JP2016533869A - 高光沢金属効果紙 - Google Patents
高光沢金属効果紙 Download PDFInfo
- Publication number
- JP2016533869A JP2016533869A JP2016519992A JP2016519992A JP2016533869A JP 2016533869 A JP2016533869 A JP 2016533869A JP 2016519992 A JP2016519992 A JP 2016519992A JP 2016519992 A JP2016519992 A JP 2016519992A JP 2016533869 A JP2016533869 A JP 2016533869A
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- JP
- Japan
- Prior art keywords
- paper
- phenyl
- alkyl
- paperboard
- acrylate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 229910052751 metal Inorganic materials 0.000 title abstract description 19
- 239000002184 metal Substances 0.000 title abstract description 19
- 230000000694 effects Effects 0.000 title description 3
- 238000000034 method Methods 0.000 claims abstract description 35
- 239000000758 substrate Substances 0.000 claims abstract description 33
- 239000011248 coating agent Substances 0.000 claims abstract description 22
- 238000000576 coating method Methods 0.000 claims abstract description 22
- 238000004806 packaging method and process Methods 0.000 claims abstract description 7
- 239000000123 paper Substances 0.000 claims description 80
- 239000000203 mixture Substances 0.000 claims description 74
- 229910052782 aluminium Inorganic materials 0.000 claims description 35
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 35
- 150000001875 compounds Chemical class 0.000 claims description 30
- 238000007639 printing Methods 0.000 claims description 30
- 239000011087 paperboard Substances 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 25
- 239000011230 binding agent Substances 0.000 claims description 20
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 17
- 229920006317 cationic polymer Polymers 0.000 claims description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 8
- 229920000728 polyester Polymers 0.000 claims description 8
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 7
- 229910052753 mercury Inorganic materials 0.000 claims description 7
- 229920000570 polyether Polymers 0.000 claims description 7
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 6
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 claims description 6
- 150000001412 amines Chemical class 0.000 claims description 5
- 229910052733 gallium Inorganic materials 0.000 claims description 4
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- MPQXHAGKBWFSNV-UHFFFAOYSA-N oxidophosphanium Chemical class [PH3]=O MPQXHAGKBWFSNV-UHFFFAOYSA-N 0.000 claims description 3
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims description 2
- 230000001747 exhibiting effect Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- -1 oxime ester compounds Chemical class 0.000 description 105
- 125000000217 alkyl group Chemical group 0.000 description 63
- 239000000049 pigment Substances 0.000 description 62
- 239000000976 ink Substances 0.000 description 46
