JP2006160964A - Polishing-agent containing detergent - Google Patents
Polishing-agent containing detergent Download PDFInfo
- Publication number
- JP2006160964A JP2006160964A JP2004357631A JP2004357631A JP2006160964A JP 2006160964 A JP2006160964 A JP 2006160964A JP 2004357631 A JP2004357631 A JP 2004357631A JP 2004357631 A JP2004357631 A JP 2004357631A JP 2006160964 A JP2006160964 A JP 2006160964A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- alkyl
- polyoxyethylene
- alcohol
- abrasive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 8
- 239000003599 detergent Substances 0.000 title abstract description 6
- 239000004094 surface-active agent Substances 0.000 claims abstract description 20
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims abstract description 12
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical group CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims abstract description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 9
- 125000001165 hydrophobic group Chemical group 0.000 claims abstract description 9
- 238000004140 cleaning Methods 0.000 claims abstract description 8
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 26
- 239000012459 cleaning agent Substances 0.000 claims description 19
- 125000004432 carbon atom Chemical group C* 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 238000005498 polishing Methods 0.000 claims description 3
- 125000003198 secondary alcohol group Chemical group 0.000 claims 1
- 239000010730 cutting oil Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 5
- 230000002085 persistent effect Effects 0.000 abstract 1
- -1 polyoxyethylene Polymers 0.000 description 100
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 36
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 35
- 235000014113 dietary fatty acids Nutrition 0.000 description 27
- 239000000194 fatty acid Substances 0.000 description 27
- 229930195729 fatty acid Natural products 0.000 description 27
- 238000011156 evaluation Methods 0.000 description 26
- 229920001296 polysiloxane Polymers 0.000 description 25
- 150000005215 alkyl ethers Chemical class 0.000 description 18
- 125000000217 alkyl group Chemical group 0.000 description 16
- 235000002639 sodium chloride Nutrition 0.000 description 14
- 150000004665 fatty acids Chemical class 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 239000000284 extract Substances 0.000 description 12
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- JVTIXNMXDLQEJE-UHFFFAOYSA-N 2-decanoyloxypropyl decanoate 2-octanoyloxypropyl octanoate Chemical compound C(CCCCCCC)(=O)OCC(C)OC(CCCCCCC)=O.C(=O)(CCCCCCCCC)OCC(C)OC(=O)CCCCCCCCC JVTIXNMXDLQEJE-UHFFFAOYSA-N 0.000 description 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 11
- 239000004166 Lanolin Substances 0.000 description 11
- 235000019388 lanolin Nutrition 0.000 description 11
- 229940039717 lanolin Drugs 0.000 description 11
- 239000008213 purified water Substances 0.000 description 11
- 239000002280 amphoteric surfactant Substances 0.000 description 10
- 150000003839 salts Chemical class 0.000 description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- 239000002253 acid Substances 0.000 description 9
- 239000003945 anionic surfactant Substances 0.000 description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 239000003921 oil Substances 0.000 description 7
- 235000019198 oils Nutrition 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 6
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 206010040880 Skin irritation Diseases 0.000 description 6
- 125000005211 alkyl trimethyl ammonium group Chemical group 0.000 description 6
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 description 6
- 229960003237 betaine Drugs 0.000 description 6
- 239000004359 castor oil Substances 0.000 description 6
- 235000019438 castor oil Nutrition 0.000 description 6
- 239000003240 coconut oil Substances 0.000 description 6
- 235000019864 coconut oil Nutrition 0.000 description 6
- 235000011187 glycerol Nutrition 0.000 description 6
- 229960005150 glycerol Drugs 0.000 description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- 230000036556 skin irritation Effects 0.000 description 6
- 231100000475 skin irritation Toxicity 0.000 description 6
- 235000015424 sodium Nutrition 0.000 description 6
- 229940083542 sodium Drugs 0.000 description 6
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- 239000004519 grease Substances 0.000 description 5
- 229940060184 oil ingredients Drugs 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 4
- MPDGHEJMBKOTSU-YKLVYJNSSA-N 18beta-glycyrrhetic acid Chemical compound C([C@H]1C2=CC(=O)[C@H]34)[C@@](C)(C(O)=O)CC[C@]1(C)CC[C@@]2(C)[C@]4(C)CC[C@@H]1[C@]3(C)CC[C@H](O)C1(C)C MPDGHEJMBKOTSU-YKLVYJNSSA-N 0.000 description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- 241000283690 Bos taurus Species 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 4
- 239000002202 Polyethylene glycol Substances 0.000 description 4
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 4
- 244000269722 Thea sinensis Species 0.000 description 4
- CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 4
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
- FUWUEFKEXZQKKA-UHFFFAOYSA-N beta-thujaplicin Chemical compound CC(C)C=1C=CC=C(O)C(=O)C=1 FUWUEFKEXZQKKA-UHFFFAOYSA-N 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 210000002826 placenta Anatomy 0.000 description 4
- 229920000573 polyethylene Polymers 0.000 description 4
- 229920001223 polyethylene glycol Polymers 0.000 description 4
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 description 4
- 229920001451 polypropylene glycol Polymers 0.000 description 4
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 4
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 4
- 125000003944 tolyl group Chemical group 0.000 description 4
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 4
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 235000019482 Palm oil Nutrition 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 229960000458 allantoin Drugs 0.000 description 3
- 239000006229 carbon black Substances 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 229960002449 glycine Drugs 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 3
- 239000002540 palm oil Substances 0.000 description 3
- 229940081974 saccharin Drugs 0.000 description 3
- 235000019204 saccharin Nutrition 0.000 description 3
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 description 3
- 150000003333 secondary alcohols Chemical group 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 235000010356 sorbitol Nutrition 0.000 description 3
- 239000000600 sorbitol Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229940088594 vitamin Drugs 0.000 description 3
- 229930003231 vitamin Natural products 0.000 description 3
- 235000013343 vitamin Nutrition 0.000 description 3
- 239000011782 vitamin Substances 0.000 description 3
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 description 2
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 description 2
- ARXKVVRQIIOZGF-UHFFFAOYSA-N 1,2,4-butanetriol Chemical compound OCCC(O)CO ARXKVVRQIIOZGF-UHFFFAOYSA-N 0.000 description 2
- GKQHIYSTBXDYNQ-UHFFFAOYSA-M 1-dodecylpyridin-1-ium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+]1=CC=CC=C1 GKQHIYSTBXDYNQ-UHFFFAOYSA-M 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 2
- GRVMJKAAXNELJW-UHFFFAOYSA-N 1-phenylpropan-1-amine;hydrochloride Chemical compound [Cl-].CCC([NH3+])C1=CC=CC=C1 GRVMJKAAXNELJW-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 2
- WJYAJBDKANFOID-UHFFFAOYSA-N 2-(dodecylamino)propanoic acid Chemical compound CCCCCCCCCCCCNC(C)C(O)=O WJYAJBDKANFOID-UHFFFAOYSA-N 0.000 description 2
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- XZIIFPSPUDAGJM-UHFFFAOYSA-N 6-chloro-2-n,2-n-diethylpyrimidine-2,4-diamine Chemical compound CCN(CC)C1=NC(N)=CC(Cl)=N1 XZIIFPSPUDAGJM-UHFFFAOYSA-N 0.000 description 2
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- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 description 1
Abstract
Description
本発明は、エチレンオキシド残基及びプロピレンオキサイド残基からなる親水基を有し炭素数が8〜14の分枝鎖状の飽和または不飽和炭素鎖を疎水基とする界面活性剤を配合してなる研磨剤含有洗浄剤に関する。 The present invention comprises a surfactant having a hydrophilic group composed of an ethylene oxide residue and a propylene oxide residue and having a branched saturated or unsaturated carbon chain having 8 to 14 carbon atoms as a hydrophobic group. The present invention relates to an abrasive-containing cleaning agent.
