JP7234211B2 - 油中水型乳化化粧料 - Google Patents
油中水型乳化化粧料 Download PDFInfo
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Description
(A)0.1~20質量%の金属石鹸処理粉末、及び、
(B)0.01~2質量%のカルボキシル基を有する吸水性ポリマーを含有することを特徴とする油中水型乳化化粧料を提供する。
即ち、表面処理剤として好ましく用いられる金属石鹸の例として、ミリスチン酸マグネシウム、ミリスチン酸亜鉛、ステアリン酸マグネシウム、ステアリン酸亜鉛、ステアリン酸アルミニウム、ジステアリン酸アルミニウム、オレイン酸アルミニウム、パルミチン酸アルミニウム、ラウリン酸アルミニウム,ミリスチン酸アルミニウム、ジミリスチン酸アルミニウム、シリコーン金属石鹸(末端カルボキシル基を有するオルガノシロキサン誘導体の2価又は3価の金属塩)等が挙げられる。
市販されている球状有機樹脂粉末としては、球状PMMA粉末粒子(ガンツパールGMX-0810:アイカ工業株式会社製)、マイクロスフェアM-100、M-330:松本油脂製薬株式会社製)、球状ウレタン粒子(Plastic Powder D-400:東色ピグメント株式会社製)等が挙げられる。
本発明の油中水型乳化化粧料における水の配合量は、特に限定されないが、例えば、約30質量%以下、約25質量%以下、あるいは約20質量%で調製することができる。
(1)よれにくさ
(2)凹凸(毛穴等)補正効果
(3)金属石鹸処理粉末と吸水性ポリマーとの会合体形成の有無
(1)及び(2)については、専門パネルによる実使用試験によって以下のように評価した。
A+:非常に優れている
A:優れている
B:若干劣っている
C:劣っている
会合体形成が観察された=「あり」
会合体形成が観察されなかった=「なし」
配合成分 配合量(質量%)
(1)揮発性ジメチルポリシロキサン 30.00
(2)デカメチルシクロペンタシロキサン 10.00
(3)メチルポリシロキサン 3.00
(4)PEG-10ジメチコン 1.00
(5)PEG-9ポリジメチルシロキシエチルジメチコン 2.00
(6)イソステアリン酸 1.00
(7)ビスブチルジメチコンポリグリセリル-3 1.00
(8)(ジメチコン/ポリグリセリン-3)クロスポリマー 1.00
(9)ジステアルジモニウムヘクトライト 1.00
(10)(ビニルジメチコン/メチコンシルセスキオキサン)クロスポリマー
3.00
(11)(ジフェニルジメチコン/ビニルジフェニルジメチコン/シルセスキオキサン)
クロスポリマー 2.00
(12)疎水化シリコーン処理微粒子酸化チタン 5.00
(13)疎水化シリコーン処理顔料級酸化チタン 3.00
(14)疎水化シリコーン処理黄酸化鉄 1.25
(15)疎水化シリコーン処理赤酸化鉄 0.35
(16)疎水化シリコーン処理黒酸化鉄 0.02
(17)架橋型カルボマーNa 0.25
(18)ミリスチン酸マグネシウム処理硫酸バリウム 3.00
(19)イオン交換水 残余
(20)ジプロピレングリコール 5.00
(21)グリセリン 3.00
(22)防腐剤 0.10
配合成分 配合量(質量%)
(1)揮発性ジメチルポリシロキサン 25.00
(2)デカメチルシクロペンタシロキサン 10.00
(3)イソドデカン 3.00
(4)ジフェニルシロキシフェニルトリメチコン 5.00
(5)PEG-10ジメチコン 2.00
(6)ラウリルPEG-9ポリジメチルシロキシエチルジメチコン
1.00
(7)(ジメチコン/ポリグリセリン-3)クロスポリマー 1.00
(8)イソノナン酸イソノニル 3.00
(9)ジステアルジモニウムヘクトライト 1.00
(10)球状シリカ 2.00
(11)シリル化シリカ 1.00
(12)疎水化シリコーン処理酸化亜鉛 5.00
(13)疎水化シリコーン処理顔料級酸化チタン 2.00
(14)疎水化シリコーン処理黄酸化鉄 0.12
(15)疎水化シリコーン処理赤酸化鉄 0.17
