JP2013509703A - エッチング液組成物 - Google Patents
エッチング液組成物 Download PDFInfo
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- JP2013509703A JP2013509703A JP2012536673A JP2012536673A JP2013509703A JP 2013509703 A JP2013509703 A JP 2013509703A JP 2012536673 A JP2012536673 A JP 2012536673A JP 2012536673 A JP2012536673 A JP 2012536673A JP 2013509703 A JP2013509703 A JP 2013509703A
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- 238000005530 etching Methods 0.000 title claims abstract description 82
- 239000000203 mixture Substances 0.000 title claims abstract description 62
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 37
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 31
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052738 indium Inorganic materials 0.000 claims abstract description 14
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000011737 fluorine Substances 0.000 claims abstract description 10
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 10
- 150000001875 compounds Chemical class 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 7
- 239000010452 phosphate Substances 0.000 claims abstract description 7
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 5
- 239000010408 film Substances 0.000 claims description 94
- 229910052751 metal Inorganic materials 0.000 claims description 34
- 239000002184 metal Substances 0.000 claims description 34
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 19
- 239000011733 molybdenum Substances 0.000 claims description 19
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 18
- 239000000758 substrate Substances 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 11
- 229910000838 Al alloy Inorganic materials 0.000 claims description 9
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 229910052759 nickel Inorganic materials 0.000 claims description 6
- 229910052779 Neodymium Inorganic materials 0.000 claims description 5
- 229910045601 alloy Inorganic materials 0.000 claims description 5
- 239000000956 alloy Substances 0.000 claims description 5
- 229910052804 chromium Inorganic materials 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 229910052749 magnesium Inorganic materials 0.000 claims description 5
- 229910052758 niobium Inorganic materials 0.000 claims description 5
- 229910052710 silicon Inorganic materials 0.000 claims description 5
- 229910052712 strontium Inorganic materials 0.000 claims description 5
- 229910052715 tantalum Inorganic materials 0.000 claims description 5
- 229910052718 tin Inorganic materials 0.000 claims description 5
- 229910052721 tungsten Inorganic materials 0.000 claims description 5
- 229910052725 zinc Inorganic materials 0.000 claims description 5
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 4
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 3
- 239000010409 thin film Substances 0.000 claims description 3
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 claims description 2
- MIMUSZHMZBJBPO-UHFFFAOYSA-N 6-methoxy-8-nitroquinoline Chemical compound N1=CC=CC2=CC(OC)=CC([N+]([O-])=O)=C21 MIMUSZHMZBJBPO-UHFFFAOYSA-N 0.000 claims description 2
- 239000004254 Ammonium phosphate Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 229910000148 ammonium phosphate Inorganic materials 0.000 claims description 2
- 235000019289 ammonium phosphates Nutrition 0.000 claims description 2
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 2
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 2
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 2
- QVLTXCYWHPZMCA-UHFFFAOYSA-N po4-po4 Chemical compound OP(O)(O)=O.OP(O)(O)=O QVLTXCYWHPZMCA-UHFFFAOYSA-N 0.000 claims description 2
