JP7508443B2 - 環境に優しいポリウレタンスプレーフォーム系 - Google Patents
環境に優しいポリウレタンスプレーフォーム系 Download PDFInfo
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- JP7508443B2 JP7508443B2 JP2021508000A JP2021508000A JP7508443B2 JP 7508443 B2 JP7508443 B2 JP 7508443B2 JP 2021508000 A JP2021508000 A JP 2021508000A JP 2021508000 A JP2021508000 A JP 2021508000A JP 7508443 B2 JP7508443 B2 JP 7508443B2
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- isocyanate
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- 239000004814 polyurethane Substances 0.000 title description 19
- 239000011493 spray foam Substances 0.000 title description 7
- 150000003077 polyols Chemical class 0.000 claims description 72
- 239000012948 isocyanate Substances 0.000 claims description 70
- 229920005862 polyol Polymers 0.000 claims description 70
- 150000002513 isocyanates Chemical class 0.000 claims description 69
- 239000000203 mixture Substances 0.000 claims description 58
- 239000004604 Blowing Agent Substances 0.000 claims description 53
- 239000003054 catalyst Substances 0.000 claims description 50
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 42
- 239000000194 fatty acid Substances 0.000 claims description 42
- 229930195729 fatty acid Natural products 0.000 claims description 42
- -1 aliphatic halogenated hydrocarbon Chemical group 0.000 claims description 41
- 150000004665 fatty acids Chemical class 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 38
- 150000001875 compounds Chemical class 0.000 claims description 35
- 229920005906 polyester polyol Polymers 0.000 claims description 31
- 229920005830 Polyurethane Foam Polymers 0.000 claims description 28
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- 239000007858 starting material Substances 0.000 claims description 26
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- 229920000570 polyether Polymers 0.000 claims description 20
- 239000003063 flame retardant Substances 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 18
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 16
- 239000011541 reaction mixture Substances 0.000 claims description 16
- 125000004432 carbon atom Chemical group C* 0.000 claims description 14
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 12
- 239000002666 chemical blowing agent Substances 0.000 claims description 12
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
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- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims description 8
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- 239000004094 surface-active agent Substances 0.000 claims description 6
- DQWPFSLDHJDLRL-UHFFFAOYSA-N triethyl phosphate Chemical compound CCOP(=O)(OCC)OCC DQWPFSLDHJDLRL-UHFFFAOYSA-N 0.000 claims description 6