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 37
- 229920000642 polymer Polymers 0.000 description 27
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 24
- 239000001257 hydrogen Substances 0.000 description 24
- 229910052739 hydrogen Inorganic materials 0.000 description 24
- 239000002904 solvent Substances 0.000 description 24
- 239000002966 varnish Substances 0.000 description 23
- 150000002431 hydrogen Chemical class 0.000 description 20
- 125000001624 naphthyl group Chemical group 0.000 description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 19
- 229910052736 halogen Inorganic materials 0.000 description 19
- 150000002367 halogens Chemical class 0.000 description 19
- 239000000020 Nitrocellulose Chemical group 0.000 description 17
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical group O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 description 17
- 229920001220 nitrocellulos Chemical group 0.000 description 17
- 229920001577 copolymer Polymers 0.000 description 16
- 235000019441 ethanol Nutrition 0.000 description 16
- 229920005989 resin Polymers 0.000 description 16
- 239000011347 resin Substances 0.000 description 16
- 239000010410 layer Substances 0.000 description 14
- 150000002148 esters Chemical class 0.000 description 13
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 12
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 12
- 239000000178 monomer Substances 0.000 description 12
- 239000000047 product Substances 0.000 description 12
- 125000003545 alkoxy group Chemical group 0.000 description 11
- 239000000975 dye Substances 0.000 description 11
- 239000010408 film Substances 0.000 description 11
- 229920005862 polyol Polymers 0.000 description 11
- 125000006552 (C3-C8) cycloalkyl group Chemical group 0.000 description 10
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 10
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 10
- 239000004922 lacquer Substances 0.000 description 10
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical class CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 150000003077 polyols Chemical class 0.000 description 9
- 229910052717 sulfur Inorganic materials 0.000 description 9
- 125000004414 alkyl thio group Chemical group 0.000 description 8
- 125000002768 hydroxyalkyl group Chemical group 0.000 description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 125000004642 (C1-C12) alkoxy group Chemical group 0.000 description 7
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 7
- 229920002678 cellulose Polymers 0.000 description 7
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 6
- 125000002947 alkylene group Chemical group 0.000 description 6
- 239000012965 benzophenone Substances 0.000 description 6
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 6
- 239000001913 cellulose Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- 229920000647 polyepoxide Polymers 0.000 description 6
