JP2012512319A - 洗浄組成物及び方法 - Google Patents
洗浄組成物及び方法 Download PDFInfo
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- JP2012512319A JP2012512319A JP2011542454A JP2011542454A JP2012512319A JP 2012512319 A JP2012512319 A JP 2012512319A JP 2011542454 A JP2011542454 A JP 2011542454A JP 2011542454 A JP2011542454 A JP 2011542454A JP 2012512319 A JP2012512319 A JP 2012512319A
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- surfactant
- solvent
- olefin
- alkyl
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- 239000000203 mixture Substances 0.000 title claims abstract description 108
- 238000000034 method Methods 0.000 title claims description 17
- 238000004140 cleaning Methods 0.000 title abstract description 5
- 239000004094 surface-active agent Substances 0.000 claims abstract description 98
- 239000002904 solvent Substances 0.000 claims abstract description 69
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000005108 dry cleaning Methods 0.000 claims abstract description 14
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 8
- -1 C 1 -C 5 fluoroalkyl Chemical group 0.000 claims description 20
- 125000000217 alkyl group Chemical group 0.000 claims description 18
- 239000000758 substrate Substances 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 15
- 239000004744 fabric Substances 0.000 claims description 14
- 229910052731 fluorine Inorganic materials 0.000 claims description 14
- 229910019142 PO4 Inorganic materials 0.000 claims description 13
- 125000003709 fluoroalkyl group Chemical group 0.000 claims description 13
- 239000010452 phosphate Substances 0.000 claims description 13
- 125000003118 aryl group Chemical group 0.000 claims description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- 150000003839 salts Chemical class 0.000 claims description 11
- 239000002689 soil Substances 0.000 claims description 11
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 9
- 125000002877 alkyl aryl group Chemical group 0.000 claims description 9
- 229910052801 chlorine Inorganic materials 0.000 claims description 9
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 claims description 8
- 239000001257 hydrogen Substances 0.000 claims description 8
- 239000011737 fluorine Substances 0.000 claims description 6
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 5
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims description 5
- 125000006182 dimethyl benzyl group Chemical group 0.000 claims description 4
- 230000002209 hydrophobic effect Effects 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 3
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 125000004407 fluoroaryl group Chemical group 0.000 claims description 2
- 150000002431 hydrogen Chemical class 0.000 claims 3
- XXBDWLFCJWSEKW-UHFFFAOYSA-N dimethylbenzylamine Chemical class CN(C)CC1=CC=CC=C1 XXBDWLFCJWSEKW-UHFFFAOYSA-N 0.000 claims 1
- BAVYZALUXZFZLV-UHFFFAOYSA-N mono-methylamine Natural products NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 claims 1
- 230000003373 anti-fouling effect Effects 0.000 abstract description 4
