JP2015500807A - 塩素化アルカンの製造方法 - Google Patents
塩素化アルカンの製造方法 Download PDFInfo
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- JP2015500807A JP2015500807A JP2014544918A JP2014544918A JP2015500807A JP 2015500807 A JP2015500807 A JP 2015500807A JP 2014544918 A JP2014544918 A JP 2014544918A JP 2014544918 A JP2014544918 A JP 2014544918A JP 2015500807 A JP2015500807 A JP 2015500807A
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- JP
- Japan
- Prior art keywords
- alkane
- ppm
- alkene
- chloride
- chlorinated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
[1]
1つ又は複数の非金属ヨウ化物及び/又は10,000ppm未満の元素状ヨウ素並びに少なくとも1つのルイス酸を含む触媒システムで、少なくとも2個の塩素原子のアルカン及び/又はアルケンへの付加を触媒することを含む、塩素化アルカンの製造方法。
[2]
塩素原子の源が、塩素ガス、塩化スルフリル又はそれらの組み合わせを含む、項目1に記載の方法。
[3]
該ルイス酸が塩化アルミニウムを含む、項目1に記載の方法。
[4]
該元素状ヨウ素が、1ppm〜5000ppmの量で用いられる、項目1に記載の方法。
[5]
クロロカーボン溶媒の存在下で実施される、項目1に記載の方法。
[6]
該クロロカーボン溶媒が塩化メチレン又は1,2,3−トリクロロプロパンを含む、項目5に記載の方法。
[7]
該アルカン及び/又はアルケンが0〜4個の塩素原子を含む、項目1に記載の方法。
[8]
該アルカン及び/又はアルケンがトリクロロアルカン又はトリクロロアルケンである、項目7に記載の方法。
[9]
該アルカン又はアルケンが2〜6個の炭素原子を含む、項目1又は7に記載の方法。
[10]
該アルカン又はアルケンがプロパン又はプロペンを含む、項目9に記載の方法。
[11]
該塩素化アルカンが2〜6個の塩素原子を含む、項目1、5、又は7に記載の方法。
[12]
該塩素化アルカンがペンタクロロプロパンを含む、項目11に記載の方法。
[13]
該塩素化アルカンが1,1,2,2,3−ペンタクロロプロパンを含む、項目12に記載の方法。
[14]
該非金属ヨウ化物が、ヨードベンゼン、ペンタクロロヨードベンゼン、塩素化ヨードベンゼン、及びそれらの誘導体、塩化フェニルクロロヨードニウム及びその誘導体、ヨウ素化ポリマー、三ハロゲン化ヨウ素、又は任意の数のそれらの組み合わせを含む、項目1に記載の方法。
[15]
該非金属ヨウ化物がヨードベンゼンを含む、項目14に記載の方法。
Claims (15)
- 1つ又は複数の非金属ヨウ化物及び/又は10,000ppm未満の元素状ヨウ素並びに少なくとも1つのルイス酸を含む触媒システムで、少なくとも2個の塩素原子のアルカン及び/又はアルケンへの付加を触媒することを含む、塩素化アルカンの製造方法。
- 塩素原子の源が、塩素ガス、塩化スルフリル又はそれらの組み合わせを含む、請求項1に記載の方法。
- 該ルイス酸が塩化アルミニウムを含む、請求項1に記載の方法。
- 該元素状ヨウ素が、1ppm〜5000ppmの量で用いられる、請求項1に記載の方法。
- クロロカーボン溶媒の存在下で実施される、請求項1に記載の方法。
- 該クロロカーボン溶媒が塩化メチレン又は1,2,3−トリクロロプロパンを含む、請求項5に記載の方法。
- 該アルカン及び/又はアルケンが0〜4個の塩素原子を含む、請求項1に記載の方法。
- 該アルカン及び/又はアルケンがトリクロロアルカン又はトリクロロアルケンである、請求項7に記載の方法。
- 該アルカン又はアルケンが2〜6個の炭素原子を含む、請求項1又は7に記載の方法。
- 該アルカン又はアルケンがプロパン又はプロペンを含む、請求項9に記載の方法。
- 該塩素化アルカンが2〜6個の塩素原子を含む、請求項1、5、又は7に記載の方法。
- 該塩素化アルカンがペンタクロロプロパンを含む、請求項11に記載の方法。
- 該塩素化アルカンが1,1,2,2,3−ペンタクロロプロパンを含む、請求項12に記載の方法。
- 該非金属ヨウ化物が、ヨードベンゼン、ペンタクロロヨードベンゼン、塩素化ヨードベンゼン、及びそれらの誘導体、塩化フェニルクロロヨードニウム及びその誘導体、ヨウ素化ポリマー、三ハロゲン化ヨウ素、又は任意の数のそれらの組み合わせを含む、請求項1に記載の方法。
- 該非金属ヨウ化物がヨードベンゼンを含む、請求項14に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161566202P | 2011-12-02 | 2011-12-02 | |
US61/566,202 | 2011-12-02 | ||
PCT/US2012/067261 WO2013082404A1 (en) | 2011-12-02 | 2012-11-30 | Process for the production of chlorinated alkanes |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2015500807A true JP2015500807A (ja) | 2015-01-08 |
JP6059246B2 JP6059246B2 (ja) | 2017-01-11 |
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Application Number | Title | Priority Date | Filing Date |
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JP2014544918A Expired - Fee Related JP6059246B2 (ja) | 2011-12-02 | 2012-11-30 | 塩素化アルカンの製造方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US9199899B2 (ja) |
EP (1) | EP2785670B1 (ja) |
JP (1) | JP6059246B2 (ja) |
CN (1) | CN104024186B (ja) |
CA (1) | CA2856545A1 (ja) |
WO (1) | WO2013082404A1 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2015500239A (ja) * | 2011-12-02 | 2015-01-05 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2739595B1 (en) | 2011-08-07 | 2018-12-12 | Blue Cube IP LLC | Process for the production of chlorinated propenes |
JP6420145B2 (ja) | 2011-08-07 | 2018-11-07 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンの製造方法 |
CN104024186B (zh) | 2011-12-02 | 2016-10-12 | 蓝立方知识产权有限责任公司 | 生产氯化烷烃的方法 |
WO2013096706A1 (en) | 2011-12-23 | 2013-06-27 | Dow Global Technologies, Llc | Process for the production of alkenes and/or aromatic compounds |
EP2897930A1 (en) | 2012-09-20 | 2015-07-29 | Dow Global Technologies LLC | Process for the production of chlorinated propenes |
EP2897932A1 (en) | 2012-09-20 | 2015-07-29 | Dow Global Technologies LLC | Process for the production of chlorinated propenes |
CA2885329A1 (en) | 2012-09-30 | 2014-03-04 | Dow Global Technologies Llc | Weir quench and processes incorporating the same |