- 239000004814 polyurethane Substances 0.000 description 6
- 239000002002 slurry Substances 0.000 description 6
- 125000006710 (C2-C12) alkenyl group Chemical group 0.000 description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 5
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 5
- 239000004593 Epoxy Substances 0.000 description 5
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical group CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 5
- 239000004952 Polyamide Substances 0.000 description 5
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical class C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 5
- 150000001298 alcohols Chemical class 0.000 description 5
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 5
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 238000000151 deposition Methods 0.000 description 5
- 230000008021 deposition Effects 0.000 description 5
- 125000004430 oxygen atom Chemical group O* 0.000 description 5
- 238000005240 physical vapour deposition Methods 0.000 description 5
- 229920002647 polyamide Polymers 0.000 description 5
- 229920002635 polyurethane Polymers 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 229920006395 saturated elastomer Polymers 0.000 description 5
- 239000000600 sorbitol Substances 0.000 description 5
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 4
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 125000003277 amino group Chemical group 0.000 description 4
- 125000005428 anthryl group Chemical group [H]C1=C([H])C([H])=C2C([H])=C3C(*)=C([H])C([H])=C([H])C3=C([H])C2=C1[H] 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- 150000008366 benzophenones Chemical class 0.000 description 4
- 150000001735 carboxylic acids Chemical class 0.000 description 4
- 229920002301 cellulose acetate Polymers 0.000 description 4
- 229920006217 cellulose acetate butyrate Polymers 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 150000002009 diols Chemical class 0.000 description 4
- PPSZHCXTGRHULJ-UHFFFAOYSA-N dioxazine Chemical compound O1ON=CC=C1 PPSZHCXTGRHULJ-UHFFFAOYSA-N 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 229920001519 homopolymer Polymers 0.000 description 4
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 4
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 4
- 229940011051 isopropyl acetate Drugs 0.000 description 4
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 4
- GWYFCOCPABKNJV-UHFFFAOYSA-M isovalerate Chemical compound CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 description 4
- 150000002576 ketones Chemical class 0.000 description 4
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 4
- 239000011976 maleic acid Substances 0.000 description 4
- 125000005561 phenanthryl group Chemical group 0.000 description 4
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 229920000098 polyolefin Polymers 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 230000003746 surface roughness Effects 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 4
