JP2016523909A - 毛髪を処置するための組成物及び方法 - Google Patents
毛髪を処置するための組成物及び方法 Download PDFInfo
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- JP2016523909A JP2016523909A JP2016523878A JP2016523878A JP2016523909A JP 2016523909 A JP2016523909 A JP 2016523909A JP 2016523878 A JP2016523878 A JP 2016523878A JP 2016523878 A JP2016523878 A JP 2016523878A JP 2016523909 A JP2016523909 A JP 2016523909A
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- composition
- polymer
- latex
- mpa
- hair
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- 230000036961 partial effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920006149 polyester-amide block copolymer Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 230000036316 preload Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
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- AZIQALWHRUQPHV-UHFFFAOYSA-N prop-2-eneperoxoic acid Chemical compound OOC(=O)C=C AZIQALWHRUQPHV-UHFFFAOYSA-N 0.000 description 1
- SOGFHWHHBILCSX-UHFFFAOYSA-J prop-2-enoate silicon(4+) Chemical compound [Si+4].[O-]C(=O)C=C.[O-]C(=O)C=C.[O-]C(=O)C=C.[O-]C(=O)C=C SOGFHWHHBILCSX-UHFFFAOYSA-J 0.000 description 1
- LYBIZMNPXTXVMV-UHFFFAOYSA-N propan-2-yl prop-2-enoate Chemical compound CC(C)OC(=O)C=C LYBIZMNPXTXVMV-UHFFFAOYSA-N 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- VJURMBXGVSZCFO-UHFFFAOYSA-N propane-1,2-diol;n-propylpropan-1-amine Chemical compound CC(O)CO.CCCNCCC VJURMBXGVSZCFO-UHFFFAOYSA-N 0.000 description 1
- AKNQYIXNIUXHFU-UHFFFAOYSA-N propane-1,3-diol;n-propylpropan-1-amine Chemical compound OCCCO.CCCNCCC AKNQYIXNIUXHFU-UHFFFAOYSA-N 0.000 description 1
- AOHJOMMDDJHIJH-UHFFFAOYSA-N propylenediamine Chemical compound CC(N)CN AOHJOMMDDJHIJH-UHFFFAOYSA-N 0.000 description 1
- KIDHWZJUCRJVML-UHFFFAOYSA-N putrescine Chemical compound NCCCCN KIDHWZJUCRJVML-UHFFFAOYSA-N 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000012421 spiking Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- UFDHBDMSHIXOKF-UHFFFAOYSA-N tetrahydrophthalic acid Natural products OC(=O)C1=C(C(O)=O)CCCC1 UFDHBDMSHIXOKF-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- YODZTKMDCQEPHD-UHFFFAOYSA-N thiodiglycol Chemical compound OCCSCCO YODZTKMDCQEPHD-UHFFFAOYSA-N 0.000 description 1
