set to <2% and <2%, respectively.
%, <0.5%, <2%. (2) Range of internal hardness, surface hardness and decarburization depth of bolt Internal hardness> HV430 If the internal hardness is HV430 or less, a desired tensile strength cannot be secured. Therefore, it exceeds HV430.

【0009】表面硬さ<HV250 表面硬さがHV250以上では遅れ破壊感受性が高い。
従って、HV250未満である。 0.1mm<脱炭深さ≦0.3mm 脱炭深さが0.1mm以下では表面硬さが低くても遅れ
破壊抑制の効果がない。また、0.3mmを超えるとボ
ルト実体での強度にばらつきが出やすい。従って、0.
1mm超えで0.3mm以下である。
Surface hardness <HV250 When the surface hardness is HV250 or more, the delayed fracture sensitivity is high.
Therefore, it is less than HV250. 0.1 mm <decarburization depth ≦ 0.3 mm When the decarburization depth is 0.1 mm or less, there is no effect of suppressing delayed fracture even if the surface hardness is low. On the other hand, if it exceeds 0.3 mm, the strength of the bolt body tends to vary. Therefore, 0.
More than 1 mm and 0.3 mm or less.

【0010】なお、上記(2)の範囲に調整するための
鋼の熱処理条件については、本発明では特に規定しない
が、焼入れ温度を750〜900℃に制御することが好
ましい。
The conditions for heat treatment of the steel for adjusting to the range of the above (2) are not particularly defined in the present invention, but it is preferable to control the quenching temperature to 750 to 900 ° C.

【0011】900℃を超えて焼入れした場合、結晶粒
の粗大化により靭性が低下するため、上限を900℃と
するのが好ましい。一方、750℃未満ではフェライト
分率が増え、必要な強度が出ないため、また脱炭深さが
浅いため、下限を750℃とするのが好ましい。
When quenching is performed at a temperature exceeding 900 ° C., the toughness is reduced due to coarsening of crystal grains. Therefore, the upper limit is preferably set to 900 ° C. On the other hand, if the temperature is lower than 750 ° C, the lower limit is preferably set to 750 ° C because the ferrite fraction increases and the required strength is not obtained and the decarburization depth is shallow.

【0012】上記の鋼成分範囲及びボルトの内部硬さ、
表面硬さ及び脱炭深さの範囲に調整することにより、遅
れ破壊特性に優れた引張強さ:1420N/mm2 超え
の高強度ボルトを得ることが可能である。以下に本発明
の実施例を挙げ、本発明の効果を立証する。
[0012] The above steel composition range and the internal hardness of the bolt,
By adjusting the surface hardness and the decarburization depth within the ranges, it is possible to obtain a high-strength bolt excellent in delayed fracture characteristics and having a tensile strength of more than 1420 N / mm 2 . Hereinafter, examples of the present invention will be described to demonstrate the effects of the present invention.

【0013】[0013]

【実施例】【Example】

(実施例1)SCM435(C:0.35%,Si:0.23
%,Mn:0.77%,P:0.009 %,S:0.008 %,C
r:1.06%,Mo:0.15%)のM22ボルトを用い、焼
入れ焼き戻しを行い、所定の強度を付与した。この際、
雰囲気制御を行い、脱炭性とし、焼入れ温度を750〜
900℃に制御し、内部硬さ、表面硬さ及び脱炭深さを
変化させた。熱処理後、ボルト軸部を切断し研磨後、硬
さをマイクロビッカース硬度計で測定した。
(Example 1) SCM435 (C: 0.35%, Si: 0.23
%, Mn: 0.77%, P: 0.009%, S: 0.008%, C
(r: 1.06%, Mo: 0.15%), quenching and tempering were performed using M22 bolts to give a predetermined strength. On this occasion,
Atmosphere control, decarburization, quenching temperature 750 ~
The temperature was controlled at 900 ° C., and the internal hardness, surface hardness, and decarburization depth were changed. After the heat treatment, the bolt shaft was cut and polished, and the hardness was measured with a micro Vickers hardness meter.