- 238000001771 vacuum deposition Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 125000006729 (C2-C5) alkenyl group Chemical group 0.000 description 3
- PCKZAVNWRLEHIP-UHFFFAOYSA-N 2-hydroxy-1-[4-[[4-(2-hydroxy-2-methylpropanoyl)phenyl]methyl]phenyl]-2-methylpropan-1-one Chemical compound C1=CC(C(=O)C(C)(O)C)=CC=C1CC1=CC=C(C(=O)C(C)(C)O)C=C1 PCKZAVNWRLEHIP-UHFFFAOYSA-N 0.000 description 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 3
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 3
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 3
- 125000003860 C1-C20 alkoxy group Chemical group 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 3
- 239000001856 Ethyl cellulose Substances 0.000 description 3
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 3
- 239000004642 Polyimide Substances 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 3
- 238000003848 UV Light-Curing Methods 0.000 description 3
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 3
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 3
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 3
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 3
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 3
- 150000001408 amides Chemical class 0.000 description 3
- 150000001450 anions Chemical class 0.000 description 3
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 3
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 229910052794 bromium Inorganic materials 0.000 description 3
- 229940043232 butyl acetate Drugs 0.000 description 3
- 125000001589 carboacyl group Chemical group 0.000 description 3
- 239000008199 coating composition Substances 0.000 description 3
- 238000001723 curing Methods 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 239000003085 diluting agent Substances 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000003822 epoxy resin Substances 0.000 description 3
- 229940093499 ethyl acetate Drugs 0.000 description 3
- 229920001249 ethyl cellulose Polymers 0.000 description 3
- 235000019325 ethyl cellulose Nutrition 0.000 description 3
- 239000005038 ethylene vinyl acetate Substances 0.000 description 3
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 3
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical class I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 235000019239 indanthrene blue RS Nutrition 0.000 description 3
- 239000001023 inorganic pigment Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 150000002734 metacrylic acid derivatives Chemical class 0.000 description 3
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- FAQJJMHZNSSFSM-UHFFFAOYSA-N phenylglyoxylic acid Chemical class OC(=O)C(=O)C1=CC=CC=C1 FAQJJMHZNSSFSM-UHFFFAOYSA-N 0.000 description 3
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 3