- GTRSAMFYSUBAGN-UHFFFAOYSA-N tris(2-chloropropyl) phosphate Chemical compound CC(Cl)COP(=O)(OCC(C)Cl)OCC(C)Cl GTRSAMFYSUBAGN-UHFFFAOYSA-N 0.000 claims description 6
- XMNDMAQKWSQVOV-UHFFFAOYSA-N (2-methylphenyl) diphenyl phosphate Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C=CC=CC=1)OC1=CC=CC=C1 XMNDMAQKWSQVOV-UHFFFAOYSA-N 0.000 claims description 5
- AATNZNJRDOVKDD-UHFFFAOYSA-N 1-[ethoxy(ethyl)phosphoryl]oxyethane Chemical compound CCOP(=O)(CC)OCC AATNZNJRDOVKDD-UHFFFAOYSA-N 0.000 claims description 5
- YWDFOLFVOVCBIU-UHFFFAOYSA-N 1-dimethoxyphosphorylpropane Chemical compound CCCP(=O)(OC)OC YWDFOLFVOVCBIU-UHFFFAOYSA-N 0.000 claims description 5
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- 125000000524 functional group Chemical group 0.000 claims description 4
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- 125000001153 fluoro group Chemical group F* 0.000 claims 1
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- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 36
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 35
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 description 24
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 18
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 16
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 15
- 235000011187 glycerol Nutrition 0.000 description 13
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 12
- 150000001412 amines Chemical class 0.000 description 12
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 12
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 12
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 11
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- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 11
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- 239000000654 additive Substances 0.000 description 10
- 239000003225 biodiesel Substances 0.000 description 10
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 10
- 150000003839 salts Chemical class 0.000 description 10
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 9
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 9
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 description 9
- 239000005642 Oleic acid Substances 0.000 description 9
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 9
- 239000002253 acid Substances 0.000 description 9
- 229910052783 alkali metal Inorganic materials 0.000 description 9
- 229960002887 deanol Drugs 0.000 description 9
- 229930195733 hydrocarbon Natural products 0.000 description 9
- 150000002430 hydrocarbons Chemical class 0.000 description 9
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 9
- 239000003921 oil Substances 0.000 description 9
- 235000019198 oils Nutrition 0.000 description 9
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 description 8
- 239000004971 Cross linker Substances 0.000 description 8
