JP6097046B2 - 防錆剤組成物及び防錆剤被覆鋼材 - Google Patents
防錆剤組成物及び防錆剤被覆鋼材 Download PDFInfo
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- JP6097046B2 JP6097046B2 JP2012230899A JP2012230899A JP6097046B2 JP 6097046 B2 JP6097046 B2 JP 6097046B2 JP 2012230899 A JP2012230899 A JP 2012230899A JP 2012230899 A JP2012230899 A JP 2012230899A JP 6097046 B2 JP6097046 B2 JP 6097046B2
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- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000005536 corrosion prevention Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- LDHQCZJRKDOVOX-NSCUHMNNSA-N crotonic acid Chemical compound C\C=C\C(O)=O LDHQCZJRKDOVOX-NSCUHMNNSA-N 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- QSAWQNUELGIYBC-UHFFFAOYSA-N cyclohexane-1,2-dicarboxylic acid Chemical compound OC(=O)C1CCCCC1C(O)=O QSAWQNUELGIYBC-UHFFFAOYSA-N 0.000 description 1
- XBZSBBLNHFMTEB-UHFFFAOYSA-N cyclohexane-1,3-dicarboxylic acid Chemical compound OC(=O)C1CCCC(C(O)=O)C1 XBZSBBLNHFMTEB-UHFFFAOYSA-N 0.000 description 1
- FOTKYAAJKYLFFN-UHFFFAOYSA-N decane-1,10-diol Chemical compound OCCCCCCCCCCO FOTKYAAJKYLFFN-UHFFFAOYSA-N 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 description 1
- 235000019414 erythritol Nutrition 0.000 description 1
- 229940009714 erythritol Drugs 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 239000000594 mannitol Substances 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- KBJFYLLAMSZSOG-UHFFFAOYSA-N n-(3-trimethoxysilylpropyl)aniline Chemical compound CO[Si](OC)(OC)CCCNC1=CC=CC=C1 KBJFYLLAMSZSOG-UHFFFAOYSA-N 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 229960002969 oleic acid Drugs 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- XRVCFZPJAHWYTB-UHFFFAOYSA-N prenderol Chemical compound CCC(CC)(CO)CO XRVCFZPJAHWYTB-UHFFFAOYSA-N 0.000 description 1
- 229950006800 prenderol Drugs 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000004224 protection Effects 0.000 description 1
- 229960003656 ricinoleic acid Drugs 0.000 description 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- AUHHYELHRWCWEZ-UHFFFAOYSA-N tetrachlorophthalic anhydride Chemical compound ClC1=C(Cl)C(Cl)=C2C(=O)OC(=O)C2=C1Cl AUHHYELHRWCWEZ-UHFFFAOYSA-N 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- WXBXVVIUZANZAU-CMDGGOBGSA-N trans-2-decenoic acid Chemical compound CCCCCCC\C=C\C(O)=O WXBXVVIUZANZAU-CMDGGOBGSA-N 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