- 229920000768 polyamine Polymers 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 description 3
- 239000005020 polyethylene terephthalate Substances 0.000 description 3
- 229920001721 polyimide Polymers 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical class CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
- 239000005060 rubber Substances 0.000 description 3
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 3
- 125000005409 triarylsulfonium group Chemical group 0.000 description 3
- 229920006305 unsaturated polyester Polymers 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- XEESNYHCBUBXIN-UHFFFAOYSA-N 1,1'-biphenyl;4-(2-hydroxyethylsulfanyl)benzaldehyde Chemical compound C1=CC=CC=C1C1=CC=CC=C1.OCCSC1=CC=C(C=O)C=C1 XEESNYHCBUBXIN-UHFFFAOYSA-N 0.000 description 2
- MYWOJODOMFBVCB-UHFFFAOYSA-N 1,2,6-trimethylphenanthrene Chemical compound CC1=CC=C2C3=CC(C)=CC=C3C=CC2=C1C MYWOJODOMFBVCB-UHFFFAOYSA-N 0.000 description 2
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
- 239000012956 1-hydroxycyclohexylphenyl-ketone Substances 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- HCLJOFJIQIJXHS-UHFFFAOYSA-N 2-[2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOCCOC(=O)C=C HCLJOFJIQIJXHS-UHFFFAOYSA-N 0.000 description 2
- PTJWCLYPVFJWMP-UHFFFAOYSA-N 2-[[3-hydroxy-2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)COCC(CO)(CO)CO PTJWCLYPVFJWMP-UHFFFAOYSA-N 0.000 description 2
- XMLYCEVDHLAQEL-UHFFFAOYSA-N 2-hydroxy-2-methyl-1-phenylpropan-1-one Chemical compound CC(C)(O)C(=O)C1=CC=CC=C1 XMLYCEVDHLAQEL-UHFFFAOYSA-N 0.000 description 2
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- 125000002948 undecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 238000001429 visible spectrum Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000002025 wood fiber Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
- WGEATSXPYVGFCC-UHFFFAOYSA-N zinc ferrite Chemical compound O=[Zn].O=[Fe]O[Fe]=O WGEATSXPYVGFCC-UHFFFAOYSA-N 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
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Abstract
Description
本発明は、紙基材上に鮮やかな光沢のある金属コーティングを製造するための方法に関する。本発明の更なる態様は、本方法を用いて得られる紙製品及びかかる紙の装飾又は包装目的のための使用である。
A)1種以上のエチレン性不飽和化合物と1種以上の光開始剤を含む硬化性組成物を紙基材の表側の少なくとも一部分に適用する工程;
B)UVランプを使用して組成物を硬化する工程;及び
C)バインダー並びに5.0μm〜15μmの平均直径及び7nm〜32nmの厚さを有する蒸着アルミニウム粒子を含むアルミニウム層を、硬化組成物上に印刷する工程
を含む、前記方法に関する。
a)紙基材を、装置を介して供給するための機構、
b)液状のUV硬化性組成物の供給源及び該供給源からの液体組成物を基材の表面に適用するための手段、及び該組成物を硬化するための手段を含むコーティングステーション及び
c)メタリックインクを印刷し、その後、該インクを乾燥させるための手段
を含む、印刷装置で実施される。
− テスリン(Teslin)(登録商標)(PPGインダストリーズ、微多孔質、高充填、単層(sinle layer)、ポリオレフィン系合成材料)又はYupo(登録商標)(Covert−All, Inc.;不透明な白色、多層二軸延伸ポリプロピレン(BOPP)製品)のようなフィルム合成紙;
− ファイバー合成紙(木繊維の代わりのポリマー繊維);及び
− フィルム積層合成紙:紙/フィルム/紙、例えば、Durasafe(登録商標)(Land−quart社);フィルム/紙/フィルム、例えば、ハイブリッド紙幣基材(Giesecke & Devrient社;綿繊維コアの周りの保護ポリエステルフィルムの組み合わせ)。
− 中圧水銀アークは、スペクトル出力を変化させるために小さな割合で金属ハロゲン化物の封入によって変更される:
− 鉄ドープ−350〜450nmにシフトされたスペクトル出力;
