JPH02293713A - Method for sealing thin-film el panel with protective liquid - Google Patents

Method for sealing thin-film el panel with protective liquid

Info

Publication number
JPH02293713A
JPH02293713A JP1114849A JP11484989A JPH02293713A JP H02293713 A JPH02293713 A JP H02293713A JP 1114849 A JP1114849 A JP 1114849A JP 11484989 A JP11484989 A JP 11484989A JP H02293713 A JPH02293713 A JP H02293713A
Authority
JP
Japan
Prior art keywords
adhesive agent
panel
glass
glass plate
film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1114849A
Other languages
Japanese (ja)
Other versions
JPH07105271B2 (en
Inventor
Toshiaki Ishii
利昭 石井
Akio Inohara
猪原 章夫
Hiroshi Kishishita
岸下 博
Hisashi Kamiide
上出 久
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sharp Corp
Original Assignee
Sharp Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sharp Corp filed Critical Sharp Corp
Priority to JP1114849A priority Critical patent/JPH07105271B2/en
Publication of JPH02293713A publication Critical patent/JPH02293713A/en
Publication of JPH07105271B2 publication Critical patent/JPH07105271B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Abstract

PURPOSE:To provide a sure sealing against the permeation of moisture and to prevent the deterioration in the element characteristics of the thin-film EL panel by sealing the infiltrating liquid injecting hole provided on a rear glass plate with a glass cap by using an adhesive agent having a small coefft. of moisture permeation and a quick setting adhesive agent. CONSTITUTION:The infiltrating liquid is injected into a gap 4 from the infiltrating liquid injecting hole 5 provided on the rear glass surface 3 of the thin-film EL panel formed by holding the EL element 7 in the gap 4 enclosed with a transparent electrode 2 on a glass substrate 1 and the rear glass plate 3. A spot facing hole 6 is formed on the outside surface of the injecting hole 5. The injected liquid is sealed in the spot facing hole 6 by covering the outside end part of the residual piece 8'' of an injecting pipe 8 by the adhesive agent 9 consisting of an epoxy resin or photo-curing resin, etc. The glass cap 11 is thereafter fixed by using the adhesive agent 12 for tentative adhering and the adhesive agent 10 for regular adhering of different kinds. The adhesive agent 1 for tentative adhering is the resin adhesive agent having a quick setting property and the glass cap 22 is fixed in an early period before the resin adhesive agent having the small coefft. of moisture permeation sets. The sure sealing operation is thus possible.

Description

【発明の詳細な説明】 く産業上の利用分野〉 本発明は交流電界型の]liEL素子を使用した薄膜E
Lパネルの保護液封止方法に関する。
[Detailed description of the invention] Industrial application field> The present invention is directed to a thin film E using an AC electric field type LiEL element.
This invention relates to a protective liquid sealing method for an L panel.

〈従来の技術〉 従来の交流電界型薄膜ELパネルは、第5図並びに第6
図に示すように構成されている。
<Prior art> Conventional AC electric field type thin film EL panels are as shown in Figures 5 and 6.
It is configured as shown in the figure.