- 239000002563 ionic surfactant Substances 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 23
- 150000001875 compounds Chemical class 0.000 description 12
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical group FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 10
- CDOOAUSHHFGWSA-OWOJBTEDSA-N (e)-1,3,3,3-tetrafluoroprop-1-ene Chemical compound F\C=C\C(F)(F)F CDOOAUSHHFGWSA-OWOJBTEDSA-N 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 125000005842 heteroatom Chemical group 0.000 description 8
- 238000009835 boiling Methods 0.000 description 7
- 125000002091 cationic group Chemical group 0.000 description 7
- 239000000460 chlorine Substances 0.000 description 7
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 description 6
- 238000006073 displacement reaction Methods 0.000 description 5
- 125000001153 fluoro group Chemical group F* 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- CDOOAUSHHFGWSA-UPHRSURJSA-N (z)-1,3,3,3-tetrafluoroprop-1-ene Chemical compound F\C=C/C(F)(F)F CDOOAUSHHFGWSA-UPHRSURJSA-N 0.000 description 3
- NDMMKOCNFSTXRU-UHFFFAOYSA-N 1,1,2,3,3-pentafluoroprop-1-ene Chemical compound FC(F)C(F)=C(F)F NDMMKOCNFSTXRU-UHFFFAOYSA-N 0.000 description 3
- PGJHURKAWUJHLJ-UHFFFAOYSA-N 1,1,2,3-tetrafluoroprop-1-ene Chemical compound FCC(F)=C(F)F PGJHURKAWUJHLJ-UHFFFAOYSA-N 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- ZVQOOHYFBIDMTQ-UHFFFAOYSA-N [methyl(oxido){1-[6-(trifluoromethyl)pyridin-3-yl]ethyl}-lambda(6)-sulfanylidene]cyanamide Chemical compound N#CN=S(C)(=O)C(C)C1=CC=C(C(F)(F)F)N=C1 ZVQOOHYFBIDMTQ-UHFFFAOYSA-N 0.000 description 3
- 150000001336 alkenes Chemical class 0.000 description 3
- 125000000129 anionic group Chemical group 0.000 description 3
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 125000004122 cyclic group Chemical group 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- AJDIZQLSFPQPEY-UHFFFAOYSA-N 1,1,2-Trichlorotrifluoroethane Chemical compound FC(F)(Cl)C(F)(Cl)Cl AJDIZQLSFPQPEY-UHFFFAOYSA-N 0.000 description 2
- DMUPYMORYHFFCT-UHFFFAOYSA-N 1,2,3,3,3-pentafluoroprop-1-ene Chemical compound FC=C(F)C(F)(F)F DMUPYMORYHFFCT-UHFFFAOYSA-N 0.000 description 2
- CDOOAUSHHFGWSA-UHFFFAOYSA-N 1,3,3,3-tetrafluoropropene Chemical compound FC=CC(F)(F)F CDOOAUSHHFGWSA-UHFFFAOYSA-N 0.000 description 2
- LDTMPQQAWUMPKS-UHFFFAOYSA-N 1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C=CCl LDTMPQQAWUMPKS-UHFFFAOYSA-N 0.000 description 2
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical compound FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 description 2
- 229910000619 316 stainless steel Inorganic materials 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000443 aerosol Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 125000000753 cycloalkyl group Chemical group 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 238000005191 phase separation Methods 0.000 description 2
- 230000002940 repellent Effects 0.000 description 2
- 239000005871 repellent Substances 0.000 description 2
- 239000012488 sample solution Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 125000001424 substituent group Chemical group 0.000 description 2
