JP5534988B2 - 粒状浴用剤組成物 - Google Patents
粒状浴用剤組成物 Download PDFInfo
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- JP5534988B2 JP5534988B2 JP2010158924A JP2010158924A JP5534988B2 JP 5534988 B2 JP5534988 B2 JP 5534988B2 JP 2010158924 A JP2010158924 A JP 2010158924A JP 2010158924 A JP2010158924 A JP 2010158924A JP 5534988 B2 JP5534988 B2 JP 5534988B2
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- fatty acid
- oil
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- preferable
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- 239000000203 mixture Substances 0.000 title claims description 39
- 239000013040 bath agent Substances 0.000 title claims description 34
- -1 fatty acid ester Chemical class 0.000 claims description 78
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 54
- 239000000194 fatty acid Substances 0.000 claims description 54
- 229930195729 fatty acid Natural products 0.000 claims description 54
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 29
- 239000002736 nonionic surfactant Substances 0.000 claims description 28
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 17
- 229910052751 metal Inorganic materials 0.000 claims description 17
- 239000002184 metal Substances 0.000 claims description 17
- 239000008187 granular material Substances 0.000 claims description 16
- 150000007524 organic acids Chemical class 0.000 claims description 14
- 239000003232 water-soluble binding agent Substances 0.000 claims description 14
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 9
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 6
- 150000005215 alkyl ethers Chemical class 0.000 claims description 6
- 239000000600 sorbitol Substances 0.000 claims description 6
- 229930006000 Sucrose Natural products 0.000 claims description 5
- 239000004359 castor oil Substances 0.000 claims description 5
- 235000019438 castor oil Nutrition 0.000 claims description 5
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 5
- 239000005720 sucrose Substances 0.000 claims description 5
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 86
- 239000001569 carbon dioxide Substances 0.000 description 43
- 229910002092 carbon dioxide Inorganic materials 0.000 description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 36
- 239000003921 oil Substances 0.000 description 31
- 235000019198 oils Nutrition 0.000 description 31
- 239000002245 particle Substances 0.000 description 29
- 239000007789 gas Substances 0.000 description 22
- 230000000694 effects Effects 0.000 description 19
- 238000000034 method Methods 0.000 description 15
- 238000003287 bathing Methods 0.000 description 14
- 238000005187 foaming Methods 0.000 description 14
- 230000009102 absorption Effects 0.000 description 12
- 238000010521 absorption reaction Methods 0.000 description 12
- 239000003788 bath preparation Substances 0.000 description 11
- 239000006260 foam Substances 0.000 description 9
- 238000005259 measurement Methods 0.000 description 8
- 238000002156 mixing Methods 0.000 description 8
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- 239000000843 powder Substances 0.000 description 8
- 238000001179 sorption measurement Methods 0.000 description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 7
- 230000035515 penetration Effects 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 230000001737 promoting effect Effects 0.000 description 6
- 235000002639 sodium chloride Nutrition 0.000 description 6
- 238000009826 distribution Methods 0.000 description 5
- 238000005469 granulation Methods 0.000 description 5
- 230000003179 granulation Effects 0.000 description 5
- 230000014759 maintenance of location Effects 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 4
- 239000005715 Fructose Substances 0.000 description 4
- 229930091371 Fructose Natural products 0.000 description 4
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 4