即ち、弟5図に示す薄膜ELパネルは、ガラス基板1上
に、In202又はSI102等からなる多数の平行な
帯状の透明電極2を設け、更に該透明電極2の上に、Y
20.,Ti○2,Af20:nSi*N.,Si02
等の何れかから選んだ第1の誘電体層13をスパッタリ
ング法又は電子ビーム蒸着法等によって形成すると共に
、該fjSiの誘電体層13の上面にZnS:Mn焼結
ペレットを電子ビーム蒸着法により形成せしめたZnS
発光Wi14を掩うように前記第1の誘電体層13と同
材質の第2の誘電体層15を形成する。そして、該12
の誘電体WJ15の」二にA1からなる多数の平行な帯
状の背面電極16を前記透明電極2と交叉する方向に蒸
着形成され、両電極2と16間に交流電源】7を接続し
て駆動するようにしている。そして、」二記薄膜El.
パネルは、スペース7アクタの利点を生かした平面薄型
ディスプレイディバイスとして広く文字、記号、各種画
像等の表示に利用されているが、しかし、この場合には
、第1、@2の誘電体113.15によって発光層14
を積層構成する際に発生した多数のピンホールやマイク
ロクラック等を含み、これらの欠陥部を通じて発光層1
4内に湿気が侵入し易く、これが原因でEL発光損失に
よって発熱や眉間剥離、その他素子特性の劣化等を招米
する欠点があった。
That is, the thin film EL panel shown in FIG.
20. , Ti○2, Af20:nSi*N. ,Si02
A first dielectric layer 13 selected from the above is formed by sputtering or electron beam evaporation, and ZnS:Mn sintered pellets are formed on the upper surface of the fjSi dielectric layer 13 by electron beam evaporation. ZnS formed
A second dielectric layer 15 made of the same material as the first dielectric layer 13 is formed so as to cover the light emission Wi 14. And the 12th
A large number of parallel strip-shaped back electrodes 16 made of A1 are deposited on the dielectric WJ15 in a direction intersecting the transparent electrode 2, and an AC power source 7 is connected between both electrodes 2 and 16 to drive the electrodes. I try to do that. And, “2nd Thin Film El.
The panel is widely used as a flat thin display device that takes advantage of the Space 7 Actor to display characters, symbols, various images, etc. However, in this case, the first and second dielectrics 113. Luminescent layer 14 by 15
The light-emitting layer 1
Moisture easily enters the inside of the device, which causes heat generation, peeling between the eyebrows, and other deterioration of device characteristics due to loss of EL light emission.

そこで、」二記欠陥に対処する手段として第6図に示す
ものがある。
Therefore, there is a method shown in FIG. 6 as a means to deal with the defect described in "2".

即ち、第6図はガラス基板1」二に多数の平行な帯状の
透明電極2を形成すると共1こ、該透明電極2上に第1
の誘電体層13と、ZnS発光層14と、Si3N.膜
並びにA1203膜からなる第2の誘電体層15とが順
次に積層形成され、該誘電体層15上には多数の平行な
帯状の背面電極16を前記透明電極2に対し交叉する方
向に設けている。
That is, in FIG. 6, a large number of parallel band-shaped transparent electrodes 2 are formed on a glass substrate 1''2, and a first layer is formed on the transparent electrodes 2.
dielectric layer 13, ZnS light emitting layer 14, Si3N. The film and a second dielectric layer 15 made of A1203 film are sequentially laminated, and on the dielectric layer 15, a large number of parallel strip-shaped back electrodes 16 are provided in a direction crossing the transparent electrode 2. ing.

そして、前記透明電極2上には、第1の誘電体層13、
発光[14、第2の誘電体i15及び背面電極16を囲
んでスペーサ18を設け、その上に背面ガラス板3aを
接着剤19によって#.着することにより、透明電極2
、スペーサ18、背面ガラス板3aによって空隙4aを
形成し、該空隙4a内に背面ガラス板3aに穿設した1
個乃至複数個の注入孔5からシリコンオイル、グリース
等の流体(浸潤液)を充填したにおける不良品の発生を
少なくすると共に、性能の安定した製品を提供しようと
するものである。
Then, on the transparent electrode 2, a first dielectric layer 13,
Light emission [14] A spacer 18 is provided surrounding the second dielectric material i15 and the back electrode 16, and a back glass plate 3a is attached thereon with an adhesive 19. By attaching the transparent electrode 2
A gap 4a is formed by the spacer 18 and the back glass plate 3a, and a hole 1 bored in the back glass plate 3a is formed in the gap 4a.
The purpose is to reduce the occurrence of defective products when fluid (wetting liquid) such as silicone oil or grease is filled through one or more injection holes 5, and to provide products with stable performance.

〈課題を解決するための手段〉 ガラス基板上の透明電極と背面ガラス板とで囲まれた空
隙内へ浸潤液を導くようにした注入孔部において、背面
ガラス板と、該背面ガラス板上におかれるガラスキャッ
プとのなす間隙に、注入孔を基点にしで透湿係数の小さ
い接着剤と速硬性のvA着剤とを配置して前記ガラスキ
ャップを接着するようにしでなる。
<Means for Solving the Problems> In an injection hole portion that guides the infiltrating liquid into a gap surrounded by a transparent electrode on a glass substrate and a back glass plate, An adhesive with a small moisture permeability coefficient and a fast-curing vA adhesive are placed in the gap between the glass cap and the glass cap, starting from the injection hole, to adhere the glass cap.