- 235000013024 sodium fluoride Nutrition 0.000 claims description 2
- 239000011775 sodium fluoride Substances 0.000 claims description 2
- BFXAWOHHDUIALU-UHFFFAOYSA-M sodium;hydron;difluoride Chemical compound F.[F-].[Na+] BFXAWOHHDUIALU-UHFFFAOYSA-M 0.000 claims description 2
- 230000000052 comparative effect Effects 0.000 description 14
- 229920002120 photoresistant polymer Polymers 0.000 description 7
- 229910020794 La-Ni Inorganic materials 0.000 description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 5
- 230000003139 buffering effect Effects 0.000 description 3
- AMGQUBHHOARCQH-UHFFFAOYSA-N indium;oxotin Chemical compound [In].[Sn]=O AMGQUBHHOARCQH-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- -1 fluorine ions Chemical class 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
- 229910000316 alkaline earth metal phosphate Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000001312 dry etching Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 238000001020 plasma etching Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000001039 wet etching Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K13/00—Etching, surface-brightening or pickling compositions
- C09K13/04—Etching, surface-brightening or pickling compositions containing an inorganic acid
- C09K13/08—Etching, surface-brightening or pickling compositions containing an inorganic acid containing a fluorine compound
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
- C23F1/20—Acidic compositions for etching aluminium or alloys thereof
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/135—Liquid crystal cells structurally associated with a photoconducting or a ferro-electric layer, the properties of which can be optically or electrically varied
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/30—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
- H01L21/302—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
- H01L21/306—Chemical or electrical treatment, e.g. electrolytic etching
- H01L21/30604—Chemical etching
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K3/00—Apparatus or processes for manufacturing printed circuits
- H05K3/02—Apparatus or processes for manufacturing printed circuits in which the conductive material is applied to the surface of the insulating support and is thereafter removed from such areas of the surface which are not intended for current conducting or shielding
- H05K3/06—Apparatus or processes for manufacturing printed circuits in which the conductive material is applied to the surface of the insulating support and is thereafter removed from such areas of the surface which are not intended for current conducting or shielding the conductive material being removed chemically or electrolytically, e.g. by photo-etch process
- H05K3/067—Etchants
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Nonlinear Science (AREA)
- General Physics & Mathematics (AREA)
- Weting (AREA)
- Power Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Mathematical Physics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Optics & Photonics (AREA)
- Computer Hardware Design (AREA)
- ing And Chemical Polishing (AREA)
- Internal Circuitry In Semiconductor Integrated Circuit Devices (AREA)
- Liquid Crystal (AREA)
- Devices For Indicating Variable Information By Combining Individual Elements (AREA)
Abstract
Description
下記表1に記載された成分及び組成比でエッチング液組成物が180kgとなるように、実施例1〜実施例5及び比較例1〜比較例3の組成物を製造した。
ガラス上にITO/Al−La−Ni/Moからなる三重膜が蒸着され、一定の形状にフォトレジストがパターニングされた基板を用いた。噴射式エッチング方式の実験装置(モデル:ETCHER(TFT)、SEMES社製)内に前記実施例1〜5及び比較例1〜3のエッチング液組成物を入れ、温度を40℃にセットして加温した。その後、温度が40±0.1℃に到逹した後、エッチング工程を行った。総エッチング時間をEPDを基準として60%を与えて実施した。試片を入れて噴射を始め、エッチングが完了すれば、取り出して脱イオン水で洗浄した後、熱風乾燥装置を用いて乾燥し、フォトレジスト(PR)剥離器(stripper)でフォトレジストをとり除いた。洗浄及び乾燥の後、電子走査顕微鏡(SEM)(モデル:S−4700、HITACHI社製)を用いて、エッチングプロファイルの傾斜角、サイドエッチ(CD(critical dimension))損失、エッチング残留物及び下部膜の損傷を評価し、その結果を表2及び図1〜6に示した。