- DQZNLOXENNXVAD-UHFFFAOYSA-N trimethoxy-[2-(7-oxabicyclo[4.1.0]heptan-4-yl)ethyl]silane Chemical compound C1C(CC[Si](OC)(OC)OC)CCC2OC21 DQZNLOXENNXVAD-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 239000002383 tung oil Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
Landscapes
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Laminated Bodies (AREA)
- Paints Or Removers (AREA)
Description
樹脂B:ハリアクロン8281(商品名、ハリマ化成(株)製、樹脂分50重量%、溶剤ミネラルスピリット)
樹脂C:ハリアクロン8730(商品名、ハリマ化成(株)製、樹脂分50重量%、溶剤ミネラルスピリット)
樹脂D:ハリアクロン8006G−8(商品名、ハリマ化成(株)製、樹脂分50重量%、溶剤ミネラルスピリット)
樹脂E:ハリアクロン8006G(商品名、ハリマ化成(株)製、樹脂分50重量%、溶剤ミネラルスピリット)
樹脂F:ベッコゾールES−4801−50MS(商品名、DIC(株)製、樹脂分50重量%、溶剤ミネラルスピリット)
樹脂G:ベッコゾールDK−550(商品名、DIC(株)製、樹脂分70重量%、溶剤ミネラルスピリット)
1)密着性試験
バーコーター塗布後7日間放置した塗布膜に、カッターにて碁盤目の切り目を入れ、セロテープ(登録商標)にて剥がした時に、100枡中に塗布膜が在る箇所数で以下のように判定した。
基準
○;100〜95/100 △;75〜94/100 ×;75未満/100
下記の条件下の塩水噴霧試験機に24時間入れた時の錆面積で防錆性を試験した。さび面積は、デジタル画像を二値化処理にて算出した。
塩水噴霧試験の条件(JIS−K−2246に準じる)
(i) 機内温度:35±1℃
(ii) 噴霧する液:5%塩化ナトリウム水溶液
(iii) 試験片:傾斜角45°に置く
基準
○;錆面積10%未満 △;錆面積10%以上25%未満 ×;錆面積25%以上
下記の条件下の湿潤箱試験機に168時間入れた時の錆面積で防錆性を試験した。
湿潤箱試験の条件(JIS−K−2246に準じる)
(i) 機内温度:49±1℃
(ii) 相対湿度:95%以上
(iii) 試験片:吊り下げた状態で回転させる
基準
○;錆面積10%未満 △;錆面積10%以上25%未満 ×;錆面積25%以上
下記条件下のUV照射試験48時間後に2)と同じ塩水噴霧試験機に24時間入れた後のさび面積で防錆性を試験した。さび面積は、デジタル画像を二値化処理にて算出した。
UV照射試験の条件
(i) ブラックパネル温度:63±1℃
(ii) 試料面のエネルギー(波長300nm〜400nm):60 mW/cm2
基準
○;錆面積10%未満 △;錆面積10%以上25%未満 ×;錆面積25%以上
塗膜面にPカッターを用いて鋼面に達するクロスカットを付与して試験を行った。試験は4)と同様、下記条件下のUV照射試験48時間後に2)と同じ塩水噴霧試験機に24時間入れた後のさび面積で防錆性を試験した。さび面積は、デジタル画像を二値化処理にて算出した。
UV照射試験の条件
(i) ブラックパネル温度:63±1℃
(ii) 試料面のエネルギー(波長300nm〜400nm):60 mW/cm2
基準
○;錆面積10%未満 △;錆面積10%以上25%未満 ×;錆面積25%以上
無塗装の試験鋼板を、兵庫県尼崎市において、南面30°に傾けて2ヶ月暴露し表面にさびを形成させた後、バーコーターを用いて各種樹脂を塗布、乾燥した。その後、2)の塩水噴霧試験を24時間実施した。
基準
○;錆面積10%未満 △;錆面積10%以上25%未満 ×;錆面積25%以上
Claims (3)
- アルキッド変性アクリル樹脂、反応性モノマー及び有機溶剤を含有する防錆剤組成物であって、前記アルキッド変性アクリル樹脂は、アクリル樹脂を、油変性アルキッド樹脂で変性したもので、アクリル樹脂部(a)とアルキッド樹脂変性部(b)と脂肪酸変性部(c)とから構成され、(a)を50〜90重量%、(b)を5〜25重量%、(c)を5〜25重量%の割合で含有し、前記反応性モノマーが、ビニルトリエトキシシラン、ビニルメトキシシラン、γ−グリシドキシプロピルトリメトキシシラン、γ−グリシドキシプロピルトリエトキシシラン、β−(3,4−エポキシシクロヘキシル)エチルトリメトキシシラン、γ−(2−アミノエチル)アミノプロピルトリメトキシシラン、γ−(2−アミノエチル)アミノプロピルメチルジメトキシシラン、γ−アミノプロピルトリエトキシシラン、ヘキサメチルジシラザン、及びγ−アニリノプロピルトリメトキシシランからなる群から選択される少なくとも1種である、防錆剤組成物。
- 前記アルキッド変性アクリル樹脂の重量平均分子量が5万〜20万である、請求項1に記載の防錆剤組成物。
- 請求項1又は2に記載の防錆剤組成物が鋼材の表面に塗布されてなる、防錆剤被覆鋼材。