IN2015DN03949A (ja) | 2012-10-26 | 2015-10-02 | Dow Global Technologies Llc | |
CN104870411B (zh) | 2012-12-18 | 2018-10-02 | 蓝立方知识产权有限责任公司 | 用于生产氯化丙烯的方法 |
JP6251286B2 (ja) | 2012-12-19 | 2017-12-20 | ブルー キューブ アイピー エルエルシー | 塩素化プロペン生成のための方法 |
JP2016507590A (ja) | 2013-02-27 | 2016-03-10 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンを生成するための方法 |
EP2964597B1 (en) | 2013-03-09 | 2017-10-04 | Blue Cube IP LLC | Process for the production of chlorinated alkanes |
US8969259B2 (en) * | 2013-04-05 | 2015-03-03 | Reg Synthetic Fuels, Llc | Bio-based synthetic fluids |
CN106316880B (zh) * | 2015-06-15 | 2018-02-13 | 浙江工业大学 | 一种n‑二氯亚甲基苯胺类衍生物的合成方法 |
ES2874144T3 (es) | 2016-07-05 | 2021-11-04 | Occidental Chem Co | Fotocloración de cloroformo a tetracloruro de carbono |
US11780792B2 (en) | 2019-01-10 | 2023-10-10 | Occidental Chemical Corporation | Photochlorination of partially-chlorinated chloromethanes to carbon tetrachloride |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4051182A (en) * | 1976-04-12 | 1977-09-27 | Stauffer Chemical Company | Process for the manufacture of α-chloropropionyl chloride |
JP2014520099A (ja) * | 2011-05-31 | 2014-08-21 | ダウ グローバル テクノロジーズ エルエルシー | 塩素化プロペンの製造方法 |
JP2015500239A (ja) * | 2011-12-02 | 2015-01-05 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
JP2015501801A (ja) * | 2011-11-21 | 2015-01-19 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
Family Cites Families (216)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2630461A (en) | 1953-03-03 | Production of acetylene by incom | ||
US2119484A (en) | 1935-05-06 | 1938-05-31 | Du Pont | Chlorination of propylene dichloride |
GB471186A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorine derivatives of unsaturated hydrocarbons |
GB471188A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorinated hydrocarbons |
GB471187A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorinated hydrocarbons |
US2179378A (en) | 1936-07-18 | 1939-11-07 | Air Reduction | Production of acetylene |
US2207193A (en) | 1937-09-14 | 1940-07-09 | Shell Dev | Production of allyl type halides |
US2299441A (en) | 1939-09-02 | 1942-10-20 | Shell Dev | Catalytic halo-substitution of saturated organic compounds |
US2302228A (en) | 1940-04-02 | 1942-11-17 | Du Pont | Method of chlorination with sulphuryl chloride and production of monochloro-trimethyl acetic acid |
US2370342A (en) | 1940-04-30 | 1945-02-27 | Tide Water Associated Oil Comp | Halogenation |
US2378859A (en) | 1941-08-08 | 1945-06-19 | Distillers Co Yeast Ltd | Splitting-off of hydrogen halide from halogenated hydrocarbons |
US2449286A (en) | 1945-07-16 | 1948-09-14 | Shell Dev | Production of 1, 3-dihalopropylenes |
US2435983A (en) | 1945-12-01 | 1948-02-17 | Universal Oil Prod Co | Production of liquid hydrocarbons |
US2588867A (en) | 1948-10-25 | 1952-03-11 | Dow Chemical Co | Pyrolytic production of chlorohydrocarbons |
US2688592A (en) | 1950-10-21 | 1954-09-07 | Diamond Alkali Co | Photochemical process for preparing carbon tetrachloride |
DE857955C (de) | 1951-03-23 | 1952-12-04 | Basf Ag | Verfahren zur Herstellung von Tetrachloraethylen neben Tetrachlorkohlenstoff |
US2762611A (en) | 1952-02-28 | 1956-09-11 | Pfaudler Co Inc | Tubular heat exchangers |
US2765359A (en) | 1953-02-10 | 1956-10-02 | Hydrocarbon Research Inc | Production of acetylene |
GB857086A (en) | 1956-08-30 | 1960-12-29 | Hoechst Ag | Process for the manufacture of carbon tetrachloride |
US3000980A (en) | 1958-04-07 | 1961-09-19 | Dow Chemical Co | Preparation of alkyl bromides |
US2973393A (en) | 1958-10-02 | 1961-02-28 | Dow Chemical Co | Chlorination of acetylenes |
US2964579A (en) | 1958-10-09 | 1960-12-13 | Houdry Process Corp | Selective hydrogenation of diolefins with copper chromite catalyst |
US3094567A (en) | 1960-02-25 | 1963-06-18 | Monsanto Chemicals | Chlorination of propynes |
US3112988A (en) | 1960-02-26 | 1963-12-03 | Sheil Oil Company | Mixing gases at supersonic velocity |