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 8
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 8
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 8
- 239000012972 dimethylethanolamine Substances 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 239000004970 Chain extender Substances 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
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- CDOOAUSHHFGWSA-OWOJBTEDSA-N (e)-1,3,3,3-tetrafluoroprop-1-ene Chemical compound F\C=C\C(F)(F)F CDOOAUSHHFGWSA-OWOJBTEDSA-N 0.000 description 6
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 6
- 229930006000 Sucrose Natural products 0.000 description 6
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 6
- 150000001340 alkali metals Chemical class 0.000 description 6
- 125000003118 aryl group Chemical group 0.000 description 6
- 239000004359 castor oil Substances 0.000 description 6
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- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 6
- 125000005442 diisocyanate group Chemical group 0.000 description 6
- 150000002191 fatty alcohols Chemical class 0.000 description 6
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- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 6
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- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 5
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- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 3
- 239000013543 active substance Substances 0.000 description 3
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- 150000001298 alcohols Chemical class 0.000 description 3
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- 150000008044 alkali metal hydroxides Chemical class 0.000 description 3
- 125000002947 alkylene group Chemical group 0.000 description 3
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Description
(b1a1)下記の(b1a11)及び(b1a12)を含む10~80mol%のジカルボン酸組成物:
(b1a11)20~100mol%(ジカルボン酸組成物に基づく)の1種以上の芳香族ジカルボン酸又はその誘導体、
(b1a12)0~80mol%(ジカルボン酸組成物に基づく)の1種以上の脂肪族ジカルボン酸又はその誘導体;
(b1a2)0~30mol%の1種以上の脂肪酸及び/又は脂肪酸誘導体;
(b1a3)2~70mol%の2~18個の炭素原子を有する1種以上の脂肪族又は脂環式ジオール又はそのアルコキシレート;
(b1a4)0~80mol%を超える、平均官能基が少なくとも2つ有する少なくとも1種のスターター分子のアルコキシル化生成物;
いずれの場合も、成分(b1a1)~(b1a4)の合計量(成分(b1a1)~(b1a4)は合計で100mol%)に基づいている。
4-ヒドロキシ-2,2,6,6-テトラメチル-1-ピペリジンエタノールを有するコハク酸ジエチルポリマーを含む。
パラメータは次のように決定された。
ヒドロキシル価は、DIN53240(1971-12)に従って決定された。
エンベロープ密度は、次の3つの方法で決定された。
1)ビーカー法によるエンベロープ密度
このために、既知量の出発化合物をビーカーに入れ、その中において手動で混合した。硬化後、ビーカーの端から突き出ているフォームを切り取った。ビーカー法によるエンベロープ密度は、ビーカー内のフォームの質量とその体積から計算された割算の商です。ビーカー法によるエンベロープ密度は、European standard EN 14315-1のAnnex Eに従って決定された。
コアエンベロープ密度は、反応混合物の複数の層をPEシート上に噴霧することによって決定された。フォームの硬化後のコア密度は、スキンなしで、フォームの中央から試料を切り出すことによって決定された。これらの試料の質量を量り、それらの体積を決定し、次に、これらの値を使用して密度を計算した。コアエンベロープ密度は、European standard EN ISO 845に従って決定された。