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 4
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 4
- 239000002202 Polyethylene glycol Substances 0.000 description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 4
- 125000004432 carbon atom Chemical group C* 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 229920001223 polyethylene glycol Polymers 0.000 description 4
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 230000017531 blood circulation Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001125 extrusion Methods 0.000 description 3
- 239000001530 fumaric acid Substances 0.000 description 3
- 230000001965 increasing effect Effects 0.000 description 3
- 238000000691 measurement method Methods 0.000 description 3
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 235000019830 sodium polyphosphate Nutrition 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 3
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 3
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 2
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 229920000858 Cyclodextrin Polymers 0.000 description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 2
- 239000004375 Dextrin Substances 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
- 239000005913 Maltodextrin Substances 0.000 description 2
- 229920002774 Maltodextrin Polymers 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- MMKRHZKQPFCLLS-UHFFFAOYSA-N ethyl myristate Chemical compound CCCCCCCCCCCCCC(=O)OCC MMKRHZKQPFCLLS-UHFFFAOYSA-N 0.000 description 2
- MVLVMROFTAUDAG-UHFFFAOYSA-N ethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC MVLVMROFTAUDAG-UHFFFAOYSA-N 0.000 description 2
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- 239000003925 fat Substances 0.000 description 2
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- 125000005313 fatty acid group Chemical group 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
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- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 2
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- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- ZUBZATZOEPUUQF-UHFFFAOYSA-N isononane Chemical compound CCCCCCC(C)C ZUBZATZOEPUUQF-UHFFFAOYSA-N 0.000 description 2
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- 239000000395 magnesium oxide Substances 0.000 description 2
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- 229910052943 magnesium sulfate Inorganic materials 0.000 description 2
- 235000019341 magnesium sulphate Nutrition 0.000 description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 2
- 229940035034 maltodextrin Drugs 0.000 description 2
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 2
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- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
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- 235000019477 peppermint oil Nutrition 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
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- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 239000010666 rose oil Substances 0.000 description 2
- 235000019719 rose oil Nutrition 0.000 description 2
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 2
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- 238000004062 sedimentation Methods 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
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- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
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- 239000007787 solid Substances 0.000 description 2
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- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 2
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- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
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- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