従来より、研磨剤含有洗浄剤は強力な汚れ落しとして日常雑貨や化粧品分野、工業分野等で広く一般的に使用されている。
通常、特許文献1に記載されている通り洗浄剤としては溶剤や界面活性剤等が使用されている。しかし、溶剤を使用すると洗浄力は高いが環境負荷が大きく皮膚刺激が強い等の問題が多い。一方、界面活性剤は低刺激で環境にも良好であるが洗浄力が弱い欠点を有している事が一般 的に知られている。更に、洗浄力不足を補う目的で研磨剤を配合する記載例が特許文献2や特許文献3に示されているが固体表面や手指に付着した金属加工時に使用される切削油やグリース類等の粘度が高い汚れに対しては十分な洗浄力を有してはいなかった。
Conventionally, abrasive-containing cleaning agents have been widely used in daily goods, cosmetics, industrial fields and the like as powerful stain removers.
Usually, as described in Patent Document 1, a solvent, a surfactant, or the like is used as the cleaning agent. However, when a solvent is used, there are many problems such as high detergency but large environmental load and strong skin irritation. On the other hand, it is generally known that surfactants have the disadvantages of low irritation and good environment but weak detergency. Furthermore, although the description example which mix | blends an abrasive | polishing agent for the purpose of supplementing lack of cleaning power is shown by patent document 2 and patent document 3, cutting oil, greases, etc. which are used at the time of metal processing adhering to a solid surface or fingers It did not have sufficient detergency against dirt with high viscosity.
本発明は高い洗浄力でありながら環境性が良好で皮膚刺激を低減した固体表面や手指に付着した汚れを除去する研磨剤含有洗浄剤を提供することを目的とする。 An object of the present invention is to provide a polishing agent-containing cleaning agent that removes dirt adhering to a solid surface or fingers that has a high environmental performance and good environmental properties and reduced skin irritation.
本発明者は、上記課題を解決するために鋭意研究を重ねた結果、エチレンオキシド残基及びプロピレンオキサイド残基からなる親水基を有し炭素数が8〜14の分枝鎖状の飽和または不飽和炭素鎖を疎水基とする界面活性剤を配合してなる研磨剤含有洗浄剤が、その目的に適合しうることを見出し、この知見に基づいて本発明をなすに至った。
すなわち、本発明は下記に示す通りである。
1.エチレンオキシド残基及びプロピレンオキサイド残基から選ばれる1種または2種の親水基を有し、炭素数が8〜14の分枝鎖状の飽和または不飽和炭素鎖を疎水基とする界面活性剤を配合してなる研磨剤含有洗浄剤。
2.界面活性剤として、疎水基が第2アルコールまたはゲルベアルコールであることを特徴とする前記1記載の研磨剤含有洗浄剤。
3.界面活性剤の親水基のエチレンオキシド残基及びプロピレンオキサイド残基の全平均付加モル数が1モル以上であることを特徴とする前記1又は2に記載の研磨剤含有洗浄剤。
4.固体表面の洗浄に用いられる事を特徴とする前記1〜3のいずれかに記載の研磨剤含有洗浄剤。
5.手指の清浄に用いられる事を特徴とする前記1〜4いずれかに記載の研磨剤含有洗浄剤。
As a result of intensive studies to solve the above-mentioned problems, the present inventor has obtained a branched or saturated unsaturated or unsaturated group having a hydrophilic group comprising an ethylene oxide residue and a propylene oxide residue and having 8 to 14 carbon atoms. It has been found that an abrasive-containing detergent obtained by blending a surfactant having a carbon chain as a hydrophobic group can be adapted to the purpose, and based on this finding, the present invention has been made.
That is, the present invention is as follows.
1. A surfactant having one or two kinds of hydrophilic groups selected from ethylene oxide residues and propylene oxide residues and having a branched saturated or unsaturated carbon chain having 8 to 14 carbon atoms as a hydrophobic group An abrasive-containing cleaning agent formulated.
2. 2. The abrasive-containing cleaning agent according to 1 above, wherein the surfactant is a secondary alcohol or a gel alcohol.
3. 3. The abrasive-containing cleaning agent according to 1 or 2 above, wherein the total average number of added moles of ethylene oxide residue and propylene oxide residue of the hydrophilic group of the surfactant is 1 mol or more.
4). 4. The abrasive-containing cleaning agent according to any one of 1 to 3, which is used for cleaning a solid surface.
5). The abrasive-containing cleaning agent according to any one of 1 to 4, which is used for cleaning fingers.
洗浄力がある界面活性剤や研磨剤を洗浄剤に使用することは公知技術であるが、本発明のエチレンオキシド残基及びプロピレンオキサイド残基からなる親水基を有し炭素数が8
〜14の分枝鎖状の飽和または不飽和炭素鎖を疎水基とする界面活性剤を配合してなる研磨剤含有洗浄剤は固体表面や手指に付着した金属加工時に使用される切削油やグリース類など粘性が高い油脂類に対して高い洗浄力を有し生分解が良好な効果を有する。更に驚くべき事に本発明の研磨剤含有洗浄剤は高洗浄力でありながら皮膚刺激が低い効果も有する。
Although it is a publicly known technique to use a surfactant or abrasive having a detergency as a cleaning agent, it has a hydrophilic group composed of the ethylene oxide residue and the propylene oxide residue of the present invention and has 8 carbon atoms.
Abrasive-containing cleaning agent comprising a surfactant having a branched chain saturated or unsaturated carbon chain of -14 as a hydrophobic group is a cutting oil or grease used during metal working attached to a solid surface or fingers It has a high detergency and high biodegradation effect on highly viscous oils and fats. Surprisingly, the abrasive-containing detergent of the present invention has an effect of low skin irritation while having a high detergency.
本発明について、以下具体的に説明する。
本発明のエチレンオキシド残基及びプロピレンオキサイド残基から選ばれる1種または2種の親水基を有し炭素数が8〜14の分枝鎖状の飽和または不飽和炭素鎖を疎水基とする界面活性剤を配合してなる研磨剤含有洗浄剤の界面活性剤の配合量は特に限定されるものでない。
また、界面活性剤の疎水基としては炭素数が8〜14の第2アルコールまたはゲルベアルコールが洗浄力、皮膚刺激性、生分解性の点で優れている。ここで言う第2アルコールとは、下記式1の水酸基を持つ炭素原子に1原子の水素が結合をしているものを言い、ゲルベアルコールとは、下記式2の水酸基を持つ炭素原子に2原子の水素が結合をしているものを言う。
The present invention will be specifically described below.
Surface activity having one or two hydrophilic groups selected from ethylene oxide residues and propylene oxide residues of the present invention and having a branched saturated or unsaturated carbon chain having 8 to 14 carbon atoms as a hydrophobic group The blending amount of the surfactant in the abrasive-containing detergent obtained by blending the agent is not particularly limited.
As the hydrophobic group of the surfactant, a secondary alcohol having 8 to 14 carbon atoms or Gerve alcohol is excellent in terms of detergency, skin irritation and biodegradability. The second alcohol here refers to one in which one atom of hydrogen is bonded to the carbon atom having the hydroxyl group of the following formula 1, and Gerve alcohol is two atoms to the carbon atom having the hydroxyl group of the following formula 2. The hydrogen is bonded.