− ガリウムドープ−非常に少ない紫外線を放射する;紫と青のスペクトル領域における発光(波長/nm:ガリウム(Ga)403、417及び鉄(Fe)358、372、374/5、382、386、388で金属ヨウ化物を用いて水銀アークをドープすることによる予想される追加のUVライン);及び
− 集束反射型ダイオードアレイ(FRDA)システム(igb−tech GmbH)、例えば、FRDA202は約400nmの発光ピークを有する。マルチスペクトルランプも使用され得る。
又はR50は非置換のC1〜C20アルキルであるか又は1つ以上のハロゲン、C1〜C12アルコキシ、C1〜C12アルキルチオ、NR53R54又は−(CO)−O−C1〜C24アルキルによって置換されたC1〜C20アルキルであり;
R51は非置換のシクロヘキシル、シクロペンチル、フェニル、ナフチル又はビフェニリルであるか;又は1つ以上のハロゲン、C1〜C12アルキル、C1〜C12アルコキシ、C1〜C12アルキルチオ、又はNR53R54によって置換されたシクロヘキシル、シクロペンチル、フェニル、ナフチル又はビフェニリルであるか;又はR51は−(CO)R’52であるか;又はR51は、非置換の又は1つ以上のハロゲン、C1〜C12アルコキシ、C1〜C12アルキルチオ、又はNR53R54によって置換されたC1〜C12アルキルであり;
R52及びR’52は互いに独立して非置換のシクロヘキシル、シクロペンチル、フェニル、ナフチル又はビフェニリルであるか、又は1つ以上のハロゲン、C1〜C4アルキル又はC1〜C4アルコキシによって置換されたシクロヘキシル、シクロペンチル、フェニル、ナフチル又はビフェニリルであるか;又はR52はS原子又はN原子を含む5員又は6員の複素環であり;
R53及びR54は互いに独立して水素、非置換のC1〜C12アルキル又は1つ以上のOH又はSHによって置換されたC1〜C12アルキルであり、その際、アルキル鎖は任意に1個〜4個の酸素原子によって中断されるか;又はR53及びR54は互いに独立してC2〜C12−アルケニル、シクロペンチル、シクロヘキシル、ベンジル又はフェニルである)
のものである。
R68は水素、C1〜C4アルキル、C1〜C4ハロゲンアルキル、フェニル、N(C1〜C4アルキル)2、COOCH3、
Qは2〜6個のヒドロキシ基を有するポリヒドロキシ化合物の残基であり;
xは1より大きいがQで利用可能なヒドロキシル基の数より大きくない数字であり;
Aは−[O(CH2)bCO]y−又は−[O(CH2)bCO](y−1)−[O(CHR71CHR70)a]y−であり;
R69は水素、メチル又はエチルであり;Nが1より大きい場合、基R69は互いに同じ又は互いに異なってよく;
aは1〜2の数字であり;
bは4〜5の数字であり;
yは1〜10の数字であり;
nは;且つ
mは2〜10の整数である)
の化合物である。
R30は水素、C1〜C18アルキル、C1〜C12ヒドロキシアルキル、C1〜C18アルコキシ、OCH2CH2−OR34、モルホリノ、S−C1〜C18アルキル、基−HC=CH2、−C(CH3)=CH2
d、e及びfは1〜3であり;
cは2〜10であり;
G1及びG2は互いに独立してポリマー構造の末端基、好ましくは水素又はメチルであり;
R34は水素、
R31は、ヒドロキシ、C1〜C16アルコキシ、モルホリノ、ジメチルアミノ又は−O(CH2CH2O)g−C1〜C16アルキルであり;
gは1〜20であり;
R32及びR33は、互いに独立して水素、C1〜C6アルキル、C1〜C16アルコキシ又は−O(CH2CH2O)g−C1〜C16アルキルであるか;又は非置換のフェニル又はベンジルであるか;又はC1〜C12アルキルによって置換されたフェニル又はベンジルであるか;又はR32及びR33は、それらが結合される炭素原子と一緒にシクロヘキシル環を形成し;
R35は水素、OR36又はNR37R38であり;
R36は水素、任意に1つ以上の非連続的なO原子により中断されたC1〜C12アルキルであり、その中断されていない又は中断されたC1〜C12アルキルは任意に1つ以上のOHによって置換されているか、
又はR36は
R37及びR38は、互いに独立して水素又は非置換の又は1つ以上のOHによって置換されたC1〜C12アルキルであり;
R39は、任意に1つ以上の非連続的なOによって中断されたC1〜C12アルキレン、−(CO)−NH−C1〜C12アルキレン−NH−(CO)−又は
但し、R31、R32及びR33は全て一緒にC1〜C16アルコキシ又は−O(CH2CH2O)g−C1〜C16アルキルではないことを条件とする)
のものである。
R55、R56、R57、R58及びR59は、互いに独立して、水素、非置換のC1〜C12アルキル又は1つ以上のOH、C1〜C4アルコキシ、フェニル、ナフチル、ハロゲン又はCNによって置換されたC1〜C12アルキルであり;その際、アルキル鎖は、任意に1個以上の酸素原子によって中断されているか;又はR55、R56、R57、R58及びR59は、互いに独立してC1〜C4アルコキシ、C1〜C4アルキルチオ又はNR52R53であり;
R52及びR53は互いに独立して水素、非置換のC1〜C12アルキル又は1つ以上のOH又はSHによって置換されたC1〜C12アルキルであり、その際、アルキル鎖は任意に1個〜4個の酸素原子によって中断されているか;又はR52及びR53は互いに独立してC2〜C12−アルケニル、シクロペンチル、シクロヘキシル、ベンジル又はフェニルであり;且つ
Y1は任意に1個以上の酸素原子によって中断されるC1〜C12アルキレンである)
のものである。
zは0又は1であり;
R70は、水素、C3〜C8シクロアルキル;非置換の又は1つ以上のハロゲン、フェニル又はCNによって置換されたC1〜C12アルキルであるか;又はR70はC2〜C5アルケニル;非置換の又は1つ以上のC1〜C6アルキル、ハロゲン、CN、OR73、SR74又はNR75R76によって置換されたフェニルであるか;又はR70はC1〜C8アルコキシ、ベンジルオキシ;又は非置換の又は1つ以上のC1〜C6アルキル又はハロゲンによって置換されたフェノキシであり;
R71はフェニル、ナフチル、ベンゾイル又はナフトイルであり、それぞれが、1つ以上のハロゲン、C1〜C12アルキル、C3〜C8シクロアルキル、ベンジル、フェノキシカルボニル、C2〜C12アルコキシカルボニル、OR73、SR74、SOR74、SO2R74又はNR75R76によって置換され、その際、置換基OR73、SR74及びNR75R76は任意に、フェニル環又はナフチル環上で更なる置換基と一緒に基R73、R74、R75及び/又はR76を介して5員環又は6員環を形成するか;又はそれぞれがフェニルによって又は1つ以上のOR73、SR74若しくはNR75R66によって置換されたフェニルによって置換されるか;