US3819731A (en) | 1960-03-23 | 1974-06-25 | Stauffer Chemical Co | Production of chlorinated unsaturated hydrocarbons |
BE622939A (ja) | 1961-09-28 | |||
US3446859A (en) | 1962-06-11 | 1969-05-27 | Hooker Chemical Corp | Vapor phase condensation process |
US3502734A (en) | 1966-05-11 | 1970-03-24 | Du Pont | Process for partially chlorinating methyl chloride and/or methylene chloride |
CH473072A (fr) | 1966-06-07 | 1969-05-31 | El Paso Products Co | Procédé pour la préparation de dioléfines |
DE1568921A1 (de) | 1966-07-22 | 1970-03-26 | Knapsack Ag | Verfahren zur gemeinsamen Herstellung von 2,2,3- und 1,2,3-Trichlorbutan |
US3444263A (en) | 1966-11-09 | 1969-05-13 | Gulf Research Development Co | Method for converting ethylene to alpha olefins in the presence of an organic sulfide |
CH526333A (de) | 1967-05-19 | 1972-08-15 | Bayer Ag | Verfahren und Vorrichtung zur Durchführung von Reaktionen zwischen Gasen |
FR1546709A (fr) | 1967-10-10 | 1968-11-22 | Mini Ind Chimice | Procédé et appareil pour la fabrication en système continu de nitrosodérivés d'hydrocarbures |
DE1904426C3 (de) | 1969-01-30 | 1974-02-28 | Farbwerke Hoechst Ag, Vormals Meister Lucius & Bruening, 6000 Frankfurt | Verfahren zur Herstellung von Tetrachlorkohlenstoff aus Benzol und Chlor |
US3558438A (en) | 1968-10-30 | 1971-01-26 | Du Pont | Distillation process and apparatus |
US3551512A (en) | 1968-11-01 | 1970-12-29 | Diamond Shamrock Corp | Pressure process for preparing acetylene |
CA990738A (en) | 1971-07-30 | 1976-06-08 | Bruce E. Kurtz | Isothermal chlorination of methane, ethane and other compounds in a porous tube reactor |
US4513154A (en) | 1971-07-30 | 1985-04-23 | Allied Corporation | Process for consecutive competitive gas phase reaction |
US3920757A (en) | 1971-08-25 | 1975-11-18 | Dow Chemical Co | Chlorination with sulfuryl chloride |
NL160542C (nl) | 1971-12-17 | 1979-11-15 | Monsanto Co | Werkwijze voor het bereiden van 1,1,2,3,-tetrachloorpro- peen. |
US3823195A (en) | 1971-12-27 | 1974-07-09 | Monsanto Co | Preparation of 1,1,2,3-tetrachloropropene from 1,2,3-trichloropropane |
US3926758A (en) | 1971-12-27 | 1975-12-16 | Monsanto Co | Preparation of 1,1,2,3-tetrachloropropene from 2,3-trichloropropane |
DE2257005A1 (de) | 1972-11-21 | 1974-05-22 | Merck Patent Gmbh | Loesungsmittel fuer die kernresonanzspektroskopie |
CH609022A5 (en) | 1973-06-12 | 1979-02-15 | Monsanto Co | Process for the preparation of 1,2,3-trichloropropene from 1,2,3-trichloropropane |
NL7313098A (ja) | 1973-09-22 | 1974-03-25 | ||
US3872664A (en) | 1973-10-15 | 1975-03-25 | United Aircraft Corp | Swirl combustor with vortex burning and mixing |
US3914167A (en) | 1974-08-26 | 1975-10-21 | Dow Chemical Co | Process for making cis-1,3-dichloropropene |
US4038372A (en) | 1976-05-05 | 1977-07-26 | The United States Of America As Represented By The Secretary Of The Navy | Process for manufacturing chloramine |
US4319062A (en) | 1976-08-02 | 1982-03-09 | The Dow Chemical Company | Allyl chloride process |
US4046656A (en) | 1976-12-06 | 1977-09-06 | The Dow Chemical Company | Photochlorination process for methyl aromatic compounds |
JPS5479207U (ja) | 1977-11-14 | 1979-06-05 | ||
JPS5720859Y2 (ja) | 1978-03-14 | 1982-05-06 | ||
SU899523A1 (ru) | 1979-07-03 | 1982-01-23 | Уфимский Нефтяной Институт | Способ получени 1,1,2,3-тетрахлорпропена |
WO1983000859A1 (en) | 1981-09-01 | 1983-03-17 | George Andrew Olah | Methyl halides and methyl alcohol from methane |
US4650914A (en) | 1983-07-06 | 1987-03-17 | Monsanto Company | Process for producing 1,1,2,3-tetrachloropropene |
US4535194A (en) | 1983-07-06 | 1985-08-13 | Monsanto Co. | Process for producing 1,1,2,3-tetrachloropropene |
DE3415337A1 (de) | 1983-08-25 | 1985-03-14 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 3,3-dichlor-2-methyl-propen |
DE3415334A1 (de) | 1983-08-25 | 1985-03-14 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,1,2-trichlor-2-methyl-propan |
DE3415336A1 (de) | 1984-04-25 | 1985-10-31 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,2,3-trichlor-2-methyl-propan |