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 1
- BLEZTPDKUBSTII-UHFFFAOYSA-N 1-chloro-1-fluoroprop-1-ene Chemical compound CC=C(F)Cl BLEZTPDKUBSTII-UHFFFAOYSA-N 0.000 description 1
- LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 1
- FDMFUZHCIRHGRG-UHFFFAOYSA-N 3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C=C FDMFUZHCIRHGRG-UHFFFAOYSA-N 0.000 description 1
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 229910001369 Brass Inorganic materials 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000002519 antifouling agent Substances 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 239000005388 borosilicate glass Substances 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- NHGVZTMBVDFPHJ-UHFFFAOYSA-N formyl fluoride Chemical compound FC=O NHGVZTMBVDFPHJ-UHFFFAOYSA-N 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- 125000001072 heteroaryl group Chemical group 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000004805 propylene group Chemical class [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 238000007614 solvation Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/43—Solvents
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/004—Surface-active compounds containing F
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/004—Surface-active compounds containing F
- C11D1/006—Surface-active compounds containing fluorine and phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/50—Solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/50—Solvents
- C11D7/5004—Organic solvents
- C11D7/5018—Halogenated solvents
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G5/00—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
- C23G5/02—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
- C23G5/028—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing halogenated hydrocarbons
- C23G5/02809—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing halogenated hydrocarbons containing chlorine and fluorine
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G5/00—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
- C23G5/02—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
- C23G5/028—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing halogenated hydrocarbons
- C23G5/02809—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing halogenated hydrocarbons containing chlorine and fluorine
- C23G5/02825—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing halogenated hydrocarbons containing chlorine and fluorine containing hydrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/02—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using organic solvents
- D06L1/04—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using organic solvents combined with specific additives
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
- D06M13/453—Phosphates or phosphites containing nitrogen atoms
