JP2008509397A5 - - Google Patents
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- JP2008509397A5 JP2008509397A5 JP2007524971A JP2007524971A JP2008509397A5 JP 2008509397 A5 JP2008509397 A5 JP 2008509397A5 JP 2007524971 A JP2007524971 A JP 2007524971A JP 2007524971 A JP2007524971 A JP 2007524971A JP 2008509397 A5 JP2008509397 A5 JP 2008509397A5
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- Prior art keywords
- column
- plug
- temperature
- chromatography column
- polymerization
- Prior art date
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- 238000004587 chromatography analysis Methods 0.000 claims 16
- 238000006116 polymerization reaction Methods 0.000 claims 16
- 239000000203 mixture Substances 0.000 claims 11
- 229920000642 polymer Polymers 0.000 claims 6
- 238000000034 method Methods 0.000 claims 5
- 239000003361 porogen Substances 0.000 claims 5
- 238000006243 chemical reaction Methods 0.000 claims 4
- 230000000379 polymerizing effect Effects 0.000 claims 4
- 238000005457 optimization Methods 0.000 claims 3
- 238000003825 pressing Methods 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 2
- 238000012856 packing Methods 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 150000001450 anions Chemical class 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- UJKWLAZYSLJTKA-UHFFFAOYSA-N edma Chemical compound O1CCOC2=CC(CC(C)NC)=CC=C21 UJKWLAZYSLJTKA-UHFFFAOYSA-N 0.000 claims 1
- 239000003999 initiator Substances 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 229920002959 polymer blend Polymers 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 230000008961 swelling Effects 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
Claims (9)
- サンプルインジェクター;サンプルインジェクターからサンプルを受け取るために位置するカラムケーシングの内側の少なくとも1つの透過性モノリシックポリマー性プラグ及びカラムケーシングを有する少なくとも1つのクロマトグラフィーカラム;溶剤を少なくとも1つのクロマトグラフィーカラムに供給し、それにより、サンプルが、その成分に、少なくとも1つのクロマトグラフィーカラム内で分離されるためのクロマトグラフィーカラムに連通する溶剤系;内部カラム壁表面を有するカラムケーシング壁を含む前記少なくとも1つのカラムケーシング;及び前記クロマトグラフィーカラムから液体を受け取るためのユーティリティデバイスを含むクロマトグラフシステムであって、カラム壁の内側面と接触する切れ目のない滑らかな壁を有する少なくとも1つの透過性モノリシックポリマー性、温度−時間適切化プラグにより特徴付けられるクロマトグラフシステム。
- 発熱により生じる実質的に不均一な細孔サイズなしにポリマー性モノリシックパッキング及びカラムケーシングを有するクロマトグラフィーカラムにサンプルを供給する工程;及び溶剤をクロマトグラフィーカラムに供給し、それにより、サンプルが、その成分に、クロマトグラフィーカラム内で分離される工程を含むクロマトグラフィーを行う方法であって、ポリマー性モノリシックパッキングが、温度−時間適切化されている方法。
- 内部カラム壁内の分離−有効開口部を有する透過性モノリシックポリマー性プラグ及び該カラム壁を有するクロマトグラフィーカラム支持体を含むクロマトグラフィーカラムであって、透過性モノリシックポリマー性プラグが、温度−時間適切化及び圧力下での重合により形成される断面均一性及び滑らかな壁を有するポリマーであることを特徴とするクロマトグラフィーカラム。
- 重合の間の温度変化のための手段とそれによる重合混合物が温度−時間適切化及び前記温度制御反応チャンバーにおける前記重合混合物に圧力を加えるための手段により特徴付けられる重合の間に重合混合物を含むように適応された温度制御反応チャンバーを含むクロマトグラフィーカラムを製造するための装置。
- プラグを形成するための重合の間に重合混合物を含むように適応された温度制御反応チャンバー;プラグに水溶液を加えるための水性処理手段;及び該プラグに圧力を加えて、プラグにおけるボイドを低減するための手段を含むクロマトグラフィーカラムを製造するための装置であって、温度制御反応チャンバーが、温度−時間適切化のための手段を含む装置。
- カラムケーシング内にポロゲンを含む重合混合物を置く工程を含む方法であって、低及び高温度重合の組み合わせ及び圧力を使用してカラムケーシング内の重合混合物を重合し、滑らかな壁を有するポリマープラグを形成する工程により特徴付けられる方法。
- ポロゲンを含む重合混合物を重合する工程を含むモノリシッククロマトグラフィーカラムを製造する方法であって、温度−時間適切化条件下及び圧力下で重合を行い、それにより、温度勾配が制御されて、滑らかな壁を有するモノリシッククロマトグラフィーカラムにおける空間断面変化を防止することを特徴とする方法。
- 温度−時間適切化で重合を行って、ポリマープラグを形成することにより特徴付けられるポロゲンを含む重合混合物を製造する工程;ポリマープラグを洗浄して、ポロゲンを除去する工程、ここでプラグが膨張する傾向にある;及び圧力を加えて、ポリマープラグの膨張を防止し及びボイドを排除する工程を含むモノリシッククロマトグラフィーカラムを製造する方法。
- GMA、ATMS、EDMA、開始剤及びポロゲンを混合して、重合混合物を形成する工程;及びカラム内において混合物を重合する工程を含む強アニオンカラムを製造する方法であって、混合物を、温度−時間適切化条件下で重合して、プラグを形成することを特徴とする方法。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/914,005 US20050061745A1 (en) | 2002-06-26 | 2004-08-06 | Separation system, components of a separation system and methods of making and using them |