FR2569182B1 (fr) | 1984-08-20 | 1986-12-05 | Solvay | Procede pour effectuer des reactions de chloration substitutive de composes organiques au moyen de chlore moleculaire en presence d'un produit chlore servant d'initiateur radicalaire et initiateurs radicalaires utilises dans un tel procede |
DE3432720A1 (de) | 1984-09-06 | 1986-03-06 | Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,2,3-trichlorpropan |
US4614572A (en) | 1985-07-08 | 1986-09-30 | The Dow Chemical Company | Liquid phase chlorination of chlorinated methanes |
DE3681768D1 (de) | 1985-07-30 | 1991-11-07 | Hartmut Wolf | Zerstaeubungsvorrichtung. |
US4644907A (en) | 1985-11-29 | 1987-02-24 | Hunter Edward H | Boiler tubes of enhanced efficiency and method of producing same |
US4727181A (en) | 1986-04-21 | 1988-02-23 | The Dow Chemical Company | Process for the preparation of α-halocinnamate esters |
GB8708618D0 (en) | 1987-04-10 | 1987-05-13 | Ici Plc | Production process |
US5246903A (en) | 1987-05-26 | 1993-09-21 | The Dow Chemical Company | Process and catalyst for the dehydrohalogenation of halogenated hydrocarbons or alkylene halohydrins |
GB8721964D0 (en) | 1987-09-18 | 1987-10-28 | Shell Int Research | Multitube reactor |
US5171899A (en) | 1988-05-17 | 1992-12-15 | Daikin Industries Ltd. | Process for production of 1,1,1-trifluoro-2,2-dichloroethane |
JPH01290639A (ja) | 1988-05-17 | 1989-11-22 | Daikin Ind Ltd | 1,1,1−トリフルオロ−2,2−ジクロロエタンの製造法 |
US4999102A (en) | 1988-12-16 | 1991-03-12 | The Amalgamated Sugar Company | Liquid transfer manifold system for maintaining plug flow |
US5254771A (en) | 1989-07-14 | 1993-10-19 | Hoechst Aktiengesellschaft | Process for the preparation of 1,1,1-trifluoro-2-2-dichloroethane under elevated pressure |
US5057634A (en) | 1989-12-19 | 1991-10-15 | E. I. Du Pont De Nemours And Company | Multistep synthesis of hexafluoropropylene |
US5178844A (en) | 1990-04-03 | 1993-01-12 | Phillips Petroleum Company | Method and apparatus for producing nitride products |
DE4012007A1 (de) | 1990-04-13 | 1991-10-17 | Erdoelchemie Gmbh | Verfahren zur reduktiven dehydrohalogenierung von halogenkohlenwasserstoffen und halogenethern |
GB9105167D0 (en) | 1991-03-12 | 1991-04-24 | Ici Plc | Chemical process |
US5254788A (en) | 1991-09-10 | 1993-10-19 | Stone And Webster Engineering Corporation | Process for the production of olefins from light paraffins |
US5262575A (en) | 1992-08-04 | 1993-11-16 | The Dow Chemical Company | Production of allylic chlorides |
JP2813100B2 (ja) | 1992-10-23 | 1998-10-22 | 株式会社トクヤマ | アリルクロライドの製造方法および製造装置 |
GB9315450D0 (en) | 1993-07-26 | 1993-09-08 | Zeneca Ltd | Chlorination process |
US5414166A (en) | 1993-11-29 | 1995-05-09 | Korea Institute Of Science And Technology | Process for the preparation of 1,1,1-trifluoro-2,2-dichloroethane |
JPH08119885A (ja) | 1994-10-25 | 1996-05-14 | Central Glass Co Ltd | フッ素化炭化水素の製造方法 |
US5504266A (en) | 1995-05-24 | 1996-04-02 | The Dow Chemical Company | Process to make allyl chloride and reactor useful in that process |
US5616819A (en) | 1995-08-28 | 1997-04-01 | Laroche Industries Inc. | Process for preparing fluorinated aliphatic compounds |
US6235951B1 (en) | 1996-01-17 | 2001-05-22 | Central Glass Company, Limited | Method for producing 1,1,1,3,3-pentafluoropropane |
US5689020A (en) | 1996-03-11 | 1997-11-18 | Laroche Industries Inc. | High temperature chlorination process for the preparation of polychloroolefins |
US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
US6538167B1 (en) | 1996-10-02 | 2003-03-25 | Exxonmobil Chemical Patents Inc. | Process for producing light olefins |
US5986151A (en) | 1997-02-05 | 1999-11-16 | Alliedsignal Inc. | Fluorinated propenes from pentafluoropropane |
US5811605A (en) | 1997-02-19 | 1998-09-22 | Ppg Industries, Inc. | Preparation of 1,2,3,3-tetrachloropropene |
US5895825A (en) | 1997-12-01 | 1999-04-20 | Elf Atochem North America, Inc. | Preparation of 1,1,1,3,3-pentafluoropropane |