一方、界面活性剤の親水基のエチレンオキシド残基及びプロピレンオキサイド残基の全平均付加モル数が1モル以上であれば洗浄力、皮膚刺激性、生分解性の点で優れている。エチレンオキシド残基及びプロピレンオキサイド残基から選ばれる1種または2種の全平均付加モル数の上限は特に限定されるものでないが50モル以下が好ましい。更に好ましくはエチレンオキシド残基とプロピレンオキサイド残基の全平均付加モル数が、それぞれ30モル以下であれば好ましい。
本発明の界面活性剤は特に限定されるものでないが、例えばポリオキシエチレン(2モル)アルキルエーテル(アルキル:C14の2級アルコール)、ポリオキシエチレン(30モル)アルキルエーテル(アルキル:C8のゲルベアルコール)、ポリオキシエチレン(6モル)ポリオキシプロピレン(2モル)アルキルエーテル(アルキル:C10のゲルベアルコール)、ポリオキシエチレン(10モル)ポリオキシプロピレン(10モル)アルキルエーテル(アルキル:C12の2級アルコール)等を挙げる事が出来る。特に、ポリオキシエチレン(以下POEと略す)(6)ポリオキシプロピレン(以下POPと略す)(2)アルキルエーテル(アルキル:C10のゲルベアルコール):第一工業製薬株式会社製ノイゲンXL−60やPOE(8)POP(2)アルキルエーテル(アルキル:C10のゲルベアルコール):第一工業製薬株式会社製ノイゲンXL−80、
POE(9)アルキルエーテル(アルキル:C12の2級アルコール):株式会社日本
触媒社製ソフタノール90、POE(7)アルキルエーテル(アルキル:C12の2級アルコール):株式会社日本触媒社製ソフタノール70、それらを組み合わせる等が好ましい。
On the other hand, when the total average number of added moles of ethylene oxide residue and propylene oxide residue of the hydrophilic group of the surfactant is 1 mol or more, it is excellent in terms of detergency, skin irritation and biodegradability. The upper limit of the total average number of added moles of one or two selected from ethylene oxide residues and propylene oxide residues is not particularly limited, but is preferably 50 moles or less. More preferably, the total average number of added moles of ethylene oxide residue and propylene oxide residue is 30 mol or less, respectively.
The surfactant of the present invention is not particularly limited. For example, polyoxyethylene (2 mol) alkyl ether (alkyl: secondary alcohol of C14), polyoxyethylene (30 mol) alkyl ether (alkyl: C8 gel) Alcohol), polyoxyethylene (6 mol) polyoxypropylene (2 mol) alkyl ether (alkyl: C10 Gerve alcohol), polyoxyethylene (10 mol) polyoxypropylene (10 mol) alkyl ether (alkyl: C12 2 Grade alcohol). In particular, polyoxyethylene (hereinafter abbreviated as POE) (6) polyoxypropylene (hereinafter abbreviated as POP) (2) alkyl ether (alkyl: C10 gel alcohol): Daigen XL-60 or POE manufactured by Daiichi Kogyo Seiyaku Co., Ltd. (8) POP (2) alkyl ether (alkyl: C10 Gerve alcohol): Neugen XL-80 manufactured by Daiichi Kogyo Seiyaku Co., Ltd.
POE (9) alkyl ether (alkyl: C12 secondary alcohol): Nippon Shokubai Co., Ltd. Softanol 90, POE (7) alkyl ether (alkyl: C12 secondary alcohol): Nippon Shokubai Co., Ltd. Softanol 70, It is preferable to combine them.
また、本発明の固体表面とは日常生活していると汚れが付着する固体表面の事を言う。例えば、ステンレスや机、樹脂、陶器、人工大理石、フローリング、眼鏡のフレームやレンズ、電話機、ガラス、レザー、材木、毛髪を含む人体、皮膚、動物、金属等である。特に好ましいのは人体の皮脂や手指に付着した切削油やグリース類、土汚れ、カーボン等の汚れを落とすのに適している。
本発明に使用される研磨剤は常温(25℃)で固体のものであれば何でも良く特に限定されるものでなくポリエチレンやポリビニルアルコール等の有機系、無水ケイ酸や酸化アルミニウム等の無機系、結晶セルロースやキトサン等の高分子類、ポリ乳酸やポリブチレンサクシネート等の生分解性研磨剤、コットンやレーヨン等の繊維、食塩や砂糖等の食品調味料等であれば何でも良い。特にカサ比重が小さい研磨剤はグリース類の汚れに対する洗浄力が高い。また、コットン類やアミノ酸類は皮膚に対する刺激を抑制する。例えば、ティコナジャパン株式会社製のGUR2122や旭化成ケミカルズ社製のセオラスTG−101、発泡スチロールや中空粒子等、それらの組合せ等が特に好ましい。
一方、本発明の研磨剤含有洗浄剤は、発明の効果を阻害しない範囲において通常洗浄等等に用いられる界面活性剤や溶剤、油脂類、その他添加剤等を配合する事が出来る。
Further, the solid surface of the present invention refers to a solid surface to which dirt adheres in daily life. For example, stainless steel, desk, resin, earthenware, artificial marble, flooring, glasses frame and lens, telephone, glass, leather, timber, human body including hair, skin, animals, metal, and the like. It is particularly preferable to remove dirt such as cutting oil and grease adhering to human body sebum and fingers, dirt, carbon and the like.
The abrasive used in the present invention is not particularly limited as long as it is solid at room temperature (25 ° C.), and is organic, such as polyethylene and polyvinyl alcohol, inorganic such as silicic anhydride and aluminum oxide, Any polymer such as crystalline cellulose and chitosan, biodegradable abrasives such as polylactic acid and polybutylene succinate, fibers such as cotton and rayon, and food seasonings such as salt and sugar may be used. In particular, an abrasive having a low specific gravity has a high detergency against grease stains. Cottons and amino acids suppress irritation to the skin. For example, GUR2122 manufactured by Ticona Japan Co., Ltd., Theolas TG-101 manufactured by Asahi Kasei Chemicals Co., Ltd., polystyrene foam, hollow particles, and combinations thereof are particularly preferable.
On the other hand, the abrasive-containing cleaning agent of the present invention can be blended with surfactants, solvents, fats and oils, other additives, etc. that are usually used for cleaning and the like within a range that does not impair the effects of the invention.
