JPH0449570B2 - - Google Patents

Info

Publication number: JPH0449570B2
Authority: JP; Japan
Prior art keywords: parts; silicone oil; fine particles; polysiloxane; polymer
Prior art date: 1983-12-29
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP24805483A

Other languages

English (en)

Japanese (ja)

Other versions

JPS60141714A (ja

Inventor

Hiroshi Mori

Masaharu Fujimoto

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Mitsubishi Rayon Co Ltd

Original Assignee

Mitsubishi Rayon Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-12-29

Filing date

1983-12-29

Publication date

1992-08-11

1983-12-29 Application filed by Mitsubishi Rayon Co Ltd filed Critical Mitsubishi Rayon Co Ltd

1983-12-29 Priority to JP24805483A priority Critical patent/JPS60141714A/ja

1985-07-26 Publication of JPS60141714A publication Critical patent/JPS60141714A/ja

1992-08-11 Publication of JPH0449570B2 publication Critical patent/JPH0449570B2/ja

Status Granted legal-status Critical Current

Links

-1 polysiloxane Polymers 0.000 claims description 42
229920002545 silicone oil Polymers 0.000 claims description 39
229920001296 polysiloxane Polymers 0.000 claims description 26
239000010419 fine particle Substances 0.000 claims description 24
239000000203 mixture Substances 0.000 claims description 17
229920000728 polyester Polymers 0.000 claims description 15
239000002904 solvent Substances 0.000 claims description 11
238000000034 method Methods 0.000 claims description 10
229920000058 polyacrylate Polymers 0.000 claims description 8
238000010438 heat treatment Methods 0.000 claims description 7
230000000379 polymerizing effect Effects 0.000 claims description 7
QPKOBORKPHRBPS-UHFFFAOYSA-N bis(2-hydroxyethyl) terephthalate Chemical compound OCCOC(=O)C1=CC=C(C(=O)OCCO)C=C1 QPKOBORKPHRBPS-UHFFFAOYSA-N 0.000 claims description 4
239000002245 particle Substances 0.000 claims description 3
239000003795 chemical substances by application Substances 0.000 claims 1
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 27
238000003756 stirring Methods 0.000 description 21
ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 20
239000006185 dispersion Substances 0.000 description 17
239000012299 nitrogen atmosphere Substances 0.000 description 16
229920000139 polyethylene terephthalate Polymers 0.000 description 14
239000005020 polyethylene terephthalate Substances 0.000 description 14
229920000642 polymer Polymers 0.000 description 14
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 12
239000004205 dimethyl polysiloxane Substances 0.000 description 9
235000013870 dimethyl polysiloxane Nutrition 0.000 description 9
229920000435 poly(dimethylsiloxane) Polymers 0.000 description 9
238000006068 polycondensation reaction Methods 0.000 description 7
238000006116 polymerization reaction Methods 0.000 description 7
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
238000001816 cooling Methods 0.000 description 6
239000011859 microparticle Substances 0.000 description 6
238000006243 chemical reaction Methods 0.000 description 5
239000000839 emulsion Substances 0.000 description 5
238000004519 manufacturing process Methods 0.000 description 5
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 4
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 4
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
125000004122 cyclic group Chemical group 0.000 description 4
RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 description 4
229920005573 silicon-containing polymer Polymers 0.000 description 4
WXNZTHHGJRFXKQ-UHFFFAOYSA-N 4-chlorophenol Chemical compound OC1=CC=C(Cl)C=C1 WXNZTHHGJRFXKQ-UHFFFAOYSA-N 0.000 description 3
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 3
239000003054 catalyst Substances 0.000 description 3
125000000524 functional group Chemical group 0.000 description 3
239000002609 medium Substances 0.000 description 3
239000000155 melt Substances 0.000 description 3
POPACFLNWGUDSR-UHFFFAOYSA-N methoxy(trimethyl)silane Chemical compound CO[Si](C)(C)C POPACFLNWGUDSR-UHFFFAOYSA-N 0.000 description 3
229910000077 silane Inorganic materials 0.000 description 3
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
150000003739 xylenols Chemical class 0.000 description 3
IKYAJDOSWUATPI-UHFFFAOYSA-N 3-[dimethoxy(methyl)silyl]propane-1-thiol Chemical compound CO[Si](C)(OC)CCCS IKYAJDOSWUATPI-UHFFFAOYSA-N 0.000 description 2
239000004342 Benzoyl peroxide Substances 0.000 description 2
OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 2
VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 2
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
125000003545 alkoxy group Chemical group 0.000 description 2
235000019400 benzoyl peroxide Nutrition 0.000 description 2
239000007795 chemical reaction product Substances 0.000 description 2
230000006866 deterioration Effects 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
MBGQQKKTDDNCSG-UHFFFAOYSA-N ethenyl-diethoxy-methylsilane Chemical compound CCO[Si](C)(C=C)OCC MBGQQKKTDDNCSG-UHFFFAOYSA-N 0.000 description 2
229920000578 graft copolymer Polymers 0.000 description 2
239000000463 material Substances 0.000 description 2
229940100630 metacresol Drugs 0.000 description 2
LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 2
LQERIDTXQFOHKA-UHFFFAOYSA-N nonadecane Chemical compound CCCCCCCCCCCCCCCCCCC LQERIDTXQFOHKA-UHFFFAOYSA-N 0.000 description 2
229940090668 parachlorophenol Drugs 0.000 description 2
239000000047 product Substances 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
125000005396 acrylic acid ester group Chemical group 0.000 description 1
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
125000002947 alkylene group Chemical group 0.000 description 1
125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000002612 dispersion medium Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
RSIHJDGMBDPTIM-UHFFFAOYSA-N ethoxy(trimethyl)silane Chemical compound CCO[Si](C)(C)C RSIHJDGMBDPTIM-UHFFFAOYSA-N 0.000 description 1
229960003750 ethyl chloride Drugs 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
238000000605 extraction Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
239000007788 liquid Substances 0.000 description 1
125000005397 methacrylic acid ester group Chemical group 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
150000001282 organosilanes Chemical class 0.000 description 1
150000002978 peroxides Chemical class 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
229920001707 polybutylene terephthalate Polymers 0.000 description 1
230000001737 promoting effect Effects 0.000 description 1
239000002994 raw material Substances 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
238000010008 shearing Methods 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
239000000126 substance Substances 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
125000003396 thiol group Chemical group [H]S* 0.000 description 1