く作用〉 背面ガラス板上lこ設けた浸潤液注入孔を透湿係数の小
さい接着剤と速硬性の接着剤とによりガラスキャップを
接着するようにしたので、先ず速硬性の接着剤によりガ
ラスキャップを速やかに固定し、その後透湿係数の小さ
い接着剤が硬化して湿気の侵入を阻むように作用する。
Effect〉 The glass cap is attached to the infiltrating liquid injection hole provided on the rear glass plate using an adhesive with a small moisture permeability coefficient and a fast-curing adhesive. After that, the adhesive with a low moisture permeability coefficient hardens and acts to prevent moisture from entering.

〈実施例〉 以下、本発明について図面一二示す実施例により詳細に
説明すると、f51図に示すようにガラス基後、該注入
孔5の外側に紫外線硬化at脂又はエボキシ樹脂等の樹
脂接着剤9を介して平板ガラスキャップ11を貼着する
ことにより注入孔を封11−シ、注入流体がピンホール
やマイクロクラックに起因する問題点の解決を図ってい
る。
<Example> Hereinafter, the present invention will be described in detail with reference to an example shown in FIG. By pasting a flat glass cap 11 through the hole 9, the injection hole is sealed 11--to solve problems caused by pinholes and micro-cracks in the injection fluid.

〈発明が解決しようとする課題〉 しかし、平板ガラスキャップで注入孔を封入する場合、
紫外線硬化樹脂製の接着剤9を使用すると、作業性は良
いが透湿係数がエポキシ0{脂に比べて大きいために水
分がWiv.EL、層内−\侵入し易く、信頼性が低下
する。
<Problem to be solved by the invention> However, when enclosing the injection hole with a flat glass cap,
When adhesive 9 made of ultraviolet curing resin is used, workability is good, but the moisture permeability coefficient is 0 (Wiv. EL, easy to penetrate into layers, reducing reliability.

又、上記接着剤9をエボキシ樹脂とした場合には、透湿
係数が小さく信頼性は高いが硬化反応時に急激に粘性が
低下し、流動性を増すのでELパネルの作業治艮が僅か
でも傾斜していると平板ガラスキャップがずれて位置不
良を生しるので、こうしたキャップの位置不良をなくす
には前記作業治具の水平度の管理が必要となり経費高と
なるなどの欠点があった,, 本考案は拘わる上記欠点の解決を図り、作業時板1上に
多数の平行な帯状の透明電極2を設けると共に、該透明
電極2J.には該電極領域より小面積のEL素子7を設
置する。但し、ここでEI一索子7は、従来例における
ように発光層14が第1、第2の誘電体Wi13,15
によって包囲されると共に第2の誘電体層15上に透明
電極2と交叉する方向に多数の平行な背面電極16を設
けて構成したものを包括的に示すものとする。そして、
該透明電極2及び〃ラス基板1(a子状であるから両方
に接する)上には、該EL素子7を充分掩うに足りる大
トさで深さ約1[+o/+olの空隙4をサンドエッチ
ング等により形成したソーグ〃ラス又は硼硅酸〃ラスな
どよりなる背面ガラス板3を光硬化性樹脂又はエボキシ
樹脂等により接着される。該背面ガラス板3上には直径
3−10[m/ml、深さ約1 [m/m]の注入孔5
が穿設されており、該注入孔5の外面には適当な′Rさ
の座削孔6を形成し、該注入孔5に浸潤液注入用の金属
製パイプ8の先端を挿入固着する。
In addition, when the adhesive 9 is made of epoxy resin, the moisture permeability coefficient is small and the reliability is high, but the viscosity decreases rapidly during the curing reaction and the fluidity increases, so that the working conditions of the EL panel may be tilted even slightly. If this is done, the flat glass cap will shift and cause poor positioning, so in order to eliminate such bad positioning of the cap, it is necessary to control the levelness of the work jig, which has the disadvantage of increasing costs. The present invention aims to solve the above-mentioned drawbacks, and provides a large number of parallel band-shaped transparent electrodes 2 on the plate 1 during operation, and the transparent electrodes 2J. An EL element 7 having a smaller area than the electrode area is installed. However, in the EI single element 7, the light emitting layer 14 is made of the first and second dielectric materials Wi13, 15 as in the conventional example.
This comprehensively shows a configuration in which a large number of parallel back electrodes 16 are provided on the second dielectric layer 15 in a direction intersecting with the transparent electrode 2 and surrounded by the transparent electrode 2 . and,
On the transparent electrode 2 and the lath substrate 1 (which is in contact with both because it is in the shape of an a-diaphragm), a gap 4 of approximately 1[+o/+ol] in depth is sandwiched with a thickness sufficient to cover the EL element 7. A back glass plate 3 made of sorg glass or borosilicate glass formed by etching or the like is bonded with a photocurable resin or epoxy resin. On the back glass plate 3, there is an injection hole 5 with a diameter of 3-10 [m/ml] and a depth of about 1 [m/m].
A seat hole 6 of an appropriate radius is formed on the outer surface of the injection hole 5, and the tip of a metal pipe 8 for injecting the infiltrating liquid is inserted and fixed into the injection hole 5.