例えば陽イオン性界面活性剤としてはステアリン酸ジエチルアミノエチルアミド等の脂肪族アミン塩、塩化アルキルトリメチルアンモニウム、臭化アルキルトリメチルアンモニウム、アルキルトリメチルアンモニウムサッカリン、塩化ジポリオキシエチレンアルキルメチルアンモニウム等のアルキル4級アンモニウム、塩化アルキルジメチルベンジルアンモニウム、塩化ラウリルピジニウム、塩化アルキルジメチル(エチルベンジル)アンモニウム等の環式4級アンモニウム塩等が挙げられる。この中でも特に好ましいカチオン系界面活性剤として塩化アルキルトリメチルアンモニウム、臭化アルキルトリメチルアンモニウム、アルキルトリメチルアンモニウムサッカリン、塩化ジポリオキシエチレンアルキルメチルアンモニウム等のアルキル4級アンモニウム、塩化アルキルジメチルベンジルアンモニウム、塩化ラウリルピジニウム、塩化アルキルジメチル(エチルベンジル)アンモニウム等の環式4級アンモニウム塩等を挙げる事ができる。
両イオン性界面活性剤としてはラウリルジアミノエチルグリシンナトリウム、塩化アルキルジアミノエチルグリシン、ヤシ油脂肪酸アシル−N−カルボキシエトキシエチル−N−カルボキシエチルエチレンジアミン2ナトリウム等のグリシン型両性界面活性剤、ヤシ油脂肪酸アシル−N−ヒドロキシエチルエチレンジアミンナトリウム等のラウリルアミノプロピオン酸塩等のアミノプロピオン酸型両性両性界面活性剤、アルキルジメチルアミノ酢酸ベタイン、アルキルジメチルベタインナトリウム、ヤシ油脂肪酸アミドプロピルベタインラウリン酸アミドプロピル酢酸ベタイン等のアミノ酢酸ベタイン型両性界面活性剤、ラウリルヒドロキシスルホベタイン等のスルホベタイン型両性界面活性剤等が挙げられる。この中でも特に好ましい両性界面活性剤としてラウリルジアミノエチルグリシンナトリウム、塩化アルキルジアミノエチルグリシン、ヤシ油脂肪酸アシル−N−カルボキシエトキシエチル−N−カルボキシエチルエチレンジアミン2ナトリウム等のグリシン型両性界面活性剤、ヤシ油脂肪酸アシル−N−ヒドロキシエチルエチレンジアミンナトリウム等のラウリルアミノプロピオン酸塩等のアミノプロピオン酸型両性両性界面活性剤、アルキルジメチルアミノ酢酸ベタイン、アルキルジメチルベタインナトリウム、ヤシ油脂肪酸アミドプロピルベタインラウリン酸アミドプロピル酢酸ベタイン等のアミノ酢酸ベタイン型両性界面活性剤等を挙げる事ができる。
Examples of cationic surfactants include aliphatic amine salts such as diethylaminoethyl amide stearate, alkyl quaternary compounds such as alkyltrimethylammonium chloride, alkyltrimethylammonium bromide, alkyltrimethylammonium saccharin, and dipolyoxyethylene alkylmethylammonium chloride. Examples thereof include cyclic quaternary ammonium salts such as ammonium, alkyldimethylbenzylammonium chloride, laurylpyridinium chloride, and alkyldimethyl (ethylbenzyl) ammonium chloride. Among these, particularly preferred cationic surfactants are alkyl quaternary ammonium such as alkyl trimethyl ammonium chloride, alkyl trimethyl ammonium bromide, alkyl trimethyl ammonium saccharin, dipolyoxyethylene alkyl methyl ammonium chloride, alkyl dimethyl benzyl ammonium chloride, lauryl pyridine. And cyclic quaternary ammonium salts such as ammonium and alkyldimethyl (ethylbenzyl) ammonium chloride.
Examples of amphoteric surfactants include lauryl diaminoethyl glycine sodium, alkyl diaminoethyl glycine chloride, coconut oil fatty acid acyl-N-carboxyethoxyethyl-N-carboxyethyl ethylenediamine disodium glycine type amphoteric surfactant, coconut oil fatty acid Aminoampionic amphoteric surfactants such as laurylaminopropionate such as acyl-N-hydroxyethylethylenediamine sodium, alkyldimethylaminoacetic acid betaine, sodium alkyldimethylbetaine, coconut oil fatty acid amidopropyl betaine lauric acid amidopropyl acetate betaine Examples include aminoacetic acid betaine type amphoteric surfactants such as, and sulfobetaine type amphoteric surfactants such as lauryl hydroxysulfobetaine. Of these, particularly preferred amphoteric surfactants are glycine-type amphoteric surfactants such as sodium lauryldiaminoethylglycine, alkyldiaminoethylglycine chloride, coconut oil fatty acid acyl-N-carboxyethoxyethyl-N-carboxyethylethylenediamine disodium, and palm oil. Aminoampionic amphoteric surfactants such as fatty acid acyl-N-hydroxyethylethylenediamine sodium and other laurylaminopropionates, alkyldimethylaminoacetic acid betaines, sodium alkyldimethylbetaine, coconut oil fatty acid amidopropyl betaine lauric acid amide propylacetic acid Examples include aminoacetic acid betaine-type amphoteric surfactants such as betaine.
陰イオン性界面活性剤としてはポリオキシエチレンアルキルエーテル酢酸及びその塩等のアルキルエーテルカルボン酸型アニオン系界面活性剤、N−アシルサルコシン塩、N−
アシルグルタミン酸塩、N−アシルアルキルタウリン塩等のN−アシル有機酸塩型アニオン系界面活性剤、α―オレフィンスルホン酸塩、アルキルスルホコハク酸塩等のスルホン酸塩型アニオン系界面活性剤、アルキル硫酸エステル塩等の硫酸塩型アニオン系界面活性剤、ポリオキシエチレンアルキルエーテルリン酸塩等のリン酸塩型アニオン系界面活性剤、ポリオキシエチレンラウリルエーテル硫酸ナトリウム等のポリオキシエチレンアルキルエーテル硫酸塩類等が挙げられる。この中でも特に好ましいアニオン系界面活性剤はとしてポリオキシエチレンアルキルエーテル酢酸及びその塩等のアルキルエーテルカルボン酸型アニオン系界面活性剤、N−アシルグルタミン酸塩、N−アシルアルキルタウリン塩等のN−アシル有機酸塩型アニオン系界面活性剤、ポリオキシエチレンラウリルエーテル硫酸ナトリウム等のポリオキシエチレンアルキルエーテル硫酸塩類等を挙げる事ができる。
Anionic surfactants include alkyl ether carboxylic acid type anionic surfactants such as polyoxyethylene alkyl ether acetic acid and its salts, N-acyl sarcosine salts, N-
N-acyl organic acid salt type anionic surfactants such as acyl glutamate and N-acyl alkyl taurate salt, sulfonic acid salt type anionic surfactants such as α-olefin sulfonate and alkyl sulfosuccinate, alkyl sulfate Sulfate-type anionic surfactants such as ester salts, phosphate-type anionic surfactants such as polyoxyethylene alkyl ether phosphates, polyoxyethylene alkyl ether sulfates such as sodium polyoxyethylene lauryl ether sulfate, etc. Is mentioned. Among these, particularly preferred anionic surfactants include alkyl ether carboxylic acid type anionic surfactants such as polyoxyethylene alkyl ether acetic acid and its salts, N-acyl such as N-acyl glutamate and N-acyl alkyl taurate. Examples thereof include organic acid salt type anionic surfactants and polyoxyethylene alkyl ether sulfates such as sodium polyoxyethylene lauryl ether sulfate.
