JP2019530591A - 低放射コーティング及び低放射コーティングを含む窓戸用機能性建材 - Google Patents
低放射コーティング及び低放射コーティングを含む窓戸用機能性建材 Download PDFInfo
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- JP2019530591A JP2019530591A JP2019512984A JP2019512984A JP2019530591A JP 2019530591 A JP2019530591 A JP 2019530591A JP 2019512984 A JP2019512984 A JP 2019512984A JP 2019512984 A JP2019512984 A JP 2019512984A JP 2019530591 A JP2019530591 A JP 2019530591A
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Classifications
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- E—FIXED CONSTRUCTIONS
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3644—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the metal being silver
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3649—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer made of metals other than silver
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- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
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- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/67—Units comprising two or more parallel glass or like panes permanently secured together characterised by additional arrangements or devices for heat or sound insulation or for controlled passage of light
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/67—Units comprising two or more parallel glass or like panes permanently secured together characterised by additional arrangements or devices for heat or sound insulation or for controlled passage of light
- E06B3/6715—Units comprising two or more parallel glass or like panes permanently secured together characterised by additional arrangements or devices for heat or sound insulation or for controlled passage of light specially adapted for increased thermal insulation or for controlled passage of light
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B9/00—Screening or protective devices for wall or similar openings, with or without operating or securing mechanisms; Closures of similar construction
- E06B9/24—Screens or other constructions affording protection against light, especially against sunshine; Similar screens for privacy or appearance; Slat blinds
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/154—Deposition methods from the vapour phase by sputtering
- C03C2218/155—Deposition methods from the vapour phase by sputtering by reactive sputtering
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
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- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/154—Deposition methods from the vapour phase by sputtering
- C03C2218/156—Deposition methods from the vapour phase by sputtering by magnetron sputtering
-
- E—FIXED CONSTRUCTIONS