次に、該注入用パイプ8の他端は最初に吸気装置(図示
せず)と接続されており、吸気装置を動作することによ
り背面ガラス板3の空隙4内にある空気を−・旦吸気し
て排除することにより内部を真空状態になし、次いで該
注入パイプの吸気装置部をシリコンオイル槽内に切換接
続して常圧状態にすることにより槽内のシリコンオイル
は空隙4内が外部に対し陰圧となっているがら空隙4内
に吸入される。
Next, the other end of the injection pipe 8 is first connected to an intake device (not shown), and by operating the intake device, the air present in the gap 4 of the rear glass plate 3 is sucked. Then, the suction device of the injection pipe is connected to the silicone oil tank to create a normal pressure state, so that the silicone oil in the tank is removed from the gap 4 to the outside. On the other hand, it is sucked into the cavity 4 even though the pressure is negative.

こうして、該空隙4内にシリコンオイルを注入口終えた
時、直ちに第2図に示すよう1こ注入パイブ8の背面ガ
ラス板3と接続する部分、即ち座削孔6内において該パ
イプ8を圧搾して狭搾部8゛を形成し、次にバイプ8を
この部分から切断することにより仮封止する。この時、
パイプの残片8”の外端が次の作業との関係で背面ガラ
ス板3の外面より十分低いことが重要で、座削孔6内に
おいて該残片8゛の外端部をエボキシ系樹脂又は光硬化
性樹脂等の接着剤9により掩って封止し、この時の硬化
性樹脂接着剤9の仕上がり状態が、背面ガラス板3の表
面より突出しないことである。
In this way, when the silicone oil is injected into the gap 4, the pipe 8 is immediately squeezed in the part connected to the back glass plate 3 of the injection pipe 8, that is, in the counterbore hole 6, as shown in FIG. A narrowed portion 8' is formed, and then the pipe 8 is cut from this portion for temporary sealing. At this time,
It is important that the outer end of the remaining piece 8" of the pipe is sufficiently lower than the outer surface of the rear glass plate 3 in relation to the next work, and the outer end of the remaining pipe 8" is coated with epoxy resin or light It is sealed by covering with an adhesive 9 such as a curable resin, and the finished state of the curable resin adhesive 9 at this time should not protrude from the surface of the back glass plate 3.

侵入するのを防止するのに役立てることができる。It can help prevent intrusions.

く発明の効果〉 本発明は、上述のように枯成されるので例え透湿係数が
大きくても、速硬性のある樹脂接着剤を使用して仮止め
しているので透湿係数の小さい樹脂接着剤が硬化するま
での間の早い時期にガラスキャップが固定される。従っ
て、ガラスキャップが位置ずれすることなく確実に所定
位置に貼着される。
Effects of the Invention As described above, even if the moisture permeability coefficient is large due to drying, the present invention uses a fast-curing resin adhesive to temporarily fix the resin, so even if the moisture permeability coefficient is high, the resin adhesive with a small moisture permeability coefficient The glass cap is fixed early until the adhesive hardens. Therefore, the glass cap can be reliably attached to a predetermined position without being displaced.