非イオン性界面活性剤としてはレシチン、高分子乳化剤、グリセリン脂肪酸エステル、親油型モノステアリン酸グリセリン等のグリセリン脂肪酸エステル類、モノオレイン酸ポリグリセリル、ペンタオレイン酸ポリグリセリル、デカオレイン酸ポリグリセリル等のポリグリセリン脂肪酸エステル類、モノステアリン酸ポリオキシエチレングリセリン等のポリオキシエチレングリセリン脂肪酸エステル類、モノラウリン酸ソルビタン、モノオレイン酸ソルビタン、トリオレイン酸ソルビタン等のソルビタン脂肪酸エステル類、モノステアリン酸ポリオキシエチレンソルビタン、トリオレイン酸ポリオキシエチレンソルビタン等のポリオキシエチレンソルビタン脂肪酸エステル類、モノラウリン酸ポリオキシエチレンソルビット、テトラオレイン酸ポリオキシエチレンソルビット等のポリオキシエチレンソルビット脂肪酸エステル類、ポリオキシエチレンラノリン、ポリオキシエチレンソルビットミツロウ等のポリオキシエチレンラノリン・ラノリンアルコール・ミツロウ誘導体、ポリオキシエチレンヒマシ油、ポリオキシエチレン硬化ヒマシ油等のポリオキシエチレンヒマシ油・硬化ヒマシ油類、ポリオキシエチレンコレスタノールエーテル等のポリオキシエチレンステロール・水素添加ステロール類、モノステアリン酸エチレングリコール、モノオレイン酸ポリエチレングリコール等のポリエチレングリコール脂肪酸エステル類、ポリオキシエチレンラウリルエーテル、ポリオキシエチレンセチルエーテル、ポリオキシエチレンベヘニルエーテル等のポリオキシエチレンアルキルエーテル類、ポリオキシエチレンポリオキシプロピレンセチルエーテル、ポリオキシエチレンポリオキシプロピレンデシルテトラデシルエーテル等のポリオキシエチレンポリオキシプロピレンアルキルエーテル類、ポリオキシエチレンノニルフェニルエーテル等のポリオキシエチレンアルキルフェニルエーテル類、ポリオキシエチレンステアリン酸アミド等のポリオキシエチレンアルキルアミン・脂肪酸アミド類、ショ糖脂肪酸エステル、アルキルグルコシド等を挙げる事ができる。この中でも特に好ましいノニオン系界面活性剤としてレシチン、グリセリン脂肪酸エステル、親油型モノステアリン酸グリセリン等のグリセリン脂肪酸エステル類、モノオレイン酸ポリグリセリル、ペンタオレイン酸ポリグリセリル、デカオレイン酸ポリグリセリル等のポリグリセリン脂肪酸エステル類、モノラウリン酸ソルビタン、モノオレイン酸ソルビタン、トリオレイン酸ソルビタン等のソルビタン脂肪酸エステル類、ショ糖脂肪酸エステル、アルキルグルコシド等を挙げる事ができる。
これらの界面活性剤は1種単独あるいは2種以上と組み合わせて用いる事ができる。
Nonionic surfactants include lecithin, polymer emulsifiers, glycerin fatty acid esters, glycerin fatty acid esters such as lipophilic glyceryl monostearate, polyglyceryl fatty acids such as polyglyceryl monooleate, polyglyceryl pentaoleate, and polyglyceryl dekaoleate. Esters, polyoxyethylene glycerin fatty acid esters such as polyoxyethylene glyceryl monostearate, sorbitan fatty acid esters such as sorbitan monolaurate, sorbitan monooleate, sorbitan trioleate, polyoxyethylene sorbitan monostearate, triolein Polyoxyethylene sorbitan fatty acid esters such as polyoxyethylene sorbitan acid, polyoxyethylene sorbitol monolaurate, tetraolein Polyoxyethylene sorbite fatty acid esters such as polyoxyethylene sorbitol, polyoxyethylene lanolin, polyoxyethylene lanolin alcohol and beeswax derivatives such as polyoxyethylene lanolin, beeswax, polyoxyethylene castor oil, polyoxyethylene hydrogenated castor oil, etc. Polyoxyethylene castor oil / hardened castor oil, polyoxyethylene sterols / hydrogenated sterols such as polyoxyethylene cholestanol ether, polyethylene glycol fatty acid esters such as polyethylene glycol monostearate and polyethylene glycol monooleate, poly Polyoxyethylene alkyl ethers such as oxyethylene lauryl ether, polyoxyethylene cetyl ether and polyoxyethylene behenyl ether Tellurium, polyoxyethylene polyoxypropylene cetyl ether, polyoxyethylene polyoxypropylene decyl tetradecyl ether and other polyoxyethylene polyoxypropylene alkyl ethers, polyoxyethylene nonylphenyl ether and other polyoxyethylene alkylphenyl ethers, Examples include polyoxyethylene alkylamine / fatty acid amides such as polyoxyethylene stearamide, sucrose fatty acid esters, alkyl glucosides, and the like. Among these, particularly preferred nonionic surfactants include glycerin fatty acid esters such as lecithin, glycerin fatty acid ester, lipophilic glyceryl monostearate, polyglyceryl fatty acid esters such as polyglyceryl monooleate, polyglyceryl pentaoleate, and polyglyceryl dekaoleate. And sorbitan fatty acid esters such as sorbitan monolaurate, sorbitan monooleate and sorbitan trioleate, sucrose fatty acid esters, alkyl glucosides and the like.
These surfactants can be used alone or in combination of two or more.
本発明に使用できる溶剤として低級アルコールは炭素数1〜4の水溶性アルコール類であり具体的にはメタノール、エタノール、プロパノール、イソプロピルアルコール、2−メトキシエタノール、2−エトキシエタノール、2−メトキシプロパノール、2−メトキシイソプロパノール等のモノオール類やエチレングリコール、プロピレングリコール、1,3―プロパンジオール、2,3−ブタンジオール、1,2−ブタンジオール、1,3−ブタンジオール、1,4−ブタンジオール、2−メチルー1、2−プロパンジオール、ジエチレングリコール、1,4−ブチンジオール等のジオール類やグリセリン、1,2,4−ブタントリオール、エリスリトール等のポリオールが挙げられる。
これらの低級アルコールは1種単独あるいは2種以上と組み合わせて用いる事ができる
。
As the solvent that can be used in the present invention, the lower alcohol is a water-soluble alcohol having 1 to 4 carbon atoms, specifically, methanol, ethanol, propanol, isopropyl alcohol, 2-methoxyethanol, 2-ethoxyethanol, 2-methoxypropanol, Monools such as 2-methoxyisopropanol, ethylene glycol, propylene glycol, 1,3-propanediol, 2,3-butanediol, 1,2-butanediol, 1,3-butanediol, 1,4-butanediol Diols such as 2-methyl-1,2-propanediol, diethylene glycol and 1,4-butynediol, and polyols such as glycerin, 1,2,4-butanetriol and erythritol.
These lower alcohols can be used alone or in combination of two or more.