- 229950006389 thiodiglycol Drugs 0.000 description 1
- 235000019303 thiodipropionic acid Nutrition 0.000 description 1
- 229940029614 triethanolamine stearate Drugs 0.000 description 1
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- 229920001567 vinyl ester resin Polymers 0.000 description 1
- NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 description 1
- 229920003176 water-insoluble polymer Polymers 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
Classifications
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D7/00—Processes of waving, straightening or curling hair
- A45D7/06—Processes of waving, straightening or curling hair combined chemical and thermal
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D7/00—Processes of waving, straightening or curling hair
- A45D2007/002—Processes of dressing hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/594—Mixtures of polymers
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Cosmetics (AREA)
Abstract
Description
本出願は、2013年6月28日に出願された米国特許出願第13/931,187号に基づく優先権を主張し、その全体が参照により本明細書に組み込まれる。
本開示の様々な例示的実施形態によれば、少なくとも1種が皮膜形成ポリマーである少なくとも2種のラテックスポリマーは、約0.05MPaから約5GPaのヤング率、及び/又は0.5MPaの応力下で約300%までの範囲の歪みを有する皮膜を生成する組成物を提供するよう選択されてもよい。本開示の様々な例示的実施形態において、少なくとも2種のラテックスポリマーが、組成物の質量に対して、約0.1質量%から約30質量%の範囲の合わせた量で存在している。他の実施形態において、少なくとも2種のラテックスポリマーが、約10:1から約1:10の質量比で組成物中に存在している。
による任意のプレポリマーであってもよい。
H2N-R4-NH2
(式中、R4は、アルキレン基又はアルキレンオキシド基から選択され、前記基は、イオン性基又は潜在的イオン性基で置換されていない)
による少なくとも1種の鎖延長剤から選択されてもよい。
H2N-R5-NH2
(式中、R5は、イオン性基又は潜在的イオン性基で置換されているアルキレン基から選択される)
による少なくとも1種の鎖延長剤から選択されてもよい。少なくともある特定の例示的実施形態において、化合物は、イオン性基又は潜在的イオン性基及び2つのイソシアネート反応性基を有していてもよい。
本明細書に記載のとおり、本開示による例示的な組成物は、少なくとも2種のラテックスポリマーを含んでいてもよく、ラテックスポリマーのうちの少なくとも1種は皮膜形成ポリマーである。ある特定の実施形態において、ラテックスポリマーのそれぞれは、組成物の質量に対して、約0.05質量%から約10質量%、たとえば約0.1質量%から約7.5質量%、たとえば約0.25質量%から約5質量%、たとえば約0.5質量%から約2.5質量%、又は約0.5質量%から約1.5質量%の範囲の量で、その間のすべての範囲及び部分的範囲を含めて存在する。他の実施形態において、ラテックスポリマーのそれぞれは、組成物の質量に対して、約1質量%から約15質量%、たとえば約1質量%から約12質量%、たとえば約1.2質量%から約12質量%、たとえば約1.5質量%から約10質量%、又はたとえば約10質量%未満の範囲の量で、その間のすべての範囲及び部分的範囲を含めて存在する。また他の実施形態において、ラテックスポリマーのそれぞれは、組成物の質量に対して、約0.1質量%から約2質量%、たとえば約0.15質量%から約1.9質量%、又はたとえば約0.18質量%から約1.8質量%の範囲の量で、その間のすべての範囲及び部分的範囲を含めて存在する。