又はR71はチオキサンチル、又は
R72は水素;非置換のC1〜C20アルキル又は1つ以上のハロゲン、OR73、SR74、C3〜C8シクロアルキル若しくはフェニルによって置換されたC1〜C20アルキルであるか;又はC3〜C8シクロアルキルであるか;又は非置換の又は1つ以上のC1〜C6アルキル、フェニル、ハロゲン、OR73、SR74又はNR75R76によって置換されたフェニルであるか;又は非置換の又は1つ以上のC1〜C6アルキル、フェニル、OR73、SR74又はNR75R76によって置換されたC2〜C20アルカノイル又はベンゾイルであるか;又はC2〜C12アルコキシカルボニル、フェノキシカルボニル、CN、CONR75R76、NO2、C1〜C4ハロアルキル、S(O)y−C1〜C6アルキル、又はS(O)y−フェニルであり、
yは1又は2であり;
Y2は直接結合しているか又は結合していない;
Y3はNO2又は
R73及びR74は互いに独立して水素、C1〜C20アルキル、C2〜C12アルケニル、C3〜C8シクロアルキル、1つ以上、好ましくは2つのOによって中断されたC3〜C8シクロアルキル、フェニル−C1〜C3アルキルであるか;又はOH、SH、CN、C1〜C8アルコキシ、C1〜C8アルカノイル、C3〜C8シクロアルキルによって、1つ以上のOによって中断されたC3〜C8シクロアルキルによって置換されたC1〜C8アルキルであるか、又はそのC1〜C8アルキルが非置換の又は1つ以上のC1〜C6アルキル、ハロゲン、OH、C1〜C4アルコキシ又はC1〜C4アルキルスルファニルによって置換されたベンゾイルによって置換されるか;又はフェニル又はナフチルであり、それぞれが非置換であるか又はハロゲン、C1〜C12アルキル、C1〜C12アルコキシ、フェニル−C1〜C3アルキルオキシ、フェノキシ、C1〜C12アルキルスルファニル、フェニルスルファニル、N(C1〜C12アルキル)2、ジフェニルアミノ又は
R75及びR76は、互いに独立して、水素、C1〜C20アルキル、C2〜C4ヒドロキシアルキル、C2〜C10アルコキシアルキル、C2〜C5アルケニル、C3〜C8シクロアルキル、フェニル−C1〜C3アルキル、C1〜C8アルカノイル、C3〜C12アルケノイル、ベンゾイルであるか;又はフェニル又はナフチルであり、それぞれが非置換であるか又はC1〜C12アルキル、ベンゾイル又はC1〜C12アルコキシによって置換されるか;又はR75及びR76は、一緒になって、任意にO又はNR73によって中断されたC2〜C6アルキレンであり且つ任意にヒドロキシル、C1〜C4アルコキシ、C2〜C4アルカノイルオキシ又はベンゾイルオキシによって置換され;
R77は、C1〜C12アルキル、チエニル又は非置換の又はC1〜C12アルキル、OR73、モルホリノ又はN−カルバゾリルによって置換されたフェニルである)
のものである。
R83は直接結合、S、O、CH2、(CH2)2、CO又はNR89であり;
R84、R85、R86及びR87は、互いに独立して、水素、C1〜C20アルキル、C3〜C8シクロアルキル、C1〜C20アルコキシ、C2〜C20アルケニル、CN、OH、ハロゲン、C1〜C6アルキルチオ、フェニル、ナフチル、フェニル−C1〜C7アルキル、ナフチル−C1〜C3アルキル、フェノキシ、ナフチルオキシ、フェニル−C1〜C7アルキルオキシ、ナフチル−C1〜C3アルキルオキシ、フェニル−C2〜C6アルケニル、ナフチル−C2〜C4アルケニル、S−フェニル、(CO)R89、O(CO)R89、(CO)OR89、SO2R89又はOSO2R89であり;
R88は、C1〜C20アルキル、C1〜C20ヒドロキシアルキル、
R89は、水素、C1〜C12アルキル、C1〜C12ヒドロキシアルキル、フェニル、ナフチル又はビフェニリルであり;
R90、R91、R92及びR93は、互いに独立して、R84に対して与えられた意味の1つを有するか;又はR90及びR91は、それらが結合されるベンゼン環と縮合環系を形成するように接合され;
R95は、直接結合、S、O又はCH2であり;
R96は、水素、C1〜C20アルキル;1つ以上のOによって中断されたC2〜C20アルキル;又は−L−M−R98又は−L−R98であり;
R97は、R96に対して与えられた意味の1つを有するか又は
R98は一価の増感剤又は光開始剤の部分であり;
Ar1及びAr2は、互いに独立して、非置換の又はC1〜C20アルキル、ハロゲン又はOR99によって置換されたフェニルであるか;
又は非置換のナフチル、アントリル、フェナントリル又はビフェニリルであるか;
又はC1〜C20アルキル、OH又はOR99によって置換されたナフチル、アントリル、フェナントリル又はビフェニリルであるか;
又は−Ar4−A1−Ar3又は
Ar3は、非置換のフェニル、ナフチル、アントリル、フェナントリル又はビフェニリルであるか;
又はフェニル、ナフチル、アントリル、フェナントリル又はC1〜C20アルキル、OR99若しくはベンゾイルによって置換されたビフェニリルであり;
Ar4は、フェニレン、ナフチレン、アントリレン又はフェナントリレンであり;
A1は、直接結合、S、O又はC1〜C20アルキレンであり;
Xは、CO、C(O)O、OC(O)、O、S又はNR99であり;
Lは、直接結合、S、O、C1〜C20アルキレン又は1つ以上の非連続的なOによって中断されたC2〜C20アルキレンであり;
R99は、C1〜C20アルキル又はC1〜C20ヒドロキシアルキルであるか;又はO(CO)R102によって置換されたC1〜C20アルキルであり;
M1は、S、CO又はNR100であり;
M2は、直接結合、CH2、O又はSであり;
R100及びR101は互いに独立して水素、ハロゲン、C1〜C8アルキル、C1〜C8アルコキシ又はフェニルであり;
R102はC1〜C20アルキルであり;
R103は
Eはアニオン、特にPF6、SbF6、AsF6、BF4、(C6F5)4B、Cl、Br、HSO4、CF3−SO3、F−SO3、
のものである。
Eは、アニオン、特にPF6、SbF6、AsF6、BF4、(C6F5)4B、Cl、Br、HSO4、CF3−SO3、F−SO3、
のものである。
(a)5.0〜0.5質量%、特に5.0〜1.0質量%、非常に特に4.0〜2.5質量%の光開始剤、及び
(b)99.5〜95質量%、特に99〜95質量%、非常に特に97.5〜96質量%の1種以上のエチレン性不飽和樹脂、モノマー又はそれらの混合物
を含み、
その際、成分a)〜c)の合計は100%である。
基材:ホワイトボード、Invercote T 220g/m2、275μm(高品質コート紙、Iggesund Paperboard Europe社)。印刷面を完全に被覆し、マットレベルに仕上げる。表面粗さ1.1μm
