JPH0581524B2 - - Google Patents
Info
- Publication number
- JPH0581524B2 JPH0581524B2 JP58070743A JP7074383A JPH0581524B2 JP H0581524 B2 JPH0581524 B2 JP H0581524B2 JP 58070743 A JP58070743 A JP 58070743A JP 7074383 A JP7074383 A JP 7074383A JP H0581524 B2 JPH0581524 B2 JP H0581524B2
- Authority
- JP
- Japan
- Prior art keywords
- silica
- solution
- sodium silicate
- silicate solution
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 113
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 75
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 46
- 239000004115 Sodium Silicate Substances 0.000 claims description 43
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 43
- 239000006227 byproduct Substances 0.000 claims description 41
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 19
- 239000011575 calcium Substances 0.000 claims description 16
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 12
- 239000000920 calcium hydroxide Substances 0.000 claims description 12
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 12
- 239000011734 sodium Substances 0.000 claims description 8
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 7
- MKTRXTLKNXLULX-UHFFFAOYSA-P pentacalcium;dioxido(oxo)silane;hydron;tetrahydrate Chemical compound [H+].[H+].O.O.O.O.[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O MKTRXTLKNXLULX-UHFFFAOYSA-P 0.000 claims description 5
- 230000002194 synthesizing effect Effects 0.000 claims description 5
- UGGQKDBXXFIWJD-UHFFFAOYSA-N calcium;dihydroxy(oxo)silane;hydrate Chemical compound O.[Ca].O[Si](O)=O UGGQKDBXXFIWJD-UHFFFAOYSA-N 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000000243 solution Substances 0.000 description 78
- 239000000377 silicon dioxide Substances 0.000 description 54
- 238000000034 method Methods 0.000 description 34
- 238000001914 filtration Methods 0.000 description 20
- 239000000126 substance Substances 0.000 description 18
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 17
- 239000010457 zeolite Substances 0.000 description 17
- 229910021536 Zeolite Inorganic materials 0.000 description 16
- 238000004519 manufacturing process Methods 0.000 description 13
- 238000004090 dissolution Methods 0.000 description 11
- 230000000704 physical effect Effects 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 8
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 8
- 229910052791 calcium Inorganic materials 0.000 description 8
- 229910001388 sodium aluminate Inorganic materials 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 4
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000019353 potassium silicate Nutrition 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- -1 xonotrite Chemical compound 0.000 description 3
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000000292 calcium oxide Substances 0.000 description 2
- 235000012255 calcium oxide Nutrition 0.000 description 2
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 150000002222 fluorine compounds Chemical class 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229940043430 calcium compound Drugs 0.000 description 1
- 150000001674 calcium compounds Chemical class 0.000 description 1
- 239000000378 calcium silicate Substances 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000006063 cullet Substances 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000000271 synthetic detergent Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Silicon Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7074383A JPS59195518A (ja) | 1983-04-21 | 1983-04-21 | 珪酸ナトリウム溶液の製造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7074383A JPS59195518A (ja) | 1983-04-21 | 1983-04-21 | 珪酸ナトリウム溶液の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS59195518A JPS59195518A (ja) | 1984-11-06 |
JPH0581524B2 true JPH0581524B2 (ko) | 1993-11-15 |
Family
ID=13440294
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP7074383A Granted JPS59195518A (ja) | 1983-04-21 | 1983-04-21 | 珪酸ナトリウム溶液の製造方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS59195518A (ko) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102707461B (zh) * | 2012-05-31 | 2015-03-04 | 福建华科光电有限公司 | 偏振无关光学隔离器的制造方法、光学件键合工艺和溶液 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4984999A (ko) * | 1972-12-11 | 1974-08-15 | ||
JPS49113814A (ko) * | 1973-03-05 | 1974-10-30 | ||
JPS49134599A (ko) * | 1973-04-28 | 1974-12-25 |
-
1983
- 1983-04-21 JP JP7074383A patent/JPS59195518A/ja active Granted
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4984999A (ko) * | 1972-12-11 | 1974-08-15 | ||
JPS49113814A (ko) * | 1973-03-05 | 1974-10-30 | ||
JPS49134599A (ko) * | 1973-04-28 | 1974-12-25 |
Also Published As
Publication number | Publication date |
---|---|
JPS59195518A (ja) | 1984-11-06 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US5215732A (en) | Method for producing alkali metal silicates by heating cristobalite or tempered quartz sand with naoh or koh under atmospheric pressure | |
CA1095877A (en) | Process for producing silicon-dioxide-containing waste fines to crystalline zeolitic type-a molecular sieves | |
US5000933A (en) | Process for hydrothermal production of sodium silicate solutions | |
CA2001063C (en) | Method for producing aqueous solutions of basic poly aluminum sulphate | |
CA1093535A (en) | Process for processing silicon-dioxide-containing air- borne waste fines to crystalline type-y molecular sieves having a faujasite structure | |
JPH0648725A (ja) | ベータ型ゼオライトの製造方法 | |
JPH01278419A (ja) | 粒状の結晶化されたジルコニウム酸化物からのジルコニウム酸化物水和物の製造方法 | |
JPH01119510A (ja) | 生物系シリカから可溶性シリケートを製造する方法 | |
US3898319A (en) | Process for preparing zeolite Y | |
GB2038301A (en) | Process for the production of zeolite A | |
US4693878A (en) | Process for the production of soluble alkali silicates | |
EP1027285B1 (en) | Process for production of zeolites from raw materials containing alkali alumino hydro-silicates | |
JPH0581524B2 (ko) | ||
JPS63162520A (ja) | 合成マザイトの製造方法 | |
CA2057588C (en) | A process to obtain zeolite 4a starting from bauxite | |
KR960010897B1 (ko) | 비표면적이 향상된 제올라이트 흡착제 제조방법 | |
KR20060109596A (ko) | 알루미늄재를 이용한 소듐알루미네이트용액의 제조방법 | |
JPS62132724A (ja) | アモルフアスアルミノシリケ−トの製造方法 | |
JPH0764550B2 (ja) | アモルフアスアルミノシリケ−トの製造方法 | |
JPH09227116A (ja) | 層状ケイ酸塩の製造方法 | |
CN116022792A (zh) | 一种硅砂碱溶提纯联产水化硅酸钙的方法 | |
JPH0516372B2 (ko) | ||
SU819059A1 (ru) | Способ получени гидрогаллосиликатаНАТРи ТипА НАТРОлиТА | |
JPS6321213A (ja) | 高純度シリカの製造方法 | |
JPS596810B2 (ja) | ゼオライトの製造方法 |