A.皮膜の物理的特性の決定のための手順
皮膜プレーティング:ラテックス皮膜を、4グラムのラテックスポリマーを含有する30グラム水溶液を、100mL PFAペトリ皿(直径100mm×高さ15mm)において、室温で少なくとも3日間ゆっくりと乾燥させることにより得た。
予圧力:0.001N
等温:25℃
浸漬時間:0.5分
力傾斜率:18Nまで0.5N/min
毛髪処置:通常の漂白をした毛髪のストリップ(IHIPから、幅1cm、長さ16cm、約2.0〜2.5gの毛髪)を、ラテックス溶液で処置した(0.75gの溶液/毛髪1g)。房の表面にわたって溶液が均一に分布するまで毛髪をくしでとかした。処置した毛髪を一晩室温で乾燥させた。
試験モード=圧縮
試験前速度=2mm/sec
試験速度=2mm/sec
試験後速度=2mm/sec
ターゲットモード=距離
距離=10mm
カウント=10
トリガータイプ=オート(力)
トリガー力=1g
(F1-F10)/F1×100。
毛髪処置:通常の漂白をした毛髪束(IHIPから、長さ14.5cm、約0.5g)を、2%ラテックスポリマーの溶液で処置した(0.5gの溶液/毛髪1g)。毛髪束表面にわたって溶液が均一に分布するまで毛髪をくしでとかした。次に処置した毛髪を、スパイラルロッド(直径0.5)上に巻き、一晩室温で乾燥させた。
(Lo-Lf)/(Lo-Li)×100
(式中、Lo=完全に伸長した毛髪の長さ、Li=湿気曝露前の初期の巻いた毛髪の長さ、及びLf=曝露24時間後の最終的な毛髪の長さ)。
DAITOSOL 5000AD(INCI名:アクリレートコポリマー、0.4MPaのヤング率及び0.5MPaの応力下で>150%の歪み;ポリマーA)及びNEOREZ(登録商標) R989(INCI名:ポリカルバミルポリグリコンエステル、654MPaのヤング率及び0.5MPaの応力下で0.07%の歪み;ポリマーB)の組合せから、様々なラテックスポリマー比で透過性の皮膜を得た。これらの物理的特性をTable 1(表1)に示す。
BAYCUSAN(登録商標) C1001(INCI名:ポリウレタン-34、3MPaのヤング率及び0.5MPaの応力下で18.82%の歪み;ポリマーA)及びLUVIFLEX(登録商標) SOFT(INCI名:アクリレートコポリマー、2758MPaのヤング率及び0.5MPaの応力下で<0.01%の歪み;ポリマーB)の組合せから、様々なラテックスポリマー比で透過性の皮膜を得た。これらの物理的特性を下のTable 2(表2)に示す。
透過性の皮膜を、様々なラテックスポリマー比のBAYCUSAN(登録商標) C1001(ポリマーA)及びNEOREZ(登録商標) R989(ポリマーB)の組合せから得た。これらの物理的特性を下のTable 3(表3)に示す。
透過性の皮膜を、様々なラテックスポリマー比のDAITOSOL 5000AD(ポリマーA)及びFIXATE SUPERHOLD(商標)(INCI名:ポリアクリレート-2クロスポリマー、1151MPaのヤング率及び0.5MPaの応力下で0.01%の歪み;ポリマーB)の組合せから得た。これらの物理的特性を下のTable 4A(表4)に示す。
毛髪房を、様々なラテックスポリマー比のDAITOSOL 5000AD(ポリマーA)及びNEOREZ(登録商標) R989(ポリマーB)の2%溶液で処置した。これらの力学的特性を下のTable 5(表6)に示す。
毛髪房を、様々なラテックスポリマー比のBAYCUSAN(登録商標) C1001(ポリマーA)及びLUVIFLEX(登録商標) SOFT(ポリマーB)の2%溶液で処置した。これらの力学的特性を下のTable 6(表7)に示す。
毛髪房を、様々なラテックスポリマー比のBAYCUSAN(登録商標) C1001(ポリマーA)及びNEOREZ(登録商標) R989(ポリマーB)の2%溶液で処置した。これらの力学的特性を下のTable 7(表8)に示す。
毛髪房を、DAITOSOL 5000AD(ポリマーA)及びFIXATE SUPERHOLD(商標)(ポリマーB)の2%溶液で、様々なラテックスポリマー比で処置した。これらの力学的特性を下のTable 8A(表9)に示す。
毛髪束を、様々なラテックスポリマー比のDAITOSOL 5000AD(ポリマーA)及びNEOREZ(登録商標) R989(ポリマーB)の2%溶液で処置した。多湿カール維持の結果を下のTable 9(表11)に示す。
毛髪束を、様々なラテックスポリマー比のBAYCUSAN(登録商標) C1001(ポリマーA)及びLUVIFLEX(登録商標) SOFT(ポリマーB)の2%溶液で処置した。多湿カール維持の結果を下のTable 10A(表12)に示す。