本発明に併用しうる成分として炭酸カルシウム、タルク、マイカ、カオリン、ラウロイルリジン、二酸化チタン、二酸化亜鉛等の粉末成分;ホホバ油、マカデミアナッツ油、アボガド油、月見草油、ミンク油、ナタネ油、ヒマシ油、ヒマワリ油、トーモロコシ油、カカオ油、ヤシ油、コメヌカ油、オリーブ油、アーモンド油、ごま油、サフラワー油、大豆油、椿油、パーシック油、ヒマシ油、ミンク油、綿実油、モクロウ、パーム油、パーム核油、卵黄油、ラノリン、スクワレン等の天然動植物油脂類、合成トリグリセライド;スクワラン、流動パラフィン、ワセリン、セレシン、マイクロクリスタリンワックス、イソパラフィン等の炭化水素類;カルナバウロウ、パラフィンワックス、鯨ロウ、ミツロウ、キヤンデリラワックス、ラノリン等のワックス類;セタノール、ステアリルアルコール、ラウリルアルコール、セトステアリルアルコール、オレイルアルコール、ベヘニルアルコール、ラノリンアルコール、水添ラノリンアルコール、ヘキシルデカノール、オクチルドデカノール等の高級アルコール類;ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘニン酸、イソステアリン酸、オレイン酸、リノレン酸、リノール酸、オキシステアリン酸、ウンデシレン酸、ラノリン脂肪酸、硬質ラノリン脂肪酸、軟質ラノリン脂肪酸等の高級脂肪酸類;コレステリル−オクチルドデシル−ベヘニル等のコレステロールおよびその誘導体;イソプロピルミリスチン酸、イソプロピルパルミチン酸、イソプロピルステアリン酸、2エチルヘキサン酸グリセロール、ブチルステアリン酸、リノール酸エチル等のエステル類;ジエチレングリコールモノプロピルエーテル、ポリオキシエチレンポリオキシプロピレンペンタエリトリトールエーテル、ポリオキシプロピレンブチルエーテル等の極性オイル;その他、メチルフェニルポリシロキサン、メチルポリシロキサン、オクタメチルシクロテトラシロキサン、デカメチルシクロペンタシロキサン、ドデカメチルシクロヘキサシロキサン、メチルシクロポリシロキサン、オクタメチルトリシロキサン、デカメチルテトラシロキサン、ポリオキシエチレン・メチルポリシロキサン共重合体、ポリオキシプロピレン・メチルポリシロキサン共重合体、ポリ(オキシエチレン・オキシプロピレン)メチルポリシロキサン共重合体、メチルハイドロジェンポリシロキサン、テトラヒドロテトラメチルシクロテトラシロキサン、ステアロキシメチルポリシロキサン、セトキシメチルポリシロキサン、メチルポリシロキサンエマルション、高重合メチルポリシロキサン(1)および(2)、トリメチルシロキシケイ酸、架橋型メチルポリシロキサン、架橋型メチルフェニルポリシロキサン、架橋型メチルフェニルポリシロキサン、架橋型メチルフェニルポリシロキサン(2)等、更にはアミノ変性シリコーン、エポキシ変性シリコーン、カルボキシル変性シリコーン、カルビノール変性シリコーン、メタクリル変性シリコーン、メルカプト変性シリコーン、フェノール変性シリコーン、片末端反応性シリコーン、異種官能基変性シリコーン、ポリエーテル変性シリコーン、メチルスチリル変性シリコーン、アルキル変性シリコーン、高級脂肪酸エステル変性シリコーン、親水性特殊変性シリコーン、高級アルコキシ変性シリコーン、高級脂肪酸含有シリコーン、フッ素変性シリコーン等の各種誘導体を含むシリコーン類;を挙げることが出来る。 Powder components such as calcium carbonate, talc, mica, kaolin, lauroyl lysine, titanium dioxide, zinc dioxide as components that can be used in the present invention; jojoba oil, macadamia nut oil, avocado oil, evening primrose oil, mink oil, rapeseed oil, castor oil , Sunflower oil, corn oil, cacao oil, palm oil, rice bran oil, olive oil, almond oil, sesame oil, safflower oil, soybean oil, coconut oil, persic oil, castor oil, mink oil, cottonseed oil, owl, palm oil, palm kernel Oils, egg yolk oil, lanolin, squalene and other natural animal and vegetable oils, synthetic triglycerides; Squalane, liquid paraffin, petrolatum, ceresin, microcrystalline wax, isoparaffins and other hydrocarbons; carnauba wax, paraffin wax, sperm Wax, lanolin Waxes: higher alcohols such as cetanol, stearyl alcohol, lauryl alcohol, cetostearyl alcohol, oleyl alcohol, behenyl alcohol, lanolin alcohol, hydrogenated lanolin alcohol, hexyl decanol, octyldodecanol; lauric acid, myristic acid, palmitic acid, stearin Higher fatty acids such as acid, behenic acid, isostearic acid, oleic acid, linolenic acid, linoleic acid, oxystearic acid, undecylenic acid, lanolin fatty acid, hard lanolin fatty acid, soft lanolin fatty acid; cholesterol such as cholesteryl-octyldodecyl-behenyl and Derivatives thereof: isopropyl myristic acid, isopropyl palmitic acid, isopropyl stearic acid, glycerol 2-ethylhexanoate, butyl stearate Esters such as phosphoric acid and ethyl linoleate; polar oils such as diethylene glycol monopropyl ether, polyoxyethylene polyoxypropylene pentaerythritol ether, polyoxypropylene butyl ether; and others, methylphenyl polysiloxane, methyl polysiloxane, octamethylcyclotetra Siloxane, Decamethylcyclopentasiloxane, Dodecamethylcyclohexasiloxane, Methylcyclopolysiloxane, Octamethyltrisiloxane, Decamethyltetrasiloxane, Polyoxyethylene / methylpolysiloxane copolymer, Polyoxypropylene / methylpolysiloxane copolymer , Poly (oxyethylene oxypropylene) methyl polysiloxane copolymer, methyl hydrogen polysiloxane, tetrahy Drotetramethylcyclotetrasiloxane, stearoxymethylpolysiloxane, cetoxymethylpolysiloxane, methylpolysiloxane emulsion, highly polymerized methylpolysiloxane (1) and (2), trimethylsiloxysilicic acid, crosslinked methylpolysiloxane, crosslinked Methylphenyl polysiloxane, cross-linked methylphenyl polysiloxane, cross-linked methylphenyl polysiloxane (2), and the like, amino-modified silicone, epoxy-modified silicone, carboxyl-modified silicone, carbinol-modified silicone, methacryl-modified silicone, mercapto-modified silicone, Phenol-modified silicone, one-end reactive silicone, heterogeneous functional group-modified silicone, polyether-modified silicone, methylstyryl-modified silicone, alkyl-modified silicone Emissions, higher fatty acid ester modified silicone, hydrophilic special modified silicone, higher alkoxy-modified silicones, higher fatty acid-containing silicone, silicones containing various derivatives and fluorine-modified silicone; can be exemplified.
また、その他添加剤としてパラアミノ安息香酸およびその誘導体、ホモメチル−7N−アセチルアラントイラニレート、ブチルメトキシベンゾイルメタン、ジ−パラメトキシケイ皮酸ーモノー2ーエチルヘキサン酸グリセリル、オクチルシンナメート等のパラメトキシケイ皮酸誘導体、アミルサリシレート等のサリチル酸誘導体、2,4−ジヒドロキシベンゾフェノン等のベンゾフェノン誘導体、ジメトキシベンジリデンジオキソイミダゾリンプロピオン酸エチルヘキシル、酢酸液状ラノリン、コガネバナ根抽出エキス、トリアニリノ−p−カルボエチルヘキシルオキシ−トリアジン等の紫外線吸収剤;アルブチン、コウジ酸、リン酸アスコルビン酸マグネシウムなどのアスコルビン酸およびその誘導体、グルタチオン、甘草エキス、チョウジエキス、茶抽出物、アスタキサンチン、牛胎盤エキス、トコフェロールおよびその誘導体、トラネキサム酸およびその塩、アズレン、γ−ヒドロキシ酪酸等の美白成分;マルチトール、ソルビトール、グリセリン、プロピレングリコー