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/10—Processes in which the treating agent is dissolved or dispersed in organic solvents; Processes for the recovery of organic solvents thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Textile Engineering (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Dispersion Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Detergent Compositions (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Cleaning By Liquid Or Steam (AREA)
Abstract
【選択図】なし
Description
[02]本発明は、洗浄及び/又は脱水組成物並びに方法に関する。
であり、但しR1、R2、及びR3基の1以下は水素であり、nは1〜16であり、Rfはフルオロカーボン基、好ましくはCmF2m+1(ここで、mは2、4、6、8、10、又は12である)
である)
による界面活性剤、又は複数のかかる界面活性剤の混合物から選択される。好ましくは、nは2、3、又は4である。より好ましくは、nは2であり、Rfは6〜8の平均m値を有するα−フルオロポリジフルオロメチレンである。Rf=F(CF2)x。好適な分布は以下のものを含んでいてよい:Rf−C4H9−最大で4%;C6F13−50±3%;C8F17−29±2%;C10F21−11±2%;及びC14F29−最大で2%。例えば、Rfの平均は7.3%であり、平均分子量は553であり、平均F含量%は56%である。
であり;R4はC1〜C18ペルフルオロアルキルであり;nは1〜4であり;R5、R6、及びR7は、同一であっても異なっていてもよく、H、線状又は分岐のC1〜C16アルキル、フルオロアルキル、又はアルキルアリール基、又は
であり、但しR5、R6、及びR7の1以下はHである)
から選択されるか又はかかる複数の界面活性剤の混合物から選択される。
の構造を有する化合物を含む。
XCFzR3−z (B)
(式中、XはC2、C3、C4、又はC5の不飽和で置換又は非置換の基であり、それぞれのRは独立して、Cl、F、Br、I、又はHであり、zは1〜3である)の式Bを有する化合物を含む。幾つかの好ましい態様においては、本発明のフルオロアルケンは少なくとも4つのハロゲン置換基を有し、その少なくとも3つはFであり、更により好ましくはそれらのいずれもBrではない。幾つかの好ましい態様においては、式Bの化合物は、それぞれの非末端不飽和炭素がフッ素置換基を有する化合物、好ましくは三炭素化合物を含む。
「HFO−1234」という用語は、ここでは全てのテトラフルオロプロペンを指すように用いる。テトラフルオロプロペンの中には、1,1,1,2−テトラフルオロプロペン(HFO−1234yf)、並びにシス及びトランスの両方の1,1,1,3−テトラフルオロプロペン(HFO−1234ze)が含まれる。「HFO−1234ze」という用語は、ここでは、シス形態であるか又はトランス形態であるかに関係なく包括的に1,1,1,3−テトラフルオロプロペンを指すように用いる。「シスHFO−1234ze」及び「トランスHFO−1234ze」という用語は、ここではそれぞれ1,1,1,3−テトラフルオロプロペンのシス及びトランス形態を表すように用いる。したがって、「HFO−1234ze」という用語は、その範囲内にシスHFO−1234ze、トランスHFO−1234ze、並びにこれらの全ての組合せ及び混合物を含む。
[45]これは、ヒドロクロロフルオロ−オレフィン、ヒドロフルオロ−オレフィン、又はこれらの混合物中に界面活性剤を溶解することによって行うことができる。次に、組成物を基材によって吸収させるのに十分な時間噴霧(エアロゾル又はポンプ)又は浸漬することによって、基材を組成物で湿潤させる。更に、汚れた基材を溶媒−界面活性剤組成物と接触させることによって、基材からの固体の除去を促進させることができる。この方法は、基材が布帛である場合にその最も大きな有用性が見出されると考えられる。
[47]或いは、界面活性剤の代わりにアルコールのような第2の溶媒を含ませることができる。好ましくは、この溶媒はメタノール、エタノール、又はイソプロパノールである。この第2の溶媒をヒドロクロロフルオロ−オレフィン又はヒドロフルオロ−オレフィンと共に用いることは、上記で議論したものと同じ乾燥及びドライクリーニングにおいて用いることができる。撥汚用途のためには、本発明の1種類以上のヒドロクロロフルオロ−オレフィン又はヒドロフルオロ−オレフィン溶媒を1種類以上のアルコールと組み合わせて用いて界面活性剤を有効に溶解し、次に上記で議論したような噴霧又は浸漬適用のようなプロセスを用いてそれを布帛に付与することができる。
[49]界面活性剤−溶媒の組合せを用いる場合には、乾燥、ドライクリーニング、及び撥汚性付与(界面活性剤を存在させるドライクリーニングの結果としてか、或いは撥汚剤として界面活性剤を直接施すことによる)においては、例えば固体基材を乾燥した後に少量の界面活性剤が残留することが注記される。通常は、この残留界面活性剤は界面活性剤の単分子層である。
[52]実施例1:
[53]500重量ppmのペルフルオロアルキルピリジニウムのオクチルフェニル酸ホスフェート塩(5,856,286の実施例2において製造された界面活性剤)を含む35mLの溶媒:1−クロロ−3,3,3−トリフルオロ−1−プロペンを、冷却コイルを取り付けた100mLのビーカー内に配置することによって、本発明の溶媒−界面活性剤組成物の水置換における性能を評価した。溶液を沸騰させ、冷却コイルによって溶媒蒸気をビーカーに閉じ込めた。無水状態まで湿分を減少させた2つの316ステンレススチールの試験片を、水中、次に沸騰試料溶液中に浸漬した。試験片から水を置換するのに必要な時間を記録した。5秒間の最小観察時間を選択した。
[57]5重量%のメタノール溶媒を含む35mLの1−クロロ−3,3,3−トリフルオロ−1−プロペン溶媒を、冷却コイルを取り付けた100mLのビーカー内に配置することによって、本発明の溶媒−溶媒組成物の水置換における性能を評価した。溶液を沸騰させ、冷却コイルによって溶媒蒸気をビーカーに閉じ込めた。無水状態まで湿分を減少させた2つの316ステンレススチールの試験片を、水中、次に沸騰試料溶液中に浸漬した。5秒間の最小観察時間を用いて、試験片から水を置換するのに必要な時間を記録した。溶媒アルコールブレンドは基材から水を完全に除去することができた。
Claims (20)
- 有効量の少なくとも1種類のヒドロフルオロ−オレフィン又はヒドロクロロフルオロ−オレフィン溶媒、並びに、ヒドロフルオロ−オレフィン又はヒドロクロロフルオロ−オレフィン溶媒中に可溶の少なくとも1種類の疎水性フッ素含有界面活性剤を含む組成物。
- 界面活性剤が、式I又は式II:
であり、但しR1、R2、及びR3基の1以下は水素であり、nは1〜16であり、RfはCmF2m+1(ここで、mは2、4、6、8、10、又は12である)
である)
を有する請求項1に記載の組成物、又はかかる界面活性剤組成物の混合物。 - nが2、3、又は4である、請求項2に記載の組成物。