Claims (10)
- 組成物の総重量に対し、45〜70重量%のリン酸、2〜10重量%の硝酸、5〜25重量%の酢酸、0.01〜3重量%の含フッ素化合物、0.1〜5重量%のリン酸塩、及び残量の水を含むことを特徴とする、ITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 前記含フッ素化合物は、フッ化アンモニウム、フッ化ナトリウム、フッ化リン酸、重フッ化アンモニウム、重フッ化ナトリウム、及び重フッ化リン酸からなる群から選ばれる1種又は2種以上であることを特徴とする、請求項1に記載のITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 前記リン酸塩は、リン酸アンモニウム及びリン酸二水素カリウムからなる群から選ばれる1種又は2種以上であることを特徴とする、請求項1に記載のITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 前記ITO、Al及びMoを含む三重膜は、ITO膜、アルミニウムを含む金属膜、及びモリブデンを含む金属膜からなる三重膜であることを特徴とする、請求項1に記載のITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 前記アルミニウムを含む金属膜は、アルミニウム膜又はアルミニウム合金膜であることを特徴とする、請求項4に記載のITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 前記アルミニウム合金膜は、Al−La−X合金からなり、XはMg、Zn、In、Ca、Te、Sr、Cr、Co、Mo、Nb、Ta、W、Ni、Nd、Sn、Fe、Si、Mo、Pt及びCからなる群から選ばれる1種又は2種以上であることを特徴とする、請求項5に記載のITO、Al及びMoを含む三重膜用のエッチング液組成物。
- 請求項1に記載のエッチング液組成物を用いて、前記ITO、Al及びMoを含む三重膜をエッチングする工程を含むことを特徴とする、フラットパネル表示装置用アレイ基板の製造方法。
- 前記フラットパネル表示装置用アレイ基板は、薄膜トランジスタアレイ基板であることを特徴とする、請求項7に記載のフラットパネル表示装置用アレイ基板の製造方法。
- 請求項1に記載のエッチング液組成物を用いて形成された画素電極、ソース/ドレイン電極、及び緩衝膜を含むことを特徴とする、フラットパネル表示装置用アレイ基板。
- 薄膜トランジスタアレイ基板であることを特徴とする、請求項9に記載のフラットパネル表示装置用アレイ基板。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR20090104418 | 2009-10-30 | ||
KR10-2009-0104418 | 2009-10-30 | ||
KR1020100104831A KR101805187B1 (ko) | 2009-10-30 | 2010-10-26 | 식각액 조성물 |
KR10-2010-0104831 | 2010-10-26 | ||
PCT/KR2010/007417 WO2011052989A2 (ko) | 2009-10-30 | 2010-10-27 | 식각액 조성물 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2013509703A true JP2013509703A (ja) | 2013-03-14 |
JP5753180B2 JP5753180B2 (ja) | 2015-07-22 |
Family
ID=43922822
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012536673A Active JP5753180B2 (ja) | 2009-10-30 | 2010-10-27 | エッチング液組成物 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP5753180B2 (ja) |
KR (1) | KR101805187B1 (ja) |
CN (1) | CN102597162B (ja) |
WO (1) | WO2011052989A2 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2016025321A (ja) * | 2014-07-24 | 2016-02-08 | 関東化學株式会社 | エッチング液組成物およびエッチング方法 |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101361839B1 (ko) * | 2011-10-27 | 2014-02-11 | 한국항공대학교산학협력단 | 식각액 조성물, 및 다중금속막 식각 방법 |
KR101394469B1 (ko) * | 2012-07-20 | 2014-05-13 | 한국항공대학교산학협력단 | 식각액 조성물, 및 다중금속막 식각 방법 |
KR101404511B1 (ko) * | 2012-07-24 | 2014-06-09 | 플란제 에스이 | 식각액 조성물, 및 다중금속막 식각 방법 |
KR102091541B1 (ko) * | 2014-02-25 | 2020-03-20 | 동우 화인켐 주식회사 | 유기 발광 표시 장치의 제조 방법 |
KR102254561B1 (ko) * | 2014-09-30 | 2021-05-21 | 동우 화인켐 주식회사 | 은 나노 와이어의 식각액 조성물 |
CN105463463B (zh) * | 2015-11-25 | 2018-04-24 | 江阴江化微电子材料股份有限公司 | 一种AMOLED用ITO-Ag-ITO蚀刻液 |
KR102384563B1 (ko) * | 2016-03-24 | 2022-04-08 | 동우 화인켐 주식회사 | 인듐 산화막용 식각 조성물 |
CN107620066A (zh) * | 2017-09-14 | 2018-01-23 | 合肥惠科金扬科技有限公司 | 一种显示屏用酸性蚀刻液 |
CN109439329A (zh) * | 2018-10-29 | 2019-03-08 | 苏州博洋化学股份有限公司 | 平板显示阵列制程用新型igzo蚀刻液 |
CN110195229B (zh) * | 2019-06-21 | 2021-05-14 | 湖北兴福电子材料有限公司 | 一种钨和氮化钛金属薄膜的蚀刻液及其使用方法 |
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KR100444345B1 (ko) * | 2002-03-28 | 2004-08-16 | 테크노세미켐 주식회사 | 평판디스플레이의 박막트랜지스터 형성을 위한 금속전극용식각액 조성물 |
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JP2016025321A (ja) * | 2014-07-24 | 2016-02-08 | 関東化學株式会社 | エッチング液組成物およびエッチング方法 |
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CN102597162A (zh) | 2012-07-18 |
KR101805187B1 (ko) | 2017-12-06 |
WO2011052989A2 (ko) | 2011-05-05 |
KR20110047983A (ko) | 2011-05-09 |
WO2011052989A3 (ko) | 2011-09-15 |
JP5753180B2 (ja) | 2015-07-22 |
CN102597162B (zh) | 2014-10-01 |
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