又、こうした確実な封止作業が可能となることにより製
作上の不良部品が少なく、歩留まり良く、しかも確実な
封止ができるので長期に亘る品質の安定をも保たせるこ
とができるなど特有の効果を有する。
In addition, by being able to perform such reliable sealing work, there are fewer defective parts during manufacturing, and the yield is high, and since reliable sealing can be performed, quality stability can be maintained over a long period of time. has.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図乃至第4図は、本発明の実施例を示し、第1図、
第2図及び第3図は、それぞれ封止作業の一連の流れを
示す要部縦断側面図、第4図は、完了状態の要部拡大縦
断面図、第5図及び第6図は、従来例を示し、 次に、背面ガラス板3の座削孔6上には、円形又は四角
その他多角形等任意形状の平板ガラスキャップ11(そ
の他、プラスチック、セラミック、金属、ゴムなど何れ
でも良いが、本例では背面ガラス板との接着性能を考慮
してガラスを使用)を被せる。この場合、背面ガラス板
3かガラスキャップ11の何れかの面に、予めエボキシ
系樹脂接着剤10と、瞬間接着剤あるいは熱可塑性樹脂
接着剤又は紫外線硬化樹脂接着剤等の何れかから選択し
た仮止用接着剤12とを同時に塗布してから添設する。 尚、その他の接着手順としては、最初にガラスキャップ
11を仮止用接着剤12によって仮設した後、浸透性の
良いエボキシ系樹脂接着剤10を毛細管現象によって侵
入させることもできる。 その他、上記のように種類の異なる仮止用の接着剤12
と本付用の接着剤10を使用しているので両接着剤が最
初に混合するのを防ぐためにガラスキャップ11の背面
ガラス板3と相対する面の周辺エツヂを斜面11゛とす
ることにより、樹脂の表面張力により仮土用の接着剤1
2が本イ」用の接着剤10内へfjs S図は、薄膜E
Lパネルの拡大縦断側面図、第6図は、同上他の薄膜E
Lパネルの拡大縦断側面図である。 1・・・ガラス基板 3・・・背面ガラス板 5・・・注入孔 7・・・EL素了 8゛・・・狭搾部 9・・・接着剤 11・・・ガラスキャッ7 2・・・透明電極 4 ・空隙 6・・・座制孔 8・・・注入パイプ 8″・・・残片 10.12・・・接着剤
1 to 4 show embodiments of the present invention, and FIG.
2 and 3 are longitudinal sectional side views of the main parts showing a series of sealing operations, respectively. FIG. 4 is an enlarged longitudinal sectional view of the main parts in a completed state. FIGS. 5 and 6 are conventional An example will be shown.Next, on the seat hole 6 of the back glass plate 3, a flat glass cap 11 of any shape such as circular, square, or polygon (other shapes such as plastic, ceramic, metal, rubber, etc. may be used). In this example, glass is used in consideration of the adhesion performance with the rear glass plate). In this case, a temporary adhesive selected from epoxy resin adhesive 10, instant adhesive, thermoplastic resin adhesive, ultraviolet curing resin adhesive, etc. is applied to either the back glass plate 3 or the glass cap 11 in advance. The fixing adhesive 12 is applied at the same time and attached. As another bonding procedure, the glass cap 11 may be temporarily attached using the temporary fixing adhesive 12, and then the highly permeable epoxy resin adhesive 10 may be penetrated by capillary action. In addition, as mentioned above, different types of temporary adhesives 12
Since the adhesive 10 for attaching the book is used, in order to prevent both adhesives from mixing initially, the peripheral edge of the surface of the glass cap 11 facing the rear glass plate 3 is made to have an inclined surface 11. Adhesive 1 for temporary soil due to the surface tension of resin
Figure 2 shows the thin film E.
An enlarged longitudinal cross-sectional side view of the L panel, FIG.
FIG. 3 is an enlarged longitudinal sectional side view of the L panel. 1...Glass substrate 3...Back glass plate 5...Injection hole 7...EL finish 8゛...Narrowed part 9...Adhesive 11...Glass cap 7 2... - Transparent electrode 4 - Gap 6... Seat hole 8... Injection pipe 8''... Remaining piece 10.12... Adhesive