ワニスの調製:75.3gのニトロセルロース(DHX 3/5 IPA、70%の固形分、Nobel Enterprises、英国)を、2000mlのガラス瓶において220.5gの酢酸エチル(99〜100%の純度、Brenntag社)、557.2gのn−プロピルアセテート、147gのドワノールPMにゆっくりと添加し、室温で完全に溶解するまで穏やかに撹拌する。その後、固形分の測定を実施し、酢酸エチルの量を、ワニスの調製で5.27%の固体含有率の値を達成するように調整する。
10%のアルミニウム顔料+45%の酢酸エチル+45%のイソプロピルアセテート。
メタリックインクを調製するための手順:アルミニウム顔料のスラリーを、顔料対バインダーの比を1:1に調整するような比で上記のニトロセルロースワニスに添加し、酢酸エチルを、インクを印刷粘度に調整するために添加する(2カップ20秒の速度)。得られた分散液を、ディスパーマット(Dispermat)を用いて800rpmで10分間撹拌する。
メタリックインクの調製手順:アルミニウム顔料スラリーを、顔料対バインダーの比を3:1に調整するような比で上記のニトロセルロースワニスに添加し;酢酸エチルを、インクを印刷粘度に調整するために添加する(2カップ20秒の速度)。得られた分散液を、ディスパーマット(Dispermat)を用いて800rpmで10分間撹拌する。
印刷速度30m/分、UV硬化強度50ワット/cm2、溶媒インクの乾燥温度80℃、UVグラビアシリンダー30l/cmスクリーン、溶媒インクグラビアシリンダー120l/cmスクリーン。結果を第1表に示す。
基材:Raflabrite RH1 85g/m2、71μm(良好な印刷定義と細かなディテールを必要とする高品質のマルチカラーラベルのための多目的ラベル紙、UPMラフラタック社)。粗さ0.7μm。
様々なアルミニウム顔料グレードのUV被覆及び未被覆の板紙上での光沢の比較。
UV−ラッカーとメタリックインクを、実施例1に記載されるように調製する。第3表は様々なメタリックインクをまとめる。
紙を、ワイヤーバー1を用いてメタルインクを塗布し、空気乾燥機で乾燥させる。
試験手順:UVニスを、5質量部のIrgacure 1173(RTM)、BASFを、95質量部の樹脂に添加することによって製造する。UVニスを、ワイヤーバー0(4ミクロン)、1(6ミクロン)、2(12ミクロン)、3(24ミクロン)を用いてInvercote T板紙上に被覆する。被覆された紙を、UV光(Aktiprintミニ18−2、水銀管、位置20)下で硬化し、ワイヤーバー1を用いて金属インク1で上塗りする(6ミクロンの湿潤膜厚)。結果を第5表に示す。
UVニス1:37%のLaromer DPGDA、24%のLaromer LR8863、23%のLaromer 8986、10%のEbecryl P115、3%のIrgacure 127、3%のIrgacure 819
UVニス2:46%のLaromer LR8986、36%のLaromer PO77F、14%のLaromer TPGDA、4% Irgacure 127
インク2のアルミニウム粒子(D50、8.0μm〜12.0μm、厚さ13nm)を用いて実施例1で製造されるようなニトロセルロースワニス
Claims (14)
- 紙又は板紙の基材上で光沢を示す滑らかな装飾的な表面コーティングを形成するための方法であって、以下の工程:
A)1種以上のエチレン性不飽和化合物と1種以上の光開始剤を含む硬化性組成物を、紙基材の表側の少なくとも一部分に適用する工程;
B)UVランプを使用して組成物を硬化する工程;及び
C)バインダー及び5.0μm〜15μmの平均直径及び7nm〜32nmの厚さを有する蒸着アルミニウム粒子を含むアルミニウム層を、硬化組成物上に印刷する工程
を含む、前記方法。 - 20°のジオメトリで測定された光沢が、500の相対光沢単位よりも高い値を有する、請求項1に記載の方法。
- 蒸着アルミニウム粒子の平均直径が、8.0μm〜12μmであり、厚さが11〜18nmである、請求項1又は2に記載の方法。
- 蒸着アルミニウム粒子の平均直径が、8.0μm〜12μmであり、厚さが12〜14nmである、請求項1から3までのいずれか1項に記載の方法。
- 紙又は板紙の基材が、1.5μm未満、好ましくは1.1μm未満の粗さを有する、請求項1から4までのいずれか1項に記載の方法。
- 紙又は板紙の基材が、30g/m2〜300g/m2の質量を有する、請求項1から5までのいずれか1項に記載の方法。
- ランプが、ガリウム、又は鉄ドープ中圧水銀ランプである、請求項1から6までのいずれか1項に記載の方法。
- 光開始剤が、モノ及びビスアシルホスフィンオキシド、α−ヒドロキシケトン、α−アルコキシケトン、又はα−アミノケトン化合物及びそれらの混合物から選択される、請求項1から7までのいずれか1項に記載の方法。
- 硬化性組成物が、エトキシル化オリゴエーテルアクリレート、エトキシル化アミン変性ポリエーテルアクリレート、エポキシアクリレート、ポリエステルアクリレート又はウレタンアクリレートを含む、請求項1から8までのいずれか1項に記載の方法。
- 硬化性組成物が、エトキシル化アミン変性ポリエーテルアクリレート又はエポキシアクリレートを含む、請求項9に記載の方法。
- 紙又は板紙を、硬化性組成物を紙基材の表側の少なくとも一部に適用する前に、表側でカチオン性ポリマーを用いて処理する、請求項1から10までのいずれか1項に記載の方法。
- カチオン性ポリマーがポリビニルアミンである、請求項11に記載の方法。
- 請求項1から12までのいずれか1項に記載の方法を用いて得られる紙又は板紙製品。
- 請求項13に記載の紙又は板紙製品の、装飾又は包装目的のための使用。
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CN106103846A (zh) | 2016-11-09 |
US20160230339A1 (en) | 2016-08-11 |
JP6605455B2 (ja) | 2019-11-13 |
WO2015049262A1 (en) | 2015-04-09 |
BR112016006911B1 (pt) | 2022-01-11 |
BR112016006911A2 (pt) | 2017-08-01 |
EP3052701B1 (en) | 2017-06-28 |
US10494766B2 (en) | 2019-12-03 |
CN106103846B (zh) | 2018-08-21 |
EP3052701A1 (en) | 2016-08-10 |
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