毛髪束を、様々なラテックスポリマー比のBAYCUSAN(登録商標) C1001(ポリマーA)及びNEOREZ(登録商標) R989(ポリマーB)の2%溶液で処置した。多湿カール維持の結果を下のTable 11(表15)に示す。
毛髪束を、様々なラテックスポリマー比のDAITOSOL 5000AD(ポリマーA)及びFIXATE SUPERHOLD(商標)(ポリマーB)の2%溶液で処置した。多湿カール維持の結果を下のTable 12A(表16)に示す。
通常の漂白をした毛髪を、様々なラテックスポリマー濃度の1:1比のLUVIFLEX(登録商標) SOFT及びBAYCUSAN(登録商標) C1001の溶液で処置した。三点曲げ試験及び多湿カール維持試験を上述のとおり実施した。結果を下のTable 13A(表18)に示す。
アミンで100%まで中和されたラテックスポリマーを含む水性分散体(アミノメチルプロパノール、AMP)を、未中和ラテックスポリマーを含む水性分散体と比較する。
Claims (26)
- 少なくとも2種のラテックスポリマーを含み、少なくとも1種のラテックスポリマーが皮膜形成ポリマーである毛髪スタイリング組成物であって;
少なくとも2種のラテックスポリマーが、組成物の質量に対して、約0.1質量%から約30質量%の範囲の合わせた量で存在し;
少なくとも2種のラテックスポリマーが、約10:1から約1:10の範囲の質量比で組成物中に存在し;
前記組成物が、約0.05MPaから約5GPaの範囲のヤング率、及び0.5MPaの応力下で約300%までの範囲の歪みを有する皮膜を生成する、
毛髪スタイリング組成物。 - 少なくとも2種のラテックスポリマーが、独立に、アクリレートラテックスポリマー及びポリウレタンラテックスポリマーから選択される、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、独立に又は一緒に、水性分散媒体中の分散粒子である、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、組成物の質量に対して、約0.5質量%から約10質量%の範囲の合わせた量で存在する、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、組成物の質量に対して、約1質量%から約5質量%の範囲の合わせた量で存在する、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、組成物の質量に対して、約1質量%から約3質量%の範囲の合わせた量で存在する、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーのそれぞれが、組成物の質量に対して、約0.05質量%から約10質量%の範囲の個別の量で存在する、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーのそれぞれが、組成物の質量に対して、約1質量%から約15質量%の範囲の個別の量で存在する、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーを含む組成物が、
(1)約0.1MPaから約10MPaの範囲のヤング率、及び0.5MPaの応力下で少なくとも約1%の歪みを有するポリマーA;
(2)約10MPaから約6GPaの範囲のヤング率、及び0.5MPaの応力下で約5%未満の歪みを有するポリマーB
を含む、請求項1に記載の毛髪スタイリング組成物。 - 少なくとも2種のラテックスポリマーが、独立に、アクリレートラテックスポリマー及びポリウレタンラテックスポリマーから選択される、請求項9に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、約1:5から約5:1の質量比で組成物中に存在する、請求項9に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、約1:3から約3:1の質量比で組成物中に存在する、請求項9に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、約1:2から約2:1の質量比で組成物中に存在する、請求項9に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーが、約1:1の質量比で組成物中に存在する、請求項9に記載の毛髪スタイリング組成物。
- 皮膜が、約80MPaから約5GPaの範囲のヤング率及び0.5MPaの応力下で約0.01%から約1%未満の範囲の歪みを有する、請求項9に記載の毛髪スタイリング組成物。
- ポリマーAのポリマーBに対する質量比が、約1:10から約1:1である、請求項15に記載の毛髪スタイリング組成物。
- 皮膜が、約5MPaから約100MPaの範囲のヤング率及び0.5MPaの応力下で約0.5%から約20%未満の範囲の歪みを有する、請求項9に記載の毛髪スタイリング組成物。
- ポリマーAのポリマーBに対する質量比が、約3:1から約10:1である、請求項17に記載の毛髪スタイリング組成物。