AU740959B2 (en) | 1997-12-18 | 2001-11-15 | Dow Chemical Company, The | A method for making glycol in an adiabatic reactor system |
JP3518321B2 (ja) | 1998-03-23 | 2004-04-12 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパンの製造方法 |
US6187976B1 (en) | 1998-04-09 | 2001-02-13 | Alliedsignal Inc. | Process for the preparation of fluorine containing hydrohalocarbons |
EP0999200B1 (en) | 1998-11-04 | 2002-07-17 | Rohm And Haas Company | Process for the high yield production of methyl methacrylate or methacrylic acid |
US6273180B1 (en) | 1998-12-23 | 2001-08-14 | L'air Liquide, Societe Anonyme Pour L'etude Et L'eploitation Des Procedes Georges Claude | Heat exchanger for preheating an oxidizing gas |
TW527218B (en) | 1999-03-16 | 2003-04-11 | Basf Ag | Multitube reactor, especially for catalytic gas-phase reactions |
EP1060788A1 (en) | 1999-06-15 | 2000-12-20 | Methanol Casale S.A. | Isothermal catalytic reactor for exothermic or endothermic heterogeneous reactions |
DE50011826D1 (de) | 1999-06-16 | 2006-01-12 | Solvay Fluor Gmbh | Uv-aktivierte chlorierung |
DE19952754A1 (de) | 1999-11-02 | 2001-05-10 | Krc Umwelttechnik Gmbh | Verfahren und Vorrichtung zur Kühlung und Reinigung von Vergasungsgasen |
JP3869170B2 (ja) | 1999-11-22 | 2007-01-17 | セントラル硝子株式会社 | 1,1,1,3,3−ペンタクロロプロパンの製造方法 |
HUP0204181A2 (en) | 1999-11-22 | 2003-05-28 | Dow Chemical Co | A process for the conversion of ethylene to vinyl chloride, and novel catalyst compositions useful for such process |
US6118018A (en) * | 1999-12-06 | 2000-09-12 | Occidental Chemical Corporation | Chlorination and bromination of aromatic compounds at atmospheric pressure |
JP2001213820A (ja) | 2000-01-31 | 2001-08-07 | Central Glass Co Ltd | 1,1,1,3,3−ペンタクロロプロパンの製造方法 |
US6613127B1 (en) | 2000-05-05 | 2003-09-02 | Dow Global Technologies Inc. | Quench apparatus and method for the reformation of organic materials |
DE10054840A1 (de) | 2000-11-04 | 2002-08-08 | Xcellsis Gmbh | Verfahren und Vorrichtung zum Starten eines Reaktors in einem Gaserzeugungssystem |
US6518467B2 (en) | 2000-12-29 | 2003-02-11 | Honeywell International Inc. | Method of making hydrofluorocarbons and hydrochlorofluorocarbons |
US6551469B1 (en) | 2001-11-27 | 2003-04-22 | Honeywell International | Photochlorination of 1,1,1,3,3-pentafluoropropane |
ES2719089T3 (es) | 2002-01-11 | 2019-07-08 | Mitsubishi Chem Corp | Uso de un reactor multitubular para la producción de (met)acroleína y/o ácido (met)acrílico |
US7117934B2 (en) | 2002-03-15 | 2006-10-10 | H2Gen Innovations, Inc. | Method and apparatus for minimizing adverse effects of thermal expansion in a heat exchange reactor |
US6924403B2 (en) | 2002-06-26 | 2005-08-02 | E. I. Du Pont De Nemours And Company | Synthesis of hexafluoropropylene |
US6683216B1 (en) | 2002-11-06 | 2004-01-27 | Eastman Chemical Company | Continuous process for the preparation of amines |
GB0301660D0 (en) | 2003-01-24 | 2003-02-26 | Redding John | Dredging scouring & excavation |
WO2004067164A1 (de) | 2003-01-31 | 2004-08-12 | Man Dwe Gmbh | Mantelrohrreaktor zur durchführung katalytischer gasphasenreaktionen und verfahren zum betreiben eines solchen |
ZA200506576B (en) | 2003-03-07 | 2006-12-27 | Dow Global Technologies Inc | Continuous process and system of producing polyether polyols |
WO2005005037A1 (ja) | 2003-07-14 | 2005-01-20 | Mitsubishi Rayon Co., Ltd. | 固定床多管式反応器 |
US7880040B2 (en) | 2004-04-29 | 2011-02-01 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US20060292046A1 (en) | 2003-07-31 | 2006-12-28 | Dow Global Technologies Inc. | Oxidation process and reactor with modified feed system |
MXPA06001255A (es) | 2003-07-31 | 2006-05-15 | Dow Global Technologies Inc | Proceso de oxidacion, y reactor con sistema de alimentacion modificado. |
US6825383B1 (en) | 2003-09-22 | 2004-11-30 | Council Of Scientific And Industrial Research | Catalytic process for regiospecific chlorination of alkanes, alkenes and arenes |
US7951982B2 (en) | 2004-04-29 | 2011-05-31 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