ル、1,3−ブチレングリコール、ポリエチレングリコール、グリコール等の多価アルコール、ピロリドンカルボン酸ソーダ、乳酸ソーダ、クエン酸ソーダなど有機酸およびその塩、ヒアルロン酸ソーダなどヒアルロン酸およびその塩、酵母および酵母抽出液の加水分解物、酵母培養液、乳酸菌培養液など醗酵代謝産物;エチレンジアミン四酢酸およびその塩類、ヒドロキシエチレンジアミン3酢酸およびその塩類、リン酸、アスコルビン酸、コハク酸、グルコン酸、ポリリン酸塩類、メタリン酸塩類などの金属イオン封鎖剤;ブチルヒドロキシトルエン、トコフェロール、フィチン酸等の酸化防止剤;安息香酸、安息香酸ナトリウム、ウンデレン酸、サリチル酸、ソルビン酸、ソルビン酸カリウム、デヒドロ酢酸、デヒドロ酢酸ナトリウム、パラオキシ安息香酸エステル類及びその塩等の有機酸及びその誘導体、イソプロピルメチルフェノール、グルコン酸クロルヘキシジン、クレゾール、クロロチモール、クロロフェネシン、クロロクレゾール、ジクロロキシレノール、ジクロロベンジルアルコール、チオビスクロロフェノール、チモール、トリクロロカルバニリド、トリクロロヒドロキシジフェニルエーテル、ナトリウムフェノキシド、パラクロロフェノール、ハロカルバン、フェニルエチルアルコール、フェニルフェノール、フェニルフェノールナトリウム、フェノキシエタノール、フェノール、フェキサクロロフェン、ベンジルアルコール等のフェノール類、塩化ステアリルジメチルベンジルアルコール、塩化ステアリルトリメチルアンモニウム、塩化セチルトリメチルアンモニウム、塩化ベンザルコニウム、塩化セチルピリジウム、塩化ベンゼトニウム、塩化メチルベンゼトニウム、塩化ラウリルトリメチルアンモニウム、塩化ラウリルピリジニウム、塩化ラウロイルコラミノホルミルメチルピリジニウム、臭化アルキルイソキノリニウム、臭化セチルトリメチルアンモニウム、臭化ドミフェン、臭化ラウリルトリメチルアンモニウム、セチルトリメチルアンモニウムサッカリン等の4級アンモニウム塩、塩酸アルキルジアミノエチルグリシン等の両性界面活性剤、プラトニン、ピオニン、ルミネキス、感光素NK143等の感光素、茶エキス、ヒノキキチオール、リンゴエキス、ポリリジン等の抗菌活性を持つ植物抽出液、その他グルタラール、クロラミンT、クロルヘキシジン、ジイセチオン酸ジプロモプロパミジン、ジンクピリチオン、トリクロサン、ピリチオンNa、フルフラール、クロラミンT等が挙げられる。この中でも特に好ましい防腐剤として安息香酸及びその塩、サリチル酸、ソルビン酸、ソルビン酸カリウム、デヒドロ酢酸、デヒドロ酢酸ナトリウム、パラオキシ安息香酸エステル類、塩化セチルピリジウム、塩化ステアリルジメチルベンジルアンモニウム、茶エキス、ヒノキキチオール、リンゴエキス、ポリリジン、トリクロサン等の抗菌・防腐剤;αトコフェロール、βトコフェロール、γトコフェロール等のビタミンE類、ビタミンD類、ビタミンH、パントテン酸等のビタミン類;ニコチン酸アミド、ニコチン酸ベンジル、γ−オリザノール、アラントイン、グリチルリチン酸(塩)グリチルレチン酸およびその誘導体、ヒノキチオール、ムシジン、ビサボロール、ユーカリプトール、チモールイノシトール、サポニン類(キラヤサポニン、アズキサポニン、ヘチマサポニン等)トラネキサム酸、パントテルエチルエーテル、エチニルエストラジオール、セファランジン、プラセンタエキス、センブリエキス、セファランチン、ビタミンEおよびその誘導体、ガンマーオリザノールなどの血行促進剤;トウガラシチンキ、ショオウキョウチンキ、カンタリスチンキ、ニコチン酸ベンジルエステルなどの局所刺激剤、各種ビタミンやアミノ酸などの栄養剤、グリチルレチン酸、グリチルリチン酸誘導体、アラントイン、アズレン、アミノカプロン酸、ヒドロコルチゾンなどの抗炎症剤;酸化亜鉛、硫酸亜鉛、アラントインヒドロキシアルミニウム、塩化アルミニウム、スルホ石炭酸亜鉛、タンニン酸などの収斂剤;メントール、カンフルなどの清涼剤;抗ヒスタミン剤;トコフェロール類、BHA、BHT、没食子酸、NDGAなどの酸化防止剤等の各種薬剤サッカロマイセスなどの酵母、糸状菌、バクテリア、牛胎盤、人胎盤、人臍帯、酵母、牛コラーゲン、牛乳由来蛋白、小麦、大豆、牛血液、ブタ血液、鶏冠、カミツレ、キュウリ、コメ、シアバター、シラカバ、茶、トマト、ニンニク、ハマメリス、バラ、ヘチマ、ホップ、モモ、アンズ、レモン、キウイ、ドクダミ、トウガラシ、クララ、ギシギシ、コウホネ、セージ、ノコギリ草、ゼニアオイ、センキュウ、センブリ、タイム、トウキ、トウヒ、バーチ、スギナ、ヘチマ、マロニエ、ユキノシタ、アルニカ、ユリ、ヨモギ、シャクヤク、アロ
エ、アロエベラ、オウゴン、オウバク、コウカ、ベニバナ、サンシン、シコン、タイソウ、チンピ、ニンジン、ヨクイニン、ハトムギ、クチナシ、サワラ等の動植物・微生物およびその一部から有機溶媒、アルコール、多価アルコール、水、水性アルコール等で抽出または加水分解して得た天然エキス;色素;香料;精製水等を配合することができる。
これらの添加剤は1種単独あるいは2種以上と組み合わせて用いる事ができる。
Other additives include paraaminobenzoic acid and its derivatives, homomethyl-7N-acetylalanthranilate, butylmethoxybenzoylmethane, di-paramethoxycinnamic acid-mono-2-ethylhexanoic acid glyceryl, octylcinnamate, etc. Acid derivatives, salicylic acid derivatives such as amyl salicylate, benzophenone derivatives such as 2,4-dihydroxybenzophenone, dimethoxybenzylidene dioxoimidazoline propionate ethylhexyl, acetic acid liquid lanolin, coganebana root extract extract, trianilino-p-carboethylhexyloxy-triazine, etc. UV absorbers; arbutin, kojic acid, ascorbic acid such as magnesium ascorbate and its derivatives, glutathione, licorice extract, butterfly Whitening ingredients such as extract, tea extract, astaxanthin, bovine placenta extract, tocopherol and its derivatives, tranexamic acid and its salts, azulene, γ-hydroxybutyric acid; maltitol, sorbitol, glycerin, propylene glycol, 1,3-butylene glycol Polyhydric alcohols such as polyethylene glycol and glycol, organic acids and salts thereof such as sodium pyrrolidonecarboxylate, sodium lactate and sodium citrate, hyaluronic acid and salts thereof such as sodium hyaluronate, yeast and yeast extract hydrolysates, yeast Fermentation metabolites such as culture solution, lactic acid bacteria culture solution; ethylenediaminetetraacetic acid and its salts, hydroxyethylenediaminetriacetic acid and its salts, phosphoric acid, ascorbic acid, succinic acid, gluconic acid, polyphosphates, metaphosphates, etc. Sequestering agent; antioxidants such as butylhydroxytoluene, tocopherol, phytic acid; benzoic acid, sodium benzoate, undelenic acid, salicylic acid, sorbic acid, potassium sorbate, dehydroacetic acid, sodium dehydroacetate, paraoxybenzoic acid esters And organic acids and derivatives thereof such as isopropylmethylphenol, chlorhexidine gluconate, cresol, chlorothymol, chlorophenesin, chlorocresol, dichloroxylenol, dichlorobenzyl alcohol, thiobischlorophenol, thymol, trichlorocarbanilide, Trichlorohydroxydiphenyl ether, sodium phenoxide, parachlorophenol, halocarban, phenylethyl alcohol, phenylphenol, phenylphenol Phenols such as sodium chloride, phenoxyethanol, phenol, fexachlorophene, benzyl alcohol, stearyldimethylbenzyl alcohol, stearyltrimethylammonium chloride, cetyltrimethylammonium chloride, benzalkonium chloride, cetylpyridium chloride, benzethonium chloride, methylbenzethonium chloride , Lauryl trimethyl ammonium chloride, lauryl pyridinium chloride, lauroyl colaminoformyl methyl pyridinium chloride, alkyl isoquinolinium bromide, cetyl trimethyl ammonium bromide, domifene, lauryl trimethyl ammonium bromide, cetyl trimethyl ammonium saccharin, etc. Amphoteric surfactants such as ammonium salts and alkyldiaminoethylglycine hydrochloride, platoni , Pionine, Luminekis, Photosensitizers such as Photosensitizer NK143, Plant extracts with antibacterial activity such as tea extract, hinokitiol, apple extract, polylysine, etc., other glutaral, chloramine T, chlorhexidine, dipromopropamidine diisethionate, zinc pyrithione , Triclosan, pyrithione Na, furfural, chloramine T and the like. Of these, benzoic acid and its salts, salicylic acid, sorbic acid, potassium sorbate, dehydroacetic acid, sodium dehydroacetate, paraoxybenzoic acid esters, cetylpyridium chloride, stearyldimethylbenzylammonium chloride, tea extract, cypress Antibacterial and antiseptic agents such as chithiol, apple extract, polylysine, and triclosan; vitamins such as α-tocopherol, β-tocopherol, and