- 皮膜が、約0.05MPaから約5MPaの範囲のヤング率及び0.5MPaの応力下で約10%から約300%の範囲の歪みを有する、請求項9に記載の毛髪スタイリング組成物。
- ポリマーAのポリマーBに対する質量比が、約5:1から約10:1である、請求項19に記載の毛髪スタイリング組成物。
- 少なくとも1種の溶媒を更に含む、請求項1に記載の毛髪スタイリング組成物。
- 少なくとも2種のラテックスポリマーを含み、少なくとも1種のラテックスポリマーが皮膜形成ポリマーであり、
(1)(a)約0.1MPaから約10MPaの範囲のヤング率、及び0.5MPaの応力下で少なくとも約1%の歪みを有する少なくとも1種のポリマーA;
(b)約10MPaから約6GPaの範囲のヤング率、及び0.5MPaの応力下で約5%未満の歪みを有する少なくとも1種のポリマーB
を含む、前記水性分散体;
(2)少なくとも1種の溶媒;
を含み;
少なくとも2種のラテックスポリマーが、組成物の質量に対して、約10質量%未満の合わせた量で存在し;
少なくとも2種のラテックスポリマーが、約10:1から約1:10の範囲の質量比で組成物中に存在し;
前記組成物が、約0.05MPaから約5GPaの範囲のヤング率、及び0.5MPaの応力下で約300%までの範囲の歪みを有する皮膜を生成する、
毛髪スタイリング組成物。 - 少なくとも2種のラテックスポリマーを含む組成物を毛髪に適用する工程を含み、
少なくとも1種のラテックスポリマーが、皮膜形成ポリマーであり;
少なくとも2種のラテックスポリマーが、組成物の質量に対して、約0.1質量%から約30質量%の範囲の組合せ量で存在し;
少なくとも2種のラテックスポリマーが、約10:1から約1:10の範囲の質量比で組成物中に存在し;
前記組成物が、約0.05MPaから約5GPaの範囲のヤング率、及び0.5MPaの応力下で約300%までの範囲の歪みを有する皮膜を生成する、
毛髪のスタイリング方法。 - 前記組成物の適用前、適用中、又は適用後に、約25℃から約250℃の範囲の温度の熱で毛髪を処置する工程を更に含む、請求項23に記載の方法。
- 少なくとも2種のラテックスポリマーを含み、少なくとも1種のラテックスポリマーが皮膜形成ポリマーであり、
(1)(a)約0.1MPaから約10MPaの範囲のヤング率、及び0.5MPaの応力下で少なくとも約1%の歪みを有する少なくとも1種のポリマーA;
(b)約10MPaから約6GPaの範囲のヤング率、及び0.5MPaの応力下で約5%未満の歪みを有する少なくとも1種のポリマーB
を含む、前記水性分散体;
(2)少なくとも1種の溶媒;
を含み;
少なくとも2種のラテックスポリマーが、組成物の質量に対して、約10質量%未満の合わせた量で存在し;
少なくとも2種のラテックスポリマーが、約10:1から約1:10の範囲の質量比で組成物中に存在し;
前記組成物が、約0.05MPaから約5GPaの範囲のヤング率、及び0.5MPaの応力下で約300%までの範囲の歪みを有する皮膜を生成する、
組成物を毛髪に適用する工程を含む、毛髪のスタイリング方法。 - 前記組成物の適用前、適用中、又は適用後に、約25℃から約250℃の範囲の温度の熱で毛髪を処置する工程を更に含む、請求項25に記載の方法。
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JP6416896B2 (ja) | 2018-10-31 |
ES2902921T3 (es) | 2022-03-30 |
MX2015017044A (es) | 2016-04-21 |
US20200297616A1 (en) | 2020-09-24 |
CN105764484A (zh) | 2016-07-13 |
MX359170B (es) | 2018-09-18 |
US20150004117A1 (en) | 2015-01-01 |
US9884004B2 (en) | 2018-02-06 |
CN113230156A (zh) | 2021-08-10 |
BR112015032458B1 (pt) | 2020-12-01 |
US10973752B2 (en) | 2021-04-13 |
EP3035910A1 (en) | 2016-06-29 |
WO2014210117A1 (en) | 2014-12-31 |
US20180185266A1 (en) | 2018-07-05 |
EP3949941A1 (en) | 2022-02-09 |
US10709658B2 (en) | 2020-07-14 |
BR112015032458A2 (pt) | 2017-07-25 |
EP3035910A4 (en) | 2016-11-30 |
EP3035910B1 (en) | 2021-10-20 |
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