総フリーフォーム密度は、コアエンベロープ密度を決定する手順を使用することによって、そしてベースから表面までのすべてのスキンを有する試料の中央からフォーム試料を採取することによって決定された。これらの試料の重さを量り、それらの体積を決定し、次にこれらの値を使用して密度を計算した。総フリーフォーム密度は、European standard EN 14315-2のAnnex Cに従って決定された。
クリーム時間は、混合の開始から混合物の体積膨張の開始までの時間として決定された。 クリーム時間は、European standard EN 14315-1のAnnex Eに従って決定された。
ゲル時間は、混合と反応混合物から糸を引くことができる接合部との間の間隔として決定された。ゲル時間は、European Standard EN 14315-1のAnnex Eに従って決定された。
タックフリー時間は、混合とフォームの上面がもはや粘着性でなくなる接合部との間の間隔として決定された。タックフリー時間は、European standard EN 14315-1のAnnex Eに従って決定された。
フルライズ時間は、泡の膨張の開始と終了の間の間隔として決定された。フルライズ時間は、European standard EN 14315-1のAnnex Eに従って決定された。
発泡体試料の熱伝導率は、European standard EN 12667に従って、10℃の温度でLasercomp FOX314熱流束測定装置を使用して決定された。試料は、反応混合物の複数の層をPEシート上に噴霧することによって生成された。
10%圧縮での圧縮強度は、Instron5550R試験機器を使用してEuropean standard EN 826に従って決定された。
独立気泡の割合は、European standard EN ISO 4590に従ってACCUPYC1330ピクノメーターで決定された。
寸法安定性は、European standard EN 1604に従って決定された。試験片は、反応混合物の複数の層をポリエチレンシート上に噴霧することによって製造された。コアから200mm×200mm×30mmの試験片を切り出した。試験片の正確な長さ、幅、高さは、70℃、相対湿度90%で28時間標本を保管する前後に、それぞれスライドゲージで測定した。寸法安定性は、保管前後の測定値の差によって与えられる。
ポリオール1:スターター分子としてのvic-TDAならびにエチレンオキシド及びプロピレンオキシドから出発するポリエーテルオール(ヒドロキシル価390mgKOH/g)
ポリオール2:スターター分子としてのスクロース及びグリセロールの混合物ならびに酸化プロピレンから出発するポリエーテルオール(ヒドロキシル価450mgKOH/g)
ポリオール3:テレフタル酸、ジエチレングリコール、オレイン酸から出発するポリエステルオール、及び、スターター分子としてのグリセロール及びエチレンオキシドから出発するポリエーテルオール(ヒドロキシル価240mgKOH/g)
ポリオール4:無水フタル酸、ジエチレングリコール、及びモノエチレングリコールをベースにしたポリエステルオール(ヒドロキシル価240mgKOH/g)
ポリオール5:スターター分子としてエチレンジアミン及び酸化プロピレンから出発するポリエーテルオール(ヒドロキシル価470mgKOH/g)
ポリオール6:スターター分子としてトリメチロールプロパン及びエチレンオキシドから出発するポリエーテルオール(ヒドロキシル価250mgKOH/g)
ポリオール7:スターター分子としてのトリメチロールプロパン及びエチレンオキシドの混合物から出発するポリエーテルオール(ヒドロキシル価600mgKOH/g)
ポリオール8:テレフタル酸、無水フタル酸、ジエチレングリコール、オレイン酸、及びグリセロールから出発するポリエステルオール(ヒドロキシル価240mgKOH/g)
触媒1:ジメチルエタノールアミン
触媒2:トリス(ジメチルアミノプロピル)アミン、Evonik製のPolycat(登録商標)34
触媒3:ペンタメチルジエチレントリアミン
触媒4:ジブチルスズジラウレート、Evonik製のKosmos(登録商標)19
触媒5:85%のトリエタノールアミンと15%のジエタノールアミンとの混合物
触媒6:ジエタノールアミン
触媒7:Evonik製のPolycat 203
触媒8:Evonik製のDABCO 2040
界面活性剤1:シリコーン界面活性剤、Evonik製のDabco(登録商標)DC193
界面活性剤2:スターター分子としてノニルフェノール及びホルムアルデヒド及びエチレンオキシド(ヒドロキシル価432mgKOH/g)から出発するポリエーテル
架橋剤:グリセロール(ヒドロキシル価1825mgKOH/g)
難燃剤1:トリス(2-クロロイソプロピル)ホスフェート
難燃剤2:トリエチルホスフェート
発泡剤1:トランス-1-クロロ-3,3,3-トリフルオロプロペン(HCFO-1233zd(E))、HoneywellのSolstice(登録商標)LBA
発泡剤2:93質量%の1,1,1,3,3-ペンタフルオロブタン(HFC-365mfc)、Solvay製のSolkane(登録商標)365及び7質量%の1,1,1,2,3,3,3-ヘプタフルオロプロペイン(HFC-227ea)、Solvay製のSolkane(登録商標)227
発泡剤3:1,1,1,3,3-ペンタフルオロプロパン(HFC-245fa)、Honeywell製のEnovate(登録商標)3000
イソシアネート1:Lupranat(登録商標)M20S(25℃での粘度が約210mPa・sであり、モノマージフェニルメタンジイソシアネートの含有量が41.8質量%であるポリマーメチレンジフェニルジイソシアネート(PMDI);BASF SE製)
イソシアネート2:Lupranat(登録商標)M50(25℃での粘度が約500mPa・sであり、モノマージフェニルメタンジイソシアネートの含有量が30.6質量%であるポリマーメチレンジフェニルジイソシアネート(PMDI);BASF SE製)
ポリオール成分(B)及びイソシアネート成分(A)は、表1及び2における実施例1~6のように製造された。
貯蔵後、成分を20℃に冷却し、ポリオール成分をイソシアネート成分と激しく混合することにより発泡させた。ここでのポリオール成分の体積に対するイソシアネート成分の体積比は、表3において報告されている体積混合比による方法で選択された。表3は、また、ポリオール成分に対するイソシアネート成分の得られた質量による質量比を述べている。
