JP2011506072A5 - - Google Patents

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JP2011506072A5
JP2011506072A5 JP2010537343A JP2010537343A JP2011506072A5 JP 2011506072 A5 JP2011506072 A5 JP 2011506072A5 JP 2010537343 A JP2010537343 A JP 2010537343A JP 2010537343 A JP2010537343 A JP 2010537343A JP 2011506072 A5 JP2011506072 A5 JP 2011506072A5
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reaction
heat medium
medium
reactor
particles
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JP2010537343A
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JP2011506072A (en
JP5587200B2 (en
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Priority claimed from DE102007059967A external-priority patent/DE102007059967A1/en
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リアクター内で、少なくとも１つの第１反応性物質を含む反応媒体を加熱し、第１反応性物質中、または第１と第２の反応性物質の間で化学結合を形成または修飾することにより目的化合物を製造するための化学反応を行う方法であって、電磁誘導により加熱することができ、かつリアクターの内側にあり反応媒体により囲まれている固形熱媒体と反応媒体を接触させ、前記熱媒体を誘導子を用いて電磁誘導により加熱し、目的化合物を第１反応性物質からまたは第１反応性物質と第２反応性物質とから形成し、前記目的化合物を電熱媒体から分離する方法であり、リアクター内の反応媒体が液体として存在し、誘導子が１〜１００ｋＨｚの範囲の交番磁場を生じる方法。 In the reactor, the reaction medium containing at least one first reactive substance is heated to form or modify a chemical bond in the first reactive substance or between the first and second reactive substances. A method for performing a chemical reaction for producing a compound, wherein the reaction medium is brought into contact with a solid heat medium that can be heated by electromagnetic induction and is surrounded by the reaction medium inside the reactor. Is heated by electromagnetic induction using an inductor, the target compound is formed from the first reactive substance or from the first reactive substance and the second reactive substance, and the target compound is separated from the heating medium . A method in which the reaction medium in the reactor is present as a liquid and the inductor generates an alternating magnetic field in the range of 1 to 100 kHz. 熱媒体が導電性および／または磁化性固体の粒子から選択され、該粒子の平均粒度径が１〜１０００ｎｍである請求項１に記載の方法。   The method according to claim 1, wherein the heat medium is selected from particles of a conductive and / or magnetizable solid, and the average particle size of the particles is 1-1000 nm. 熱媒体が磁化性固体の粒子から選択され、各粒子が非磁性物質によりカプセル化された少なくとも１つの磁化性物質のコアを含んでなる請求項２に記載の方法。   3. A method according to claim 2, wherein the heat medium is selected from particles of a magnetizable solid, each particle comprising a core of at least one magnetizable material encapsulated by a non-magnetic material. 熱媒体が磁化性固体の粒子から選択され、これらが電磁誘導により加熱できないさらなる粒子との混合物中に存在している、請求項２または３に記載の方法。   The method according to claim 2 or 3, wherein the heat medium is selected from particles of a magnetizable solid, which are present in a mixture with further particles that cannot be heated by electromagnetic induction. 固形熱媒体が、化学反応に対する触媒活性物質により表面被覆されている、請求項１〜４のいずれかに記載の方法。   The method according to claim 1, wherein the solid heat medium is surface-coated with a catalytically active substance for chemical reaction. 化学反応をバッチ式で行い、反応中、反応媒体および固形熱媒体が互いに移動し合う、請求項１〜５のいずれかに記載の方法。   The method according to any one of claims 1 to 5, wherein the chemical reaction is carried out batchwise, and the reaction medium and the solid heat medium move with each other during the reaction. 反応媒体が反応槽中に熱媒体の粒子とともに存在し、反応媒体に誘導子として配置された可動素子により反応媒体を移動させることにより熱媒体の粒子を加熱する、請求項６に記載の方法。   The method according to claim 6, wherein the reaction medium is present together with the particles of the heat medium in the reaction tank, and the particles of the heat medium are heated by moving the reaction medium with a movable element arranged as an inductor in the reaction medium. 少なくとも部分的に固形熱媒体が充填されることにより、電磁誘導によって加熱し得る少なくとも１つの加熱領域を有するフロー型リアクターで化学反応を行い、反応媒体がフロー型リアクター内を流れ、誘導子がリアクター外部に配置されている、請求項１〜５のいずれかに記載の方法。   At least partially filled with a solid heat medium, a chemical reaction is performed in a flow type reactor having at least one heating region that can be heated by electromagnetic induction, the reaction medium flows in the flow type reactor, and the inductor is the reactor. The method according to claim 1, wherein the method is arranged outside. 反応媒体と熱媒体との総接触時間が１秒〜２時間の範囲になるような速度で、反応媒体がフロー型リアクター内を１回または複数回流れる、請求項８に記載の方法。   The method according to claim 8, wherein the reaction medium flows through the flow reactor one or more times at a rate such that the total contact time between the reaction medium and the heat medium is in the range of 1 second to 2 hours. リアクターが圧力リアクターとして構成され、化学反応を大気圧より高い圧力で、好ましくは少なくとも１．５ｂａｒの圧力下で行う、請求項１〜９のいずれかに記載の方法。   10. A method according to any of the preceding claims, wherein the reactor is configured as a pressure reactor and the chemical reaction is carried out at a pressure above atmospheric pressure, preferably at a pressure of at least 1.5 bar. 熱媒体が強磁性体であって、４０〜２５０℃の範囲のキュリー温度を示し、かつ、キュリー温度が選択された反応温度から２０℃より大きく異ならないように熱媒体を選択する、請求項１〜１０のいずれかに記載の方法。 The heat medium is ferromagnetic and exhibits a Curie temperature in the range of 40-250 ° C, and the heat medium is selected such that the Curie temperature does not differ more than 20 ° C from the selected reaction temperature. The method according to any one of 10 to 10 . 化学反応において、化学結合を２つの炭素原子の間に、または炭素原子と原子Ｘ〔Ｘは、Ｈ、Ｂ、Ｏ、Ｎ、Ｓ、Ｐ、Ｓｉ、Ｇｅ、Ｓｎ、Ｐｂ、Ａｓ、Ｓｂ、Ｂｉおよびハロゲンから選択される〕との間に形成する、請求項１〜１１のいずれかに記載の方法。 In a chemical reaction, a chemical bond is formed between two carbon atoms, or a carbon atom and an atom X [X is H, B, O, N, S, P, Si, Ge, Sn, Pb, As, Sb, Bi. and formed between selected from halogen], the method of any of claims 1-11.
JP2010537343A 2007-12-11 2008-10-14 Method for performing chemical reaction using inductively heated heat medium Expired - Fee Related JP5587200B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102007059967A DE102007059967A1 (en) 2007-12-11 2007-12-11 Method for carrying out chemical reactions by means of an inductively heated heating medium
DE102007059967.8 2007-12-11
PCT/EP2008/063763 WO2009074373A1 (en) 2007-12-11 2008-10-14 Method for carrying out chemical reactions with the aid of an inductively heated heating medium

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JP2011506072A JP2011506072A (en) 2011-03-03
JP2011506072A5 true JP2011506072A5 (en) 2011-12-01
JP5587200B2 JP5587200B2 (en) 2014-09-10

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US (2) US20100249404A1 (en)
EP (1) EP2219778B1 (en)
JP (1) JP5587200B2 (en)
KR (1) KR20100098387A (en)
CN (1) CN101896263B (en)
AT (1) ATE516077T1 (en)
DE (1) DE102007059967A1 (en)
ES (1) ES2367467T3 (en)
WO (1) WO2009074373A1 (en)

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