- E05—LOCKS; KEYS; WINDOW OR DOOR FITTINGS; SAFES
- E05Y—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES E05D AND E05F, RELATING TO CONSTRUCTION ELEMENTS, ELECTRIC CONTROL, POWER SUPPLY, POWER SIGNAL OR TRANSMISSION, USER INTERFACES, MOUNTING OR COUPLING, DETAILS, ACCESSORIES, AUXILIARY OPERATIONS NOT OTHERWISE PROVIDED FOR, APPLICATION THEREOF
- E05Y2900/00—Application of doors, windows, wings or fittings thereof
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Abstract
Description
マグネトロンスパッタリング蒸着機(Selcos Cetus−S)を用いて、下記のように、透明ガラス基材にコーティングされた多層構造の低放射コーティングを製造した。
上部誘電体層の上部面に最上部保護層をさらに形成したことを除いては、実施例1と同じ条件及び方法で透明ガラス基材にコーティングされた低放射コーティングを製造しており、具体的には、前記上部誘電体層の上部面にアルゴン100%雰囲気下でジルコニウムを蒸着して、4〜5nm厚さのジルコニウム層を形成した後、前記金属層の表面に後酸化工程を行い、ジルコニウム層の表面を一部酸化して3〜4nm厚さのジルコニウム酸化物層を形成しており、前記ジルコニウム層の表面を一部酸化してジルコニウム酸化物層を形成すると同時に、シリコーンアルミニウム酸窒化物を蒸着して、10nm厚さのシリコーンアルミニウム酸窒化物層を形成することによって、前記最上部保護層を形成した。
実施例1において、6mm厚さの透明ガラス基板上にSiAl targetを、窒素を含む反応性ガスであるアルゴン/ナイトロジェン(アルゴン:ナイトロジェンの流量比=80:10)雰囲気下で蒸着して、45nm厚さの下部誘電体層を単層で形成し、バリア層を形成していないことを除いては、実施例1と同じ条件及び方法で透明ガラス基材にコーティングされた低放射コーティングを製造した。
実験例1:耐熱性評価
実施例1、2及び比較例1に従って低放射コーティングがコーティングされた透明ガラス基材のヘイズを測定した。
実施例1、2及び比較例1に従って低放射コーティングがコーティングされた透明ガラス基材に対して洗滌器(MANNA,MGR−460)を用いて耐磨耗性試験を実施した。
110 第1の下部誘電体層
120 バリア層
130 第2の下部誘電体層
140、160 低放射保護層
150 低放射層
170 上部誘電体層
Claims (15)
- 順次に、第1の下部誘電体層、バリア層、第2の下部誘電体層、低放射保護層、低放射層、低放射保護層、及び上部誘電体層を含む低放射コーティング。
- 前記低放射コーティングは、前記第1の下部誘電体層、前記バリア層、及び前記第2の下部誘電体層が順次に積層した積層構造を含む、
請求項1に記載の低放射コーティング。 - 前記第1の下部誘電体層及び前記第2の下部誘電体層の各々は、厚さが5μm〜50μmである、
請求項1に記載の低放射コーティング。 - 前記バリア層は、金属酸化物、金属窒化物、金属酸窒化物、複合金属酸化物、複合金属窒化物、複合金属酸窒化物、及びこれらの組み合わせからなる群から選択された1つを含む、
請求項1に記載の低放射コーティング。 - 前記バリア層は、さらにSi、Zr又はTiの金属;SiAl、ZrSi又はTiZrの複合金属;を含む追加金属層をさらに含むか、又はシリコーン酸化物、シリコーンアルミニウム酸化物、ジルコニウム酸化物、ジルコニウムシリコーン酸化物、チタン酸化物、チタンジルコニウム酸化物、シリコーン酸窒化物、シリコーンアルミニウム酸窒化物、ジルコニウム酸窒化物、ジルコニウムシリコーン酸窒化物、チタン酸窒化物、チタンジルコニウム酸窒化物、及びこれらの組み合わせからなる群から選択された1つ以上を含む追加金属化合物層をさらに含む、
請求項1に記載の低放射コーティング。 - 前記バリア層は、厚さが1μm〜30μmである、
請求項1に記載の低放射コーティング。 - 前記低放射保護層は、単一層又は複数の層で含まれており、
前記低放射層の一面又は両面に位置する、
請求項1に記載の低放射コーティング。 - 前記低放射保護層は、可視光線領域の消衰係数が1.5〜3.5である、
請求項1に記載の低放射コーティング。 - 前記低放射保護層は、Ni、Cr、NiとCrの合金、及びこれらの組み合わせからなる群から選択された1つを含む、
請求項1に記載の低放射コーティング。 - 前記第1の下部誘電体層、前記第2の下部誘電体層、及び前記上部誘電体層の各々は、金属酸化物、金属窒化物、及びこれらの組み合わせを含む群から選択された少なくとも1つを含むか、
前記少なくとも1つにビスマス(Bi)、ホウ素(B)、アルミニウム(Al)、珪素(Si)、マグネシウム(Mg)、アンチモン(Sb)、ベリリウム(Be)、及びこれらの組み合わせからなる群から選択された少なくとも1つの元素がドーピングされた物質を含む、
請求項1に記載の低放射コーティング。 - 前記上部誘電体層の厚さは、30μm〜50μmである、
請求項1に記載の低放射コーティング。 - 前記上部誘電体層の上部に最上部保護層をさらに含む、
請求項1に記載の低放射コーティング。 - 前記最上部保護層は、金属層、金属酸化物層、及びシリコーン−アルミニウム系複合金属酸化窒化物層を順次に含む多層構造である、
請求項12に記載の低放射コーティング。 - 透明基板;及び前記透明基板の少なくとも一面にコーティングされた請求項1〜請求項13のうちいずれか一項による低放射コーティング;を含む窓戸用機能性建材。
- 前記透明基板は、80%〜100%の可視光線透過率を有するガラス又は透明プラスチック基板である、
請求項14に記載の窓戸用機能性建材。
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