- n=2であり、Rfが約6〜8の平均m値を有するα−フルオロポリジフルオロメチレンである、請求項2に記載の組成物。
- 界面活性剤が4−tert−オクチルフェニル一酸ホスフェートのオリゴマーペルフルオロアルキルピリジニウム塩、4−tert−オクチルフェニル二酸ホスフェートのオリゴマーペルフルオロアルキルピリジニウム塩、或いはこれらの混合物である、請求項2に記載の組成物。
- 界面活性剤が、式III又は式IV:
であり;R4はC1〜C18ペルフルオロアルキルであり;nは1〜4であり;R5、R6、及びR7は、同一であっても異なっていてもよく、H、線状又は分岐のC1〜C16アルキル、フルオロアルキル、又はアルキルアリール基、又は
であり、但しR5、R6、及びR7の1以下はHである)
を有する請求項1に記載の組成物、又はかかる界面活性剤の混合物。 - 界面活性剤が、オクチルフェニル(一)酸ホスフェートのジエチルメチル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩、オクチルフェニル(二)塩ホスフェートのジエチルメチル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩;オクチルフェニル(一)酸ホスフェートのジメチルベンジル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩、及びオクチルフェニル(二)酸ホスフェートのジメチルベンジル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩;オクチルフェニル(一)酸ホスフェートのジエチルベンジル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩、及びオクチルフェニル(二)酸ホスフェートのジエチルベンジル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩;からなる群から選択される、請求項6に記載の組成物。
- オクチルフェニル酸ホスフェートのジエチルメチル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩、又はオクチルフェニル酸ホスフェートのジメチルベンジル1,1,2,2−テトラヒドロペルフルオロデシルアミン塩である、請求項6に記載の組成物。
- ジメチルメチルアミン塩であり、R4がC8〜C16である、請求項6に記載の組成物。
- ジメチルベンジルアミン塩であり、R4がC8〜C16である、請求項6に記載の組成物。
- ヒドロクロロフルオロ−オレフィン溶媒として1−クロロ−3,3,3−トリフルオロ−1−プロペンを含む、請求項1に記載の組成物。
- 基材を請求項1に記載の溶媒−界面活性剤組成物と接触させ、次に物品から溶媒界面活性剤組成物を除去する工程を含む、基材の表面を乾燥する方法。
- 物品を請求項1に記載の溶媒−界面活性剤組成物に接触させ、次に物品から溶媒界面活性剤組成物を除去する工程を含む、物品をドライクリーニングする方法。
- 布帛を請求項1に記載の溶媒−界面活性剤組成物に接触させるか又は曝露し、布帛から溶媒を除去する工程を含む、布帛に撥汚性を与える方法。
- 有効量の少なくとも1種類のヒドロフルオロ−オレフィン又はヒドロクロロフルオロ−オレフィン、及びアルコールから選択される少なくとも1種類の溶媒を含む組成物。
- 溶媒が、メタノール、エタノール、及びイソプロパノールからなる群から選択される、請求項16に記載の組成物。
- 基材又は物品を請求項16に記載の組成物と接触させ、次に基材又は物品から組成物を除去する工程を含む、基材の表面を乾燥するか又は物品をドライクリーニングする方法。
- 布帛を界面活性剤及び請求項16に記載の組成物に接触させるか又は曝露し、次に組成物を除去して布帛の表面上に界面活性剤を残留させる工程を含む、布帛に撥汚性を与える方法。
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2009
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Cited By (3)
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JP2014532699A (ja) * | 2011-11-02 | 2014-12-08 | ハネウェル・インターナショナル・インコーポレーテッド | 燻蒸剤組成物及び方法 |
JP2015508435A (ja) * | 2011-12-22 | 2015-03-19 | ハネウェル・インターナショナル・インコーポレーテッド | 1−クロロ−3,3,3−トリフルオロプロペンを包含する溶媒組成物およびその使用 |
JP2014181405A (ja) * | 2013-03-15 | 2014-09-29 | Honeywell Internatl Inc | 洗浄組成物及び方法 |
Also Published As
Publication number | Publication date |
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JP5841430B2 (ja) | 2016-01-13 |
EP2376410B1 (en) | 2018-08-29 |
JP2014139320A (ja) | 2014-07-31 |
CN102317243B (zh) | 2015-03-25 |
KR20110096164A (ko) | 2011-08-29 |
EP2376410A4 (en) | 2014-10-15 |
CN104762138A (zh) | 2015-07-08 |
HUE040174T2 (hu) | 2019-02-28 |
CN102317243A (zh) | 2012-01-11 |
PL2376410T3 (pl) | 2019-02-28 |
CN104762138B (zh) | 2019-07-26 |
HK1164267A1 (en) | 2012-09-21 |
KR20170078864A (ko) | 2017-07-07 |
ES2700080T3 (es) | 2019-02-13 |
JP5934734B2 (ja) | 2016-06-15 |
JP2016186077A (ja) | 2016-10-27 |
US8637443B2 (en) | 2014-01-28 |
US20120015863A1 (en) | 2012-01-19 |
KR101753621B1 (ko) | 2017-07-19 |
EP2376410A1 (en) | 2011-10-19 |
WO2010080544A1 (en) | 2010-07-15 |
JP2018031011A (ja) | 2018-03-01 |
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