JP4864878B2 (ja) | 2004-04-29 | 2012-02-01 | ハネウェル・インターナショナル・インコーポレーテッド | 1,3,3,3−テトラフルオロプロペンの合成法 |
US8383867B2 (en) | 2004-04-29 | 2013-02-26 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
CN1972887B (zh) | 2004-04-29 | 2010-10-13 | 霍尼韦尔国际公司 | 1,3,3,3-四氟丙烯的合成方法 |
US7659434B2 (en) | 2004-04-29 | 2010-02-09 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7674939B2 (en) | 2004-04-29 | 2010-03-09 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US8058486B2 (en) | 2004-04-29 | 2011-11-15 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
MXPA06012466A (es) | 2004-04-29 | 2007-01-31 | Honeywell Int Inc | Procesos para la sintesis de 1,3,3,3-tetrafluoropropeno y 2,3,3,3-tetrafluoropropeno. |
US8084653B2 (en) | 2004-04-29 | 2011-12-27 | Honeywell International, Inc. | Method for producing fluorinated organic compounds |
US9102579B2 (en) | 2004-04-29 | 2015-08-11 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US20080021229A1 (en) | 2004-05-21 | 2008-01-24 | Maughon Bob R | Process for Preparing Epichlorhydrin from Ethane |
MY142153A (en) | 2004-12-10 | 2010-09-30 | Shell Int Research | Reactor tube apparatus |
US20070265368A1 (en) | 2004-12-22 | 2007-11-15 | Velliyur Nott Mallikarjuna Rao | Functionalized Copolymers of Terminally Functionalized Perfluoro (Alkyl Vinyl Ether) Reactor Wall for Photochemical Reactions, Process for Increasing Fluorine Content in Hydrocaebons and Halohydrocarbons and Olefin Production |
JP4501158B2 (ja) | 2005-03-30 | 2010-07-14 | 富士フイルム株式会社 | マイクロ化学装置の運転方法 |
US7396965B2 (en) | 2005-05-12 | 2008-07-08 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7511101B2 (en) | 2005-05-13 | 2009-03-31 | Fina Technology, Inc. | Plug flow reactor and polymers prepared therewith |
JP2007021396A (ja) | 2005-07-19 | 2007-02-01 | Japan Science & Technology Agency | 重金属の除去方法 |
WO2007018298A1 (en) | 2005-08-09 | 2007-02-15 | Canon Kabushiki Kaisha | Fluid-processing device and fluid-processing method |
DE102005044501A1 (de) | 2005-09-16 | 2007-03-22 | Roquette, Eberhard, Dipl.-Ing. | Veresterungsdüse |
US8071825B2 (en) | 2006-01-03 | 2011-12-06 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
WO2007079435A2 (en) | 2006-01-03 | 2007-07-12 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
EP1968922B1 (en) | 2006-01-03 | 2015-04-22 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
TWI324244B (en) | 2006-01-18 | 2010-05-01 | Lg Chemical Ltd | Shell-and-tube reactor or heat exchanger, method for producing an oxide by using the same, and method for increasing the heat transfer coefficient of first tubes of the same |
DE102007008876A1 (de) | 2006-02-21 | 2007-12-27 | Sachtleben Chemie Gmbh | Verfahren zur Durchführung chemischer und physikalischer Prozesse und Reaktionszelle |
EP2001828B1 (en) | 2006-03-31 | 2012-08-22 | E.I. Du Pont De Nemours And Company | Coproduction of hydrofluoroolefins |
US7836941B2 (en) | 2006-05-19 | 2010-11-23 | Exxonmobil Research And Engineering Company | Mitigation of in-tube fouling in heat exchangers using controlled mechanical vibration |
US20080073063A1 (en) | 2006-06-23 | 2008-03-27 | Exxonmobil Research And Engineering Company | Reduction of fouling in heat exchangers |
FR2902785B1 (fr) | 2006-06-26 | 2008-08-08 | Solvay | Procede de fabrication de 1,2-dichloroethane |
JP2008063314A (ja) | 2006-09-04 | 2008-03-21 | Tokyo Kasei Kogyo Kk | 環境調和型超原子価ヨウ素試剤 |
US8232435B2 (en) | 2006-09-05 | 2012-07-31 | E I Du Pont De Nemours And Company | 1,2,3,3,3-pentafluoropropene production processes |
US20090088547A1 (en) | 2006-10-17 | 2009-04-02 | Rpo Pty Limited | Process for producing polysiloxanes and use of the same |
EP2091897B2 (en) | 2006-10-31 | 2021-12-01 | The Chemours Company FC, LLC | Processes for the production of fluoropropanes and halopropenes |
US20080207962A1 (en) | 2007-02-23 | 2008-08-28 | Velliyur Nott Mallikarjuna Rao | Compositions containing chromium, oxygen, and at least two modifier metals selected the group consisting of gold, silver, and palladium, their preparation, and their use as catalysts and catalyst precursors |