【0014】硬さは表面から0.025mm間隔で0.
5mmまで測定し、内部は1mm間隔で測定した。表面
硬さは表面から0.025mmの硬さ、内部硬さは表面
から0.5mmより内部の硬さの平均値とした。脱炭深
さは表面硬さが内部硬さと同等になる位置とした。強度
はボルト実体で引張試験を行い、評価した。
The hardness is 0.1 at an interval of 0.025 mm from the surface.
The measurement was performed up to 5 mm, and the inside was measured at 1 mm intervals. The surface hardness was a hardness of 0.025 mm from the surface, and the internal hardness was an average value of the internal hardness from 0.5 mm from the surface. The decarburization depth was set at a position where the surface hardness was equal to the internal hardness. The strength was evaluated by performing a tensile test on a bolt body.

【0015】遅れ破壊試験は溝付きの2枚重ねの鋼板に
耐力点締め付けを行った供試ボルト100本を3.5%
食塩水中で乾湿繰り返し(1日浸漬、1日乾燥で6カ月
間)を行い、破断本数で評価した。
In the delayed fracture test, 3.5% of 100 test bolts tightened at a proof stress point on a two-ply grooved steel plate were used.
The samples were repeatedly dried and wet in a saline solution (immersion for 1 day, drying for 1 day for 6 months) and evaluated by the number of breaks.

【0016】結果を表1に示す。No.1〜3は本発明
例であり、No.4〜6は比較例である。本発明例のN
o.1〜3は、それぞれ100本の試験を行い、1本の
破断もなかった。
The results are shown in Table 1. No. Nos. 1 to 3 are examples of the present invention. 4 to 6 are comparative examples. N of the present invention example
o. In each of Nos. 1 to 3, 100 tests were performed, and there was no breakage.

【0017】これに対して、比較例のNo.4は表面硬
さが高く、No.5は脱炭深さが浅く、それぞれ本発明
の範囲から外れており、いずれも遅れ破壊特性に劣る。
また、No.6は脱炭をしない通常のボルトでこの場合
は全数破断してしまった。
On the other hand, the comparative example No. No. 4 has a high surface hardness. No. 5 has a shallow decarburization depth, which is out of the range of the present invention, and all have poor delayed fracture characteristics.
In addition, No. Reference numeral 6 denotes a normal bolt which is not decarburized. In this case, all bolts are broken.

【0018】[0018]

【表1】 [Table 1]

【0019】(実施例2)S45C(C:0.44%,S
i:0.26%,Mn:0.81%,P:0.009 %,S:0.007
%,Cr:0.16%)のM12ボルトを用い、実施例1と
同様の試験を行った。
(Example 2) S45C (C: 0.44%, S
i: 0.26%, Mn: 0.81%, P: 0.009%, S: 0.007
%, Cr: 0.16%), and the same test as in Example 1 was performed.

【0020】結果を表2に示す。No.1〜3は本発明
例であり、No.4〜6は比較例である。本発明例のN
o.1〜3は、それぞれ100本の試験を行い、1本の
破断もなかった。
The results are shown in Table 2. No. Nos. 1 to 3 are examples of the present invention. 4 to 6 are comparative examples. N of the present invention example
o. In each of Nos. 1 to 3, 100 tests were performed, and there was no breakage.

【0021】これに対して、比較例のNo.4は表面硬
さが高く、No.5は脱炭深さが浅く、それぞれ本発明
の範囲から外れており、いずれも遅れ破壊特性に劣る。
また、No.6は脱炭をしない通常のボルトでこの場合
は全数破断してしまった。
On the other hand, the comparative example No. No. 4 has a high surface hardness. No. 5 has a shallow decarburization depth, which is out of the range of the present invention, and all have poor delayed fracture characteristics.
In addition, No. Reference numeral 6 denotes a normal bolt which is not decarburized. In this case, all bolts are broken.