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US11414567B2 (en) | 2017-01-25 | 2022-08-16 | Dic Corporation | (Meth)acryloyl group-containing acrylic-modified alkyd resin and undercoat agent for inorganic-material thin film |
KR102301211B1 (ko) * | 2021-01-25 | 2021-09-13 | (주) 페트로산업 | 반경화 우레탄 방수층을 포함하는 이중 복합 방수 시트 및 이를 이용한 방수 시공 방법 |
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CA876154A (en) * | 1966-07-27 | 1971-07-20 | D. Jerabek Robert | Electrodepositable compositions |
JPS5416974B1 (ja) * | 1970-12-28 | 1979-06-26 | ||
JPS5125250B2 (ja) * | 1972-11-10 | 1976-07-29 | ||
JPS51119043A (en) * | 1975-04-11 | 1976-10-19 | Dainippon Ink & Chem Inc | A composition with high solid content for use in surface coating |
JPS51125488A (en) * | 1975-04-18 | 1976-11-01 | Dainippon Ink & Chem Inc | Resin composition |
JPS53102935A (en) * | 1977-02-22 | 1978-09-07 | Honny Chem Ind Co Ltd | Electro-deposition coating composition |
JPS54129084A (en) * | 1978-03-02 | 1979-10-06 | Hitachi Chem Co Ltd | Production of vinyl polymer modified with alkyd resin |
JPS5516071A (en) * | 1978-07-24 | 1980-02-04 | Hitachi Chem Co Ltd | Preparation of alkyd-modified vinyl polymer |
JPS58201861A (ja) * | 1982-05-18 | 1983-11-24 | Mitsui Toatsu Chem Inc | 防錆塗料組成物 |
JPS59187062A (ja) * | 1983-04-06 | 1984-10-24 | Hitachi Chem Co Ltd | 塗料用樹脂組成物 |
JPS6197367A (ja) * | 1984-10-18 | 1986-05-15 | Dainippon Toryo Co Ltd | 溶剤型塗料組成物 |
JPS61261366A (ja) * | 1985-05-14 | 1986-11-19 | Nippon Paint Co Ltd | 塗料組成物 |
JPH0621269B2 (ja) * | 1985-10-30 | 1994-03-23 | 日立化成工業株式会社 | 塗料用樹脂組成物 |
JPH06248235A (ja) * | 1993-02-26 | 1994-09-06 | Hitachi Chem Co Ltd | 水性樹脂組成物及び塗料 |
JP3585001B2 (ja) * | 1995-04-11 | 2004-11-04 | 大日本インキ化学工業株式会社 | 水性塗料用樹脂組成物 |
KR100490829B1 (ko) * | 1999-01-29 | 2005-05-24 | 닛신 오일리오그룹 가부시키가이샤 | 도료 또는 잉크 조성물 |
JP2002294140A (ja) * | 2001-03-29 | 2002-10-09 | Dainippon Ink & Chem Inc | 塗料組成物 |
JP3896825B2 (ja) * | 2001-11-16 | 2007-03-22 | 豊田合成株式会社 | めっき製品 |
JP4451080B2 (ja) * | 2003-06-04 | 2010-04-14 | 本田技研工業株式会社 | 加飾成型品用ベース塗料組成物、加飾成型品用トップクリヤー塗料組成物及び加飾成型品 |
JP2005008684A (ja) * | 2003-06-17 | 2005-01-13 | Dainippon Ink & Chem Inc | 塗料用樹脂組成物 |
JP4635275B2 (ja) * | 2004-06-09 | 2011-02-23 | 本田技研工業株式会社 | クリヤー塗料組成物、複層塗膜の形成方法及び加飾成形品 |
JP2008007716A (ja) * | 2006-06-30 | 2008-01-17 | Toyobo Co Ltd | (メタ)アクリル変性油性アルキッド樹脂、水系アルキッド塗料用樹脂組成物およびそれらの製造方法 |
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