EP2135888A4 (en) | 2007-04-10 | 2014-10-01 | Asahi Glass Co Ltd | COMPOUND CATALYST OF METAL CYANIDE COMPLEX WITH ORGANIC LIGAND, METHOD OF MANUFACTURING THEREOF, AND METHOD FOR PRODUCING POLYETHEREPOLYOLE |
JP2009000592A (ja) | 2007-06-19 | 2009-01-08 | Hitachi Ltd | 反応器および反応システム |
US8076521B2 (en) | 2007-06-27 | 2011-12-13 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
EP2158176A4 (en) | 2007-06-27 | 2011-11-09 | Arkema Inc | TWO-STAGE PROCESS FOR THE PREPARATION OF HYDROFLUOROLEFINES |
US20090018377A1 (en) | 2007-07-09 | 2009-01-15 | Boyce C Bradford | Catalytic process for the preparation of fluorinated halocarbons |
JP5339229B2 (ja) | 2007-07-24 | 2013-11-13 | ナガセケムテックス株式会社 | 超原子価ヨウ素反応剤を用いる芳香族化合物および複素環式芳香族化合物のポリマーの製造方法 |
US8258355B2 (en) | 2007-07-25 | 2012-09-04 | Honeywell International Inc. | Processes for preparing 1,1,2,3-tetrachloropropene |
US9035111B2 (en) | 2007-08-22 | 2015-05-19 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
TWI467001B (zh) | 2007-09-18 | 2015-01-01 | Thyssenkrupp Uhde Gmbh | 氣化反應器及夾帶流氣化的方法 |
CN101918357B (zh) | 2007-10-04 | 2014-07-16 | 卡萨尔尿素公司 | 尿素制备方法及设备 |
US9079818B2 (en) | 2007-10-15 | 2015-07-14 | Honeywell International Inc. | Process for synthesis of fluorinated olefins |
WO2009061954A1 (en) | 2007-11-06 | 2009-05-14 | Quantumsphere, Inc. | System and method for ammonia synthesis |
KR20100099182A (ko) | 2007-11-20 | 2010-09-10 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 하이드로플루오로알칸올 및 하이드로플루오로알켄의 합성 |
CA2708643C (en) | 2007-12-19 | 2017-05-30 | Occidental Chemical Corporation | Methods of making chlorinated hydrocarbons |
GB0800470D0 (en) | 2008-01-11 | 2008-02-20 | Redding John | Improvements in or relating to jet nozzles |
CN101215220A (zh) | 2008-01-16 | 2008-07-09 | 西安近代化学研究所 | 1,1,1,3-四氟丙烯的制备方法 |
CN101597209A (zh) | 2008-03-20 | 2009-12-09 | 霍尼韦尔国际公司 | 用于制备2,3,3,3-四氟丙烯的一体式方法 |
US8071826B2 (en) | 2008-04-04 | 2011-12-06 | Honeywell International Inc. | Process for the preparation of 2,3,3,3-tetrafluoropropene (HFO-1234yf) |
CN102119145B (zh) | 2008-08-07 | 2014-06-18 | 巴斯夫欧洲公司 | 制备芳香族异氰酸酯的方法 |
CN102164881B (zh) | 2008-09-25 | 2015-05-27 | 中央硝子株式会社 | 1,3,3,3-四氟丙烯的制造方法 |
JP6022770B2 (ja) | 2008-10-13 | 2016-11-09 | ブルー キューブ アイピー エルエルシー | 塩素化及び/又はフッ素化プロペンの製造方法 |
US8642818B2 (en) | 2008-11-19 | 2014-02-04 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
JP5582036B2 (ja) | 2008-12-25 | 2014-09-03 | 旭硝子株式会社 | 1,1−ジクロロ−2,3,3,3−テトラフルオロプロペンおよび2,3,3,3−テトラフルオロプロペンの製造方法 |
CN101492341B (zh) | 2009-03-05 | 2012-03-28 | 杨海珍 | 饱和多氯代烷烃的制备方法 |
KR101374000B1 (ko) | 2009-04-23 | 2014-03-12 | 다이킨 고교 가부시키가이샤 | 2,3,3,3-테트라플루오로프로펜의 제조 방법 |
CN101544535B (zh) | 2009-05-01 | 2012-07-18 | 浙江三美化工股份有限公司 | 一种合成1,1,1,3,3-五氯丙烷的制备方法 |
JP5459320B2 (ja) | 2009-05-13 | 2014-04-02 | ダイキン工業株式会社 | 塩素含有フルオロカーボン化合物の製造方法 |
US8581011B2 (en) | 2009-10-09 | 2013-11-12 | Dow Global Technologies, Llc | Process for the production of chlorinated and/or fluorinated propenes |
JP5782038B2 (ja) | 2009-10-09 | 2015-09-24 | ダウ グローバル テクノロジーズ エルエルシー | 等温多管式反応器及び該反応器を組み込んだプロセス |
CN102686544B (zh) | 2009-10-09 | 2017-02-15 | 蓝立方知识产权公司 | 用于生产氯化和/或氟化丙烯和高级烯烃的方法 |
JP5947214B2 (ja) | 2009-10-09 | 2016-07-06 | ブルー キューブ アイピー エルエルシー | 断熱栓流反応器及び該断熱栓流反応器を組み込んだプロセス |
CN102639475A (zh) | 2009-11-16 | 2012-08-15 | 阿科玛股份有限公司 | 纯化和稳定化氯烯烃的方法 |
JP5532131B2 (ja) | 2009-11-27 | 2014-06-25 | ダイキン工業株式会社 | 1,1,2,3−テトラクロロプロペンの製造方法 |
WO2011077191A1 (en) | 2009-12-23 | 2011-06-30 | Arkema France | Catalytic gas phase fluorination of 1230xa to 1234yf |
JP2011144148A (ja) | 2010-01-18 | 2011-07-28 | Nippon Zeon Co Ltd | 含水素ハロゲン化シクロペンタン、及びヘプタフルオロシクロペンテンの製造方法 |
CN101955414A (zh) | 2010-04-20 | 2011-01-26 | 南通泰禾化工有限公司 | 1,1,2,3-四氯丙烯生产工艺 |
DE102010022414A1 (de) | 2010-06-01 | 2011-12-01 | Günther Kramb jun. | Emulgiervorrichtung |
RS59777B1 (sr) | 2010-07-21 | 2020-02-28 | Otkrytoe Aktsionernoe Obschestvo Res & Design Institute Of Urea And Organic Synthesis Products Oao N | Reaktori gas-tečnost sa komorom sa vrtložnim mešanjem |