(16)疎水化シリコーン処理黒酸化鉄 0.01
(17)架橋型カルボマーNa 0.50
(18)ミリスチン酸マグネシウム処理硫酸バリウム 3.00
(19)イオン交換水 残余
(20)1,3-ブチレングリコール 5.00
(21)グリセリン 3.00
(22)防腐剤 0.10
配合成分 配合量(質量%)
(1)揮発性ジメチルポリシロキサン 5.00
(2)デカメチルシクロペンタシロキサン 25.00
(3)オクチルメトキシシンナメート 7.50
(4)PEG-10ジメチコン 3.00
(5)ジイソステアリン酸ポリグリセリル-2 1.00
(6)香料 0.10
(7)(ジメチコン/ポリグリセリン-3)クロスポリマー 1.00
(8)エチルヘキサン酸セチル 3.00
(9)ジステアルジモニウムヘクトライト 1.00
(10)メタクリル酸メチルクロスポリマー 2.00
(11)疎水化処理酸化亜鉛 3.00
(12)疎水化シリコーン処理微粒子酸化チタン 5.00
(13)疎水化シリコーン処理顔料級酸化チタン 3.00
(14)疎水化シリコーン処理黄酸化鉄 1.25
(15)疎水化シリコーン処理赤酸化鉄 0.35
(16)疎水化シリコーン処理黒酸化鉄 0.02
(17)架橋型カルボマーNa 0.30
(18)ミリスチン酸マグネシウム処理硫酸バリウム 3.00
(19)硫酸バリウム 1.00
(20)イオン交換水 残余
(21)1,3-ブチレングリコール 8.00
(22)防腐剤 0.10
配合成分 配合量(質量%)
(1)揮発性ジメチルポリシロキサン 30.00
(2)デカメチルシクロペンタシロキサン 10.00
(3)メチルポリシロキサン 3.00
(4)PEG-10ジメチコン 3.00
(5)ジイソステアリン酸ポリグリセリル-2 1.00
(6)香料 0.10
(7)(ジメチコン/ポリグリセリン-3)クロスポリマー 1.00
(8)イソノナン酸イソノニル 3.00
(9)ジステアルジモニウムヘクトライト 1.00
(10)疎水性フュームドシリカ 1.00
(11)架橋型カルボマーNa 0.30
(12)ミリスチン酸マグネシウム処理硫酸バリウム 3.00
(13)イオン交換水 残余
(14)1,3-ブチレングリコール 8.00
(15)グリセリン 6.00
(16)ヒアルロン酸 0.30
(17)防腐剤 0.10
(i)油相成分の混合液中に粉末を加え、これをホモミキサーなどにより撹拌混合して粉末分散液(油相)を得た。
(ii)次いで、前記粉末分散液(油相)に対して、予め混合・静置した水相を添加してホモミキサーなどにより攪拌混合し乳化物とし、製品を得た。
下記の表5に示す組成の油中水型乳化製剤(試験例1、2及び3)を常法により調製した。得られた試料から0.35mmのドクターブレードを用いて均一膜を作製し、その状態を観察比較した。
Claims (6)
- (A)0.1~20質量%の金属石鹸処理体質顔料粉末、及び、
(B)0.01~2質量%のカルボキシル基を有する吸水性ポリマーを含有することを特徴とする油中水型乳化化粧料。 - (B)カルボキシル基を有する吸水性ポリマーの吸水能が自重の10倍~1000倍であることを特徴とする請求項1に記載の化粧料。
- (A)金属石鹸処理体質顔料粉末の処理剤が、ミリスチン酸マグネシウム、ミリスチン酸亜鉛、ミリスチン酸アルミニウム、ステアリン酸マグネシウム、ステアリン酸亜鉛、ステアリン酸アルミニウム、又はシリコーン金属石鹸であることを特徴とする請求項1に記載の化粧料。
- (A)金属石鹸処理体質顔料粉末の母核がマイカ、タルク、又は硫酸バリウムである、請求項1に記載の化粧料。
- (B)カルボキシル基を有する吸水性ポリマーが、カルボマーNa又はアクリル酸Naグラフトデンプンである、請求項1に記載の化粧料。
- (B)カルボキシル基を有する吸水性ポリマーの吸水能が自重の10倍~500倍であることを特徴とする請求項2に記載の化粧料。
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