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Description
従って本発明の課題は、入浴後の皮膚に対してしっとり感を著しく持続させ、優れたスキンケア効果を発揮する粒状発泡性浴用剤を提供することにある。
(A)有機酸、分子量が100以上でありClogP値が4〜18である脂肪酸エステル、非イオン界面活性剤及び水溶性バインダーを含む造粒物、並びに
(B)炭酸ジアルカリ金属塩を含有し、且つ、炭酸水素塩を70質量%以下含有する炭酸塩
を含有する粒状浴用剤組成物を提供するものである。
ここで、ClogP値は.A.Leo Comprehensive Medicinal Chemistry,Vol.4 C.Hansch、P.G.Sammens,J.B Taylor and C.A.Ramsden,Eds.,P.295,Pergamon Press,1990に記載の方法で計算した“計算logP(ClogP)”であり、プログラムCLOGP v4.01により計算したClogP値である。
ここで、HLBは、界面活性剤の親水性と疎水性のバランスを表すのに通常使用される値であり、当分野において慣用される川上式等の幾つかの計算式により求めることができる。本発明においては、下記の川上式を採用する。
HLB=7+11.7log(Mw/M0)
Mw:親水基の分子量
M0:疎水基の分子量
流動パラフィン、ワセリン、パラフィン、マイクロクリスタリンワックス、セレシン、スクワラン、スクアレン、ジオクチルシクロヘキサン、ブリスタン等の炭化水素油;
ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘニン酸、オレイン酸、リノール酸、リノレン酸、ラノリン酸、イソステアリン酸等の高級脂肪酸類;
ラウリルアルコール、セチルアルコール、ステアリルアルコール、オレイルアルコール、コレステロール、2−ヘキシルデカノール等の高級アルコール類;
ハッカ油、ジャスミン油、ショウ脳油、ヒノキ油、トウヒ油、リュウ油、テレピン油、ケイ皮油、ベルガモット油、ミカン油、ショウブ油、パイン油、ラベンダー油、ベイ油、クローブ油、ヒバ油、バラ油、ユーカリ油、レモン油、タイム油、ペパーミント油、ローズ油、セージ油、メントール、シネオール、オイゲノール、シトラール、シトロネラール、ボルネオール、リナロール、ゲラーオール、カンファー、チモール、スピラントール、ピネン、リモネン、テルペン系化合物等の精油;
シリコーン油類等が挙げられる。
ブドウ糖、果糖、乳糖、麦芽糖、蔗糖、デキストリン、マルトデキストリン、シクロデキストリン、マルトース、フルクトース、トレハロース等の糖類;
塩化ナトリウム、硫酸ナトリウム、硝酸カリウム、硝酸ナトリウム、硝酸カルシウム、ポリリン酸ナトリウム、塩化アンモニウム、硫酸鉄、燐酸ナトリウム、チオ硫酸ナトリウム、硼酸、メタ珪酸、無水珪酸、珪酸カルシウム、硫酸マグネシウム、塩化ナトリウム、塩化カリウム、酸化マグネシウム、ポリ燐酸ナトリウム等の無機塩類;
ソウジュツ、ビャクジュツ、カノコソウ、ケイガイ、コウボク、センキュウ、橙皮、トウキ、ショウキョウ末、ニンジン、ケイヒ、シャクヤク、ハッカ葉、オウゴン、サンシシ、ブクリョウ、ドクカツ、ショウブ、ガイヨウ、マツブサ、ビャクシ、ジュウヤク、リュウノウ、サフラン、オウバクエキス、チンピ、ウイキョウ、チンピ末、カミツレ、メリッサ、ローズマリー、マロニエ、西洋ノコギリ草、アルニカ等の生薬類;
エタノール、イソプロピルアルコール等のアルコール類;
グリセリン、プロピレングリコール、ソルビトール等の多価アルコール;
酸化チタン、酸化亜鉛、タルク、イオウ、鉱砂、湯の花、カゼイン、中性白土、サリチル酸ナトリウム、カルボキシメチルセルロースナトリウム、卵黄末、イリ糠、雲母末、脱脂粉乳、殺菌防腐剤、金属封鎖剤、香料、色素、生薬類その他製剤上必要な成分等が挙げられるが、これらに限定されるものではない。これらは、本発明の効果を阻害しない範囲であれば造粒物(A)中に配合しても良い。
粒径については、以下の2つの方法により測定した。
(1)造粒物(A)及び炭酸ジアルカリ金属塩の粒径は、JIS K 8801の標準篩(目開き2000〜125μm)を用いて5分間振動させた後、篩目のサイズによる重量分率からメジアン径を算出した。
より詳細には、目開き125μm、180μm、250μm、355μm、500μm、710μm、1000μm、1400μm、2000μmの9段の篩と受け皿を用いて、受け皿上に目開きの小さな篩から順に積み重ね、最上部の2000μmの篩の上から100gの粒子を添加し、蓋をしてロータップ型ふるい振とう機(HEIKO製作所製、タッピング156回/分、ローリング:290回/分)に取り付け、5分間振動させたあと、それぞれの篩及び受け皿上に残留した該粒子の質量を測定し、各篩上の該粒子の質量割合(%)を算出した。
有機酸の吸油能測定は以下の方法で行った。吸収量測定器(あさひ総研製S410)に粉末を45g投入し、駆動羽根200rpmで回転させた。ここに油性成分及び非イオン界面活性剤を溶解した50℃混合液(花王(株)製エキセパールIPP 50質量%、花王(株)製エキセパールO−DM 15質量%、花王(株)製ルナックBA 5質量%、花王(株)製エマルゲン306P 10質量%、日光ケミカルズ(株)製ニッコールGO―440V 20質量%)を、液供給速度2mL/minで滴下し、最大トルクとなる点を見極めた。この最大トルクとなる点の70%のトルクとなる点での液添加量を粉末投入量で除算し、吸油能とした。
炭酸ガス濃度の測定には、ATR−IR法を用いた。炭酸ガスのIRスペクトルは2350cm-1付近に強い吸収を示すことが知られており、この吸収は振動モードとしては、1つであるが、気体の場合、回転の遷移が重畳するため、分解能の低い設定で測定すると見かけ上、2本の吸収に***して観測されるが、炭酸ガスが液体に溶解した場合、回転が制限されるため、1本の吸収帯として観測され、この違いから気体と液体に溶解した炭酸ガスが識別される。
測定条件装置:パーキンエルマー SpectrumOne/ユニバーサルATRユニット
分解能:16cm-1
スキャン回数:16回(約25秒)
大気補正機能:OFF
測定順序:油剤バックグラウンド測定→油相の測定→水のバックグラウンド測定→水相の測定
表1に示す成分(A)に用いる成分を混合後押出造粒機にて造粒し、(B)成分、さらに他の成分を混合して、粒状発泡性浴用剤を製造した。
表1に示す成分(A)、成分(B)及びその他成分を全て混合した後、理研社製油圧プレス(型番:CD−50−135B)により、直径55mm、厚さ15mmの円柱状の打錠物(1錠45g)にした。
表1に示す配合で各成分を混合し、液体状浴用剤を得た。
浴槽に40℃180Lのお湯を入れ、浴用剤組成物を投入し、十分攪拌し、直径5cmの円形の黒色ゴム板を浴水に沈め、肉眼で完全に見えなくなる深度をにごり度(濁度)とし測定した。深度の数値(cm)が小さいほど、より微細な泡が生じていることを示す。
20〜40才の女性合計10名のパネラーにより評価した。浴槽に40℃180Lのお湯を入れ、浴用剤組成物を投入した後、速やかにパネラーを入浴させ、出浴30分後のしっとり感を下記の基準で評価し、10名の平均値を評価点とした。
5:しっとりする。
4:ややしっとりする。
3:どちらとも言えない。
2:あまりしっとりしない。
1:しっとりしない。
20〜40才の女性合計10名のパネラーにより評価した。浴槽に40℃180Lのお湯を入れ、浴用剤組成物を投入した後、速やかにパネラーを入浴させ、入浴直後の温まり感を下記の基準で評価し、10名の平均値を評価点とした。
5:温まる。
4:やや温まる。
3:さら湯と同等。
2:さら湯と比べてやや温まらない。
1:さら湯と比べて温まらない。
Claims (4)
- 次の成分(A)並びに(B):
(A)有機酸、分子量が100以上でありClogP値が4〜18である脂肪酸エステル、非イオン界面活性剤及び水溶性バインダーを含む造粒物、並びに
(B)炭酸ジアルカリ金属塩を含有し、且つ、炭酸水素塩を70質量%以下含有する炭酸塩
を含有する粒状浴用剤組成物。 - 成分(A)中の非イオン界面活性剤の含有量が、成分(B)中の炭酸ジアルカリ金属塩100質量部に対し0.5〜30質量部である請求項1記載の粒状浴用剤組成物。
- 成分(A)中の非イオン界面活性剤が、少なくともHLB10〜20の非イオン界面活性剤を含むものである請求項1又は2記載の粒状浴用剤組成物。
- HLB10〜20の非イオン界面活性剤が、ショ糖脂肪酸エステル、ポリオキシエチレンアルキルエーテル、ポリオキシエチレンアルケニルエーテル、ポリオキシエチレンソルビトール脂肪酸エステル、ポリオキシエチレンソルビタン脂肪酸エステル及びポリオキシエチレン硬化ヒマシ油から選ばれる1種又は2種以上である請求項3記載の粒状浴用剤組成物。
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