PCT/US2005/027655 WO2006017620A2 (en) | 2004-08-06 | 2005-08-02 | Separation system, components of a separation system and methods of making and using them |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2008509397A JP2008509397A (ja) | 2008-03-27 |
JP2008509397A5 true JP2008509397A5 (ja) | 2008-08-28 |
Family
ID=35839893
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2007524971A Abandoned JP2008509397A (ja) | 2004-08-06 | 2005-08-02 | 分離システム、分離システムの構成要素及びそれらを製造及び使用する方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US20050061745A1 (ja) |
EP (1) | EP1789157A4 (ja) |
JP (1) | JP2008509397A (ja) |
KR (1) | KR20070050059A (ja) |
CN (1) | CN101035602A (ja) |
AU (1) | AU2005271426A1 (ja) |
CA (1) | CA2575570A1 (ja) |
WO (1) | WO2006017620A2 (ja) |
Families Citing this family (22)
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ITRM20060723A1 (it) * | 2006-12-29 | 2008-06-30 | Avantech Group S R L | Colonne cromatografiche ad elevate prestazioni contenenti supporti monolitici polimerici organici o compositi e relativo metodo di preparazione. |
WO2009120642A1 (en) | 2008-03-26 | 2009-10-01 | Massachusetts Institute Of Technology | Methods for fabricating electrokinetic concentration devices |
WO2011069289A1 (zh) * | 2009-12-10 | 2011-06-16 | 利穗科技(苏州)有限公司 | 可视荧光层析柱 |
GB2477093A (en) * | 2010-01-20 | 2011-07-27 | Univ Dublin City | Capillary column |
US11565197B2 (en) | 2013-06-14 | 2023-01-31 | Waters Technologies Corporation | Methodology for scaling methods between supercritical fluid chromatography systems |
US20170080357A1 (en) * | 2014-05-12 | 2017-03-23 | Waters Technologies Corporation | Column temperature compensation for carbon dioxide based chromatographic system |
EP3173783B1 (en) | 2014-07-25 | 2019-02-27 | Asahi Kasei Medical Co., Ltd. | Cation-exchange chromatography support and method for using same |
GB201418893D0 (en) | 2014-10-23 | 2014-12-10 | Univ Hull | Monolithic body |
GB201418899D0 (en) | 2014-10-23 | 2014-12-10 | Univ Hull | System for radiopharmaceutical production |
GB201418897D0 (en) | 2014-10-23 | 2014-12-10 | Univ Hull | Methods and apparatus for the analysis of compounds |
US11167264B2 (en) | 2015-03-10 | 2021-11-09 | Showa Denko K.K. | Packing material for liquid chromatography |
WO2017022695A1 (ja) * | 2015-07-31 | 2017-02-09 | 株式会社ダイセル | 超臨界流体クロマトグラフィー用の固定相 |
US10907014B2 (en) * | 2016-08-15 | 2021-02-02 | The Board Of Regents Of The Nevada System Of Higher Education On Behalf Of The University Of Nevada, Las Vegas | Polymer compositions |
JP6570795B2 (ja) * | 2017-08-25 | 2019-09-04 | 積水メディカル株式会社 | メチル化dna分離及び/又は検出用クロマトグラフィー用充填剤 |
JP7144176B2 (ja) * | 2018-04-13 | 2022-09-29 | 株式会社島津製作所 | 抽出物の回収方法および分析方法 |
US20220146541A1 (en) * | 2019-03-12 | 2022-05-12 | Shimadzu Corporation | Analysis device |
CN110426528B (zh) * | 2019-07-24 | 2024-07-05 | 云南中烟工业有限责任公司 | 一种用于多个样品前处理的装置及其使用方法 |
CN112439377A (zh) * | 2019-08-29 | 2021-03-05 | 江苏察克润滑科技有限公司 | 一种用于制备防锈液的反应釜 |
CN112831087B (zh) * | 2020-12-28 | 2022-11-11 | 珠海健科医用材料有限公司 | 血液净化用大孔聚苯乙烯树脂表面改性方法和血液净化器 |
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- 2004-08-06 US US10/914,005 patent/US20050061745A1/en not_active Abandoned
-
2005
- 2005-08-02 AU AU2005271426A patent/AU2005271426A1/en not_active Abandoned
- 2005-08-02 EP EP05783699A patent/EP1789157A4/en not_active Withdrawn
- 2005-08-02 KR KR1020077005284A patent/KR20070050059A/ko not_active Application Discontinuation
- 2005-08-02 CN CNA2005800342506A patent/CN101035602A/zh active Pending
- 2005-08-02 WO PCT/US2005/027655 patent/WO2006017620A2/en active Application Filing
- 2005-08-02 CA CA002575570A patent/CA2575570A1/en not_active Abandoned
- 2005-08-02 JP JP2007524971A patent/JP2008509397A/ja not_active Abandoned
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