Claims (16)
- (a)二官能性MDIを40質量%未満で含有するポリメリックMDI、
(b)イソシアネート基に対して反応性を有する少なくとも2個の水素原子を有すると共に、(b1)少なくとも1種のポリエステルポリオール及び(b2)少なくとも1種のポリエーテルポリオールを含む化合物、
(c)任意の難燃剤、
(d)2~5個の炭素原子及び少なくとも1個の水素原子及び少なくとも1個のフッ素原子及び/又は塩素原子から構成される少なくとも1種の脂肪族ハロゲン化炭化水素化合物(d1)が含まれている発泡剤、前記化合物(d1)が少なくとも1つの炭素-炭素二重結合を含んでいる、
(e)任意の触媒、及び
(f)任意の助剤、
を混合して反応混合物を提供すること、前記反応混合物を基材にスプレーすること、そしてその反応混合物を硬化させてポリウレタンフォームを提供することによって、ポリウレタンフォームを製造する方法であって、
ポリイソシアネート(a)と発泡剤(d1)とを含むイソシアネート成分(A)、及びイソシアネート基に対して反応性を有する少なくとも2個の水素原子を有する化合物(b)を含むポリオール成分(B)を製造して、次に、イソシアネート成分(A)とポリオール成分(B)と任意の他の化合物(c)、(e)及び(f)とを混合して前記反応混合物を提供し、ポリオール成分(B)に対するイソシアネート成分(A)の質量比が少なくとも1.2である、前記方法。 - 25℃での前記ポリイソシアネート(a)の粘度が250mPas~1000mPasである、請求項1に記載の方法。
- イソシアネート成分(A)の合計質量に基づく成分(d1)の割合が1~25質量%である、請求項1又は2に記載の方法。
- イソシアネート成分(A)が物理的発泡剤(d2)であって、(d1)以外の物理的発泡剤を更に含む、請求項1~3のいずれかに記載の方法。
- イソシアネート成分(A)が(f1)界面活性物質を含む、請求項1~4のいずれかに記載の方法。
- 25℃でのイソシアネート成分(A)の粘度が50mPas~700mPasである、請求項1~5のいずれかに記載の方法。
- 前記ポリエステルポリオール(b1)が、下記の(b1a1)~(b1a4)のエステル化によって得ることのできる少なくとも1種のポリエステルポリオール(b1a)を含む:
(b1a1)下記の(b1a11)及び(b1a12)を含む10~80mol%のジカルボン酸組成物:
(b1a11)20~100mol%(ジカルボン酸組成物に基づく)の1種以上の芳香族ジカルボン酸又はその誘導体、
(b1a12)0~80mol%(ジカルボン酸組成物に基づく)の1種以上の脂肪族ジカルボン酸又はその誘導体;
(b1a2)0~30mol%の1種以上の脂肪酸及び/又は脂肪酸誘導体;
(b1a3)2~70mol%の2~18個の炭素原子を有する1種以上の脂肪族若しくは脂環式ジオール又はそのアルコキシレート;
(b1a4)0mol%を超え80mol%までの平均官能基を少なくとも2個有する少なくとも1種のスターター分子のアルコキシル化生成物;
いずれの場合も、成分(b1a1)~(b1a4)の合計量に基づいており、成分(b1a1)~(b1a4)は合計で100mol%である、請求項1~6のいずれかに記載の方法。 - ポリエステルポリオール(b1)の数平均モル質量が400~1000g/molであり、ポリエステルポリオール(b1)の官能基が平均で少なくとも2個である、請求項7に記載の方法。
- ポリエーテルポリオール(b2)の数平均モル質量が150~3000g/molであり、ポリエーテルポリオール(b2)の平均官能基が2~6個である、請求項1~8のいずれかに記載の方法。
- ポリエステルポリオール(b1)が、ポリエステルポリオール(b1a)と共に、ポリエステルポリオール(b1b)を含み、そのポリエステルポリオール(b1b)が、成分(b1a4)の非存在下で生成される、請求項7または8に記載の方法。
- 成分(b2)に対する成分(b1)全体の質量比が0.1~7である、請求項1~10のいずれかに記載の方法。
- 使用される前記難燃剤が、トリス(2-クロロプロピル)ホスフェート(TCP)、ジエチルエタンホスホネート(DEEP)、トリエチルホスフェート(TEP)、ジメチルプロピルホスホネート(DMPP)、及びジフェニルクレシルホスフェート(DPC)からなる群から選択される少なくとも1つの化合物を含む、請求項1~11のいずれかに記載の方法。
- 使用される発泡剤が、成分(d1)と共に、少なくとも1種の化学発泡剤(d3)を含み、その化学発泡剤(d3)が、イソシアネート成分(A)の構成要素ではない、請求項1~12のいずれかに記載の方法。
- 25℃でのポリオール成分(B)の粘度が100mPas~700mPasである、請求項1~13のいずれかに記載の方法。
- ポリオール成分(B)に対するイソシアネート成分(A)の質量比が1.2越え及び2.5未満である、請求項1~14のいずれかに記載の方法。
- 請求項1~15のいずれかに記載の方法により得られるポリウレタンフォーム。
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KR102553336B1 (ko) * | 2023-03-17 | 2023-07-06 | 강응선 | 3액형 시스템을 이용한 심재 준불연성능을 가지는 폴리우레탄폼의 시공 방법 |
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MX2021001881A (es) | 2021-04-19 |
EP3837296B1 (de) | 2022-10-12 |
KR20210042962A (ko) | 2021-04-20 |
CN112566955A (zh) | 2021-03-26 |
WO2020035395A1 (de) | 2020-02-20 |
US20210198412A1 (en) | 2021-07-01 |
PT3837296T (pt) | 2022-10-31 |
CA3109540A1 (en) | 2020-02-20 |
ES2935180T3 (es) | 2023-03-02 |
CN112566955B (zh) | 2023-04-14 |
JP2021534299A (ja) | 2021-12-09 |
EP3837296A1 (de) | 2021-06-23 |
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