Claims (1)

【特許請求の範囲】[Claims] 1.ガラス基板上の透明電極と背面ガラス板とで囲まれ
た空隙内にEL素子を保持してなる薄膜ELパネルにお
いて、該背面ガラス板に穿設した浸潤液注入孔部と、該
背面ガラス板上におかれるガラスキャップとのなす間隙
に、前記注入孔を基点にして透湿係数の小さい接着剤と
速硬性の接着剤とを配置して前記ガラスキャップを接着
するようにしてなる薄膜ELパネルの保護液封止方法。
1. In a thin-film EL panel in which an EL element is held in a gap surrounded by a transparent electrode on a glass substrate and a rear glass plate, an infiltrating liquid injection hole formed in the rear glass plate and an infiltrating liquid injection hole on the rear glass plate are provided. A thin film EL panel in which an adhesive with a small moisture permeability coefficient and a fast-curing adhesive are placed in the gap formed between the glass cap and the glass cap, with the injection hole as a starting point, to adhere the glass cap. Protective liquid sealing method.
JP1114849A 1989-05-08 1989-05-08 Method of sealing protective liquid for thin film EL panel Expired - Fee Related JPH07105271B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1114849A JPH07105271B2 (en) 1989-05-08 1989-05-08 Method of sealing protective liquid for thin film EL panel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1114849A JPH07105271B2 (en) 1989-05-08 1989-05-08 Method of sealing protective liquid for thin film EL panel

Publications (2)

Publication Number Publication Date
JPH02293713A true JPH02293713A (en) 1990-12-04
JPH07105271B2 JPH07105271B2 (en) 1995-11-13

Family

ID=14648249

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1114849A Expired - Fee Related JPH07105271B2 (en) 1989-05-08 1989-05-08 Method of sealing protective liquid for thin film EL panel

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015057658A (en) * 2000-04-19 2015-03-26 株式会社半導体エネルギー研究所 Light-emitting device
WO2015100201A1 (en) * 2013-12-24 2015-07-02 Amerlux Llc Systems and methods for retrofitting existing lighting systems
JP2015132835A (en) * 2000-07-27 2015-07-23 株式会社半導体エネルギー研究所 display device
EP3355371A4 (en) * 2015-09-24 2019-07-24 Feng Li Liquid-filled led lamp

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Publication number Priority date Publication date Assignee Title
JPS6267498U (en) * 1985-10-17 1987-04-27
JPS63174195U (en) * 1988-04-27 1988-11-11

Patent Citations (2)

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JPS6267498U (en) * 1985-10-17 1987-04-27
JPS63174195U (en) * 1988-04-27 1988-11-11

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015057658A (en) * 2000-04-19 2015-03-26 株式会社半導体エネルギー研究所 Light-emitting device
US9443461B2 (en) 2000-04-19 2016-09-13 Semiconductor Energy Laboratory Co., Ltd. Electronic device and method of driving the same
JP2017117795A (en) * 2000-04-19 2017-06-29 株式会社半導体エネルギー研究所 Light emitting device
JP2015132835A (en) * 2000-07-27 2015-07-23 株式会社半導体エネルギー研究所 display device
US9489884B2 (en) 2000-07-27 2016-11-08 Semiconductor Energy Laboratory Co., Ltd. Method of driving display device
WO2015100201A1 (en) * 2013-12-24 2015-07-02 Amerlux Llc Systems and methods for retrofitting existing lighting systems
US9797585B2 (en) 2013-12-24 2017-10-24 Amerlux Llc Systems and methods for retrofitting existing lighting systems
EP3355371A4 (en) * 2015-09-24 2019-07-24 Feng Li Liquid-filled led lamp

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