CN101913979A (zh) | 2010-09-07 | 2010-12-15 | 西安近代化学研究所 | 1,1,1,3,3-五氯丁烷的生产方法 |
CN101913980A (zh) | 2010-09-07 | 2010-12-15 | 西安近代化学研究所 | 1,1,1,3,3-五氯丙烷的生产方法 |
CN101982227B (zh) | 2010-09-15 | 2013-03-20 | 山东东岳高分子材料有限公司 | 一种用于高温裂解的气体快速混合反应装置及应用 |
CN102001911B (zh) | 2010-09-20 | 2013-09-25 | 西安近代化学研究所 | 2,3,3,3-四氟丙烯的制备方法 |
WO2012081482A1 (ja) | 2010-12-16 | 2012-06-21 | 株式会社トクヤマ | 炭素数3の塩素化炭化水素の製造方法 |
CN102249846B (zh) | 2011-05-31 | 2013-05-08 | 浙江师范大学 | 一种2-氯-3, 3, 3-三氟丙烯和2, 3-二氯-1, 1-二氟丙烯的联产制备方法 |
WO2012166394A1 (en) | 2011-05-31 | 2012-12-06 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
EP2739595B1 (en) | 2011-08-07 | 2018-12-12 | Blue Cube IP LLC | Process for the production of chlorinated propenes |
JP6420145B2 (ja) | 2011-08-07 | 2018-11-07 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンの製造方法 |
CN102351637B (zh) | 2011-08-31 | 2013-10-23 | 浙江师范大学 | 一种2, 3, 3, 3-四氟丙烯的制备方法 |
CN104024186B (zh) | 2011-12-02 | 2016-10-12 | 蓝立方知识产权有限责任公司 | 生产氯化烷烃的方法 |
US9334205B2 (en) | 2011-12-13 | 2016-05-10 | Blue Cube Ip Llc | Process for the production of chlorinated propanes and propenes |
WO2013096311A1 (en) | 2011-12-22 | 2013-06-27 | Dow Global Technologies, Llc | Process for the production of tetrachloromethane |
WO2013096706A1 (en) | 2011-12-23 | 2013-06-27 | Dow Global Technologies, Llc | Process for the production of alkenes and/or aromatic compounds |
CA2858836A1 (en) | 2011-12-23 | 2013-06-27 | Dow Global Technologies Llc | Sulfuryl chloride as chlorinating agent |
JP5871633B2 (ja) | 2012-01-24 | 2016-03-01 | 関東電化工業株式会社 | ビス(1,1−ジクロロ−3,3,3−トリフルオロプロピル)エーテルおよびその製造方法 |
EP2897930A1 (en) | 2012-09-20 | 2015-07-29 | Dow Global Technologies LLC | Process for the production of chlorinated propenes |
EP2897932A1 (en) | 2012-09-20 | 2015-07-29 | Dow Global Technologies LLC | Process for the production of chlorinated propenes |
CA2885329A1 (en) | 2012-09-30 | 2014-03-04 | Dow Global Technologies Llc | Weir quench and processes incorporating the same |
IN2015DN03949A (ja) | 2012-10-26 | 2015-10-02 | Dow Global Technologies Llc | |
CN104870411B (zh) | 2012-12-18 | 2018-10-02 | 蓝立方知识产权有限责任公司 | 用于生产氯化丙烯的方法 |
JP6251286B2 (ja) | 2012-12-19 | 2017-12-20 | ブルー キューブ アイピー エルエルシー | 塩素化プロペン生成のための方法 |
JP2016507590A (ja) | 2013-02-27 | 2016-03-10 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンを生成するための方法 |
CA2901895A1 (en) | 2013-02-28 | 2014-09-04 | Blue Cube Ip Llc | Process for the production of chlorinated propanes |
EP2964597B1 (en) | 2013-03-09 | 2017-10-04 | Blue Cube IP LLC | Process for the production of chlorinated alkanes |
-
2012
- 2012-11-30 CN CN201280058855.9A patent/CN104024186B/zh not_active Expired - Fee Related
- 2012-11-30 JP JP2014544918A patent/JP6059246B2/ja not_active Expired - Fee Related
- 2012-11-30 US US14/362,249 patent/US9199899B2/en not_active Expired - Fee Related
- 2012-11-30 EP EP12798572.9A patent/EP2785670B1/en not_active Not-in-force
- 2012-11-30 WO PCT/US2012/067261 patent/WO2013082404A1/en active Application Filing
- 2012-11-30 CA CA2856545A patent/CA2856545A1/en not_active Abandoned
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4051182A (en) * | 1976-04-12 | 1977-09-27 | Stauffer Chemical Company | Process for the manufacture of α-chloropropionyl chloride |
JP2014520099A (ja) * | 2011-05-31 | 2014-08-21 | ダウ グローバル テクノロジーズ エルエルシー | 塩素化プロペンの製造方法 |
JP2015501801A (ja) * | 2011-11-21 | 2015-01-19 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
JP2015500239A (ja) * | 2011-12-02 | 2015-01-05 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2015500239A (ja) * | 2011-12-02 | 2015-01-05 | ダウ グローバル テクノロジーズ エルエルシー | クロロアルカンの製造方法 |
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WO2013082404A1 (en) | 2013-06-06 |
JP6059246B2 (ja) | 2017-01-11 |
CN104024186B (zh) | 2016-10-12 |
EP2785670A1 (en) | 2014-10-08 |
CA2856545A1 (en) | 2013-06-06 |
CN104024186A (zh) | 2014-09-03 |
US20140323775A1 (en) | 2014-10-30 |
EP2785670B1 (en) | 2017-10-25 |
US9199899B2 (en) | 2015-12-01 |
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