Landscapes

Polyesters Or Polycarbonates (AREA)

JP24805483A 1983-12-29 1983-12-29 ポリエステルの重合方法 Granted JPS60141714A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP24805483A JPS60141714A (ja)	1983-12-29	1983-12-29	ポリエステルの重合方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP24805483A JPS60141714A (ja)	1983-12-29	1983-12-29	ポリエステルの重合方法

Publications (2)

Publication Number	Publication Date
JPS60141714A JPS60141714A (ja)	1985-07-26
JPH0449570B2 true JPH0449570B2 (fr)	1992-08-11

Family

ID=17172511

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP24805483A Granted JPS60141714A (ja)	1983-12-29	1983-12-29	ポリエステルの重合方法

Country Status (1)

Country	Link
JP (1)	JPS60141714A (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6239621A (ja) *	1985-08-14	1987-02-20	Mitsubishi Rayon Co Ltd	ポリエステルの重合方法
KR100476467B1 (ko) *	2001-07-24	2005-03-18	주식회사 코오롱	알칼리 이용성 폴리에스테르의 제조방법

1983
- 1983-12-29 JP JP24805483A patent/JPS60141714A/ja active Granted

Also Published As

Publication number	Publication date
JPS60141714A (ja)	1985-07-26

Publication	Publication Date	Title
US4313870A (en)	1982-02-02	Process for producing polycondensates
US4687811A (en)	1987-08-18	Polymerization process for polyester
KR100845379B1 (ko)	2008-07-09	1,4-사이클로헥산디메타놀 및 이소프탈산을 기초로 하는폴리에스테르의 제조 방법
JPH0553815B2 (fr)	1993-08-11
US4328332A (en)	1982-05-04	Process for producing fluorescent resin for ink jet printers
JP2020514423A5 (fr)	2020-08-06
JPS6360775B2 (fr)	1988-11-25
JPH0449570B2 (fr)	1992-08-11
TWI235754B (en)	2005-07-11	Composition and process for preparing a high molecular weight polyester
JPH0449851B2 (fr)	1992-08-12
JPH11116681A (ja)	1999-04-27	ポリメチルシルセスキオキサン系微粒子及びこれを親水性媒体中に分散させた分散体
JPH0449852B2 (fr)	1992-08-12
JP2854670B2 (ja)	1999-02-03	球状複合微粒子の製造方法及び球状複合微粒子並びにその分散体
JP2701833B2 (ja)	1998-01-21	ウレタン化ポリシロキサンの製造方法
JP2942298B2 (ja)	1999-08-30	球状複合微粒子の製造方法及び球状複合微粒子並びにその分散体
JPS64484B2 (fr)	1989-01-06
JP2002513429A (ja)	2002-05-08	低濃度のジエチレングリコールを含有するポリエステルの製造方法
JPS6341528A (ja)	1988-02-22	ポリエステルの重合方法
JPS60141719A (ja)	1985-07-26	ポリエステルの重合法
JPS60141716A (ja)	1985-07-26	ポリエステルの縮合法
JPH02120320A (ja)	1990-05-08	ポリエステルの製造方法
EP0366479A2 (fr)	1990-05-02	Procédé de préparation de polyester
JPS60141717A (ja)	1985-07-26	ポリエステルの縮合方法
JPS5827717A (ja)	1983-02-18	ポリエステルの製造方法
JPH0511126B2 (fr)	1993-02-12