【0022】[0022]

【表2】 [Table 2]

【0023】[0023]

【発明の効果】本発明によれば、鋼組成及びボルトの内
部硬さ、表面硬さ及び脱炭深さを特定することにより、
1420N/mm2 超えの強度を有する高強度ボルトで
あっても、遅れ破壊を生じない遅れ破壊特性に優れた高
強度ボルトを提供することができる。また、この技術は
高強度ボルト以外にもPC鋼棒他の高強度鋼においても
適用できるなど、産業上極めて有用な効果をもたらすも
のである。
According to the present invention, by specifying the steel composition and the internal hardness, surface hardness and decarburization depth of the bolt,
Even with a high-strength bolt having a strength exceeding 1420 N / mm 2, it is possible to provide a high-strength bolt excellent in delayed fracture characteristics that does not cause delayed fracture. In addition, this technique has an industrially very useful effect, for example, it can be applied to high-strength steels such as PC steel bars in addition to high-strength bolts.

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 重量%で、C>0.3%を含有する鋼を
用いたボルトであって、内部硬さ:HV>430、表面
硬さ:HV<250及び0.1mm<脱炭深さ≦0.3
mmを満たすことを特徴とする引張強さ:1420N/
mm2 超えの遅れ破壊特性に優れた高強度ボルト。
1. A bolt made of steel containing C> 0.3% by weight, wherein the internal hardness is HV> 430 and the surface hardness is HV <250 and 0.1 mm <decarburization depth. S ≦ 0.3
mm, tensile strength: 1420 N /
mm 2 over delayed fracture properties in excellent high-strength bolts.
JP30169596A 1996-11-13 1996-11-13 High strength bolt excellent in delayed fracture Pending JPH10141341A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP30169596A JPH10141341A (en) 1996-11-13 1996-11-13 High strength bolt excellent in delayed fracture

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP30169596A JPH10141341A (en) 1996-11-13 1996-11-13 High strength bolt excellent in delayed fracture

Publications (1)

Publication Number Publication Date
JPH10141341A true JPH10141341A (en) 1998-05-26

Family

ID=17900044

Family Applications (1)

Application Number Title Priority Date Filing Date
JP30169596A Pending JPH10141341A (en) 1996-11-13 1996-11-13 High strength bolt excellent in delayed fracture

Country Status (1)

Country Link
JP (1) JPH10141341A (en)

Cited By (5)

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WO2011111872A1 (en) * 2010-03-11 2011-09-15 新日本製鐵株式会社 High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
WO2011111873A1 (en) * 2010-03-11 2011-09-15 新日本製鐵株式会社 High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
WO2019150434A1 (en) * 2018-01-30 2019-08-08 日産自動車株式会社 Bolt

Cited By (16)

* Cited by examiner, † Cited by third party
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CN102597543A (en) * 2009-09-10 2012-07-18 独立行政法人物质·材料研究机构 High-strength bolt
WO2011030853A1 (en) * 2009-09-10 2011-03-17 独立行政法人物質・材料研究機構 High-strength bolt
US8876451B2 (en) 2009-09-10 2014-11-04 National Institute For Materials Science High-strength bolt
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JP5135557B2 (en) * 2010-03-11 2013-02-06 新日鐵住金株式会社 High-strength steel material and high-strength bolt excellent in delayed fracture resistance
JP5177323B2 (en) * 2010-03-11 2013-04-03 新日鐵住金株式会社 High-strength steel material and high-strength bolt excellent in delayed fracture resistance
WO2011111873A1 (en) * 2010-03-11 2011-09-15 新日本製鐵株式会社 High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
EP2546380A4 (en) * 2010-03-11 2013-12-25 Nippon Steel & Sumitomo Metal Corp High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
KR101366375B1 (en) * 2010-03-11 2014-02-24 신닛테츠스미킨 카부시키카이샤 High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
WO2011111872A1 (en) * 2010-03-11 2011-09-15 新日本製鐵株式会社 High-strength steel and high-strength bolt with excellent resistance to delayed fracture, and manufacturing method therefor
US8951365B2 (en) 2010-03-11 2015-02-10 Nippon Steel & Sumitomo Metal Corporation High strength steel and high strength bolt excellent in delayed fracture resistance and methods of production of same
WO2019150434A1 (en) * 2018-01-30 2019-08-08 日産自動車株式会社 Bolt
JPWO2019150434A1 (en) * 2018-01-30 2021-01-14 日産自動車株式会社 bolt
US11333189B2 (en) 2018-01-30 2022-05-17 Nissan Motor Co., Ltd. Bolt

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