γ-tocopherol, vitamins such as vitamin D, vitamin H, and pantothenic acid; nicotinamide, nicotinic acid Benzyl, γ-oryzanol, allantoin, glycyrrhizic acid (salt) glycyrrhetinic acid and its derivatives, hinokitiol, mucidin, bisabolol, eucalyptol, thymol inositol, saponins (Kirayasapo) Blood circulation promoters such as tranexamic acid, pantothel ethyl ether, ethinyl estradiol, cephalandin, placenta extract, assembly extract, cephalanthin, vitamin E and its derivatives, gamma-oryzanol, etc .; red pepper tincture , Cantalis tincture, topical stimulants such as nicotinic acid benzyl ester, nutrients such as various vitamins and amino acids, anti-inflammatory agents such as glycyrrhetinic acid, glycyrrhizic acid derivatives, allantoin, azulene, aminocaproic acid, hydrocortisone; zinc oxide, zinc sulfate Astringents such as allantoin hydroxyaluminum, aluminum chloride, zinc sulfocolate and tannic acid; refreshing agents such as menthol and camphor; antihistamines; Rolls, BHA, BHT, gallic acid, various drugs such as antioxidants such as NDGA, yeast such as Saccharomyces, filamentous fungi, bacteria, cow placenta, human placenta, human umbilical cord, yeast, cow collagen, milk-derived protein, wheat, Soybean, cow blood, pig blood, chicken crown, chamomile, cucumber, rice, shea butter, birch, tea, tomato, garlic, hamamelis, rose, loofah, hop, peach, apricot, lemon, kiwi, dokudami, chili pepper, clara, burrow , Scallop, sage, sawtooth grass, mallow, senkyu, assembly, thyme, spruce, spruce, birch, horsetail, loofah, maronier, yukinoshita, arnica, lily, mugwort, peonies, aloe, aloe vera, ugon, grasshopper, buckwheat Sanshin, Sikon, Taisou, Chimpi, Carrot, Yoku Natural extracts obtained by extraction or hydrolysis from organic solvents, alcohol, polyhydric alcohols, water, aqueous alcohol, etc. from animals and plants / microorganisms such as nin, pearl barley, gardenia, sawara, and parts thereof; pigments; fragrances; purified water, etc. Can be blended.
These additives can be used alone or in combination of two or more.
下記に本発明の実施例を詳細に説明する。
実施例、比較例で使用する原料名(略称)研磨剤名称(略称)は下記の通りである。
POE(6)POP(2)アルキルエーテル(アルキル:C10のゲルベアルコール):第一工業製薬株式会社製ノイゲンXL−60(以下、XL−60と略す)。
POE(8)POP(2)アルキルエーテル(アルキル:C10のゲルベアルコール):第一工業製薬株式会社製ノイゲンXL−80(以下、XL−80と略す)。
POE(9)アルキルエーテル(アルキル:C12の2級アルコール):株式会社日本触媒社製ソフタノール90(以下、ソフタノール90と略す)。
POE(5)POP(2)アルキルエーテル(アルキル:C12の直鎖アルコール):第一工業製薬株式会社製ノイゲンLP−70E(以下、LP−70と略す)。
POE(9)アルキルエーテル(アルキル:C12の直鎖アルコール):日光ケミカルズ株式会社製NIKKOL BL−9EX(以下、BL−9EXと略す)。
POE(7)アルキルエーテル(アルキル:C12〜14の直鎖アルコール):ライオン株式会社製レオックスCC−90(以下、CC−90と略す)
結晶セルロース:旭化成ケミカルズ社製セオラスTG―101L(以下、セオラスと略す)。
ポリエチレン1:ティコナジャパン株式会社製GUR2122(以下、GUR2122と略す)。
ポリエチレン2:ティコナジャパン株式会社製GUR4150(以下、GUR4150と略す)。
ポリエチレン3:旭化成ケミカルズ社製SH810(以下、サンファインと略す)。
発泡スチロール:西日本発泡スチロールリサイクル株式会社製EN2(以下、EN2と略す)。
カルボキシルビニルポリマー:BFGoodrich社製カーボポール941(以下、カーボポール)。
25%W/W水酸化ナトリウム:純正化学株式会社製25%W/W水酸化ナトリウム(以下、25%水酸化Naと略す)。
Examples of the present invention will be described in detail below.
The raw material name (abbreviation) and abrasive name (abbreviation) used in Examples and Comparative Examples are as follows.
POE (6) POP (2) alkyl ether (alkyl: C10 Gerve alcohol): Neugen XL-60 (hereinafter abbreviated as XL-60) manufactured by Daiichi Kogyo Seiyaku Co., Ltd.
POE (8) POP (2) alkyl ether (alkyl: C10 Gerve alcohol): Neugen XL-80 (hereinafter abbreviated as XL-80) manufactured by Daiichi Kogyo Seiyaku Co., Ltd.
POE (9) alkyl ether (alkyl: C12 secondary alcohol): Nippon Shokubai Co., Ltd. Softanol 90 (hereinafter abbreviated as Softanol 90).
POE (5) POP (2) alkyl ether (alkyl: linear alcohol of C12): Neugen LP-70E (hereinafter abbreviated as LP-70) manufactured by Daiichi Kogyo Seiyaku Co., Ltd.
POE (9) alkyl ether (alkyl: linear alcohol of C12): NIKKOL BL-9EX (hereinafter abbreviated as BL-9EX) manufactured by Nikko Chemicals.
POE (7) alkyl ether (alkyl: C12-14 linear alcohol): Lion Corporation Leox CC-90 (hereinafter abbreviated as CC-90)
Crystalline cellulose: Theolas TG-101L (hereinafter abbreviated as Theolas) manufactured by Asahi Kasei Chemicals.
Polyethylene 1: GUR2122 manufactured by Ticona Japan Co., Ltd. (hereinafter abbreviated as GUR2122).
Polyethylene 2: Ticona Japan Co., Ltd. GUR4150 (hereinafter abbreviated as GUR4150).
Polyethylene 3: SH810 manufactured by Asahi Kasei Chemicals (hereinafter abbreviated as “Sun Fine”).
Styrofoam: EN2 manufactured by West Japan Styrofoam Recycle Co., Ltd. (hereinafter abbreviated as EN2).
Carboxyl vinyl polymer: Carbopol 941 (hereinafter, Carbopol) manufactured by BFGoodrich.
25% W / W sodium hydroxide: 25% W / W sodium hydroxide manufactured by Junsei Chemical Co., Ltd. (hereinafter abbreviated as 25% Na hydroxide).
実施例、比較例中で行う性能評価試験方法は下記の通りである。
洗浄力の評価:カーボンブラック(東海カーボン SEAST・KH N−339)1部に対してシリコングリース(信越化学工業株式会社製 HIVAC−G)10部を良く混ぜたものを、5cm四方に切り取った白色の人工皮(ソフトセメリー1003 カラー:1)に0.1gを塗り、その上に洗浄液(研磨剤含有洗浄剤等)を0.5g滴下した後、縦5回横5回縦5回横5回づつ指で洗浄し水道水で洗い流す。人工皮に残ったカーボンブラックの程度を色差計のL値にて判定する。評価基準は下記の通りである。
×:45以下
○:46〜60
◎:61以上
皮膚刺激性の評価:日本白色種ウサギ雄の背部を除毛した健常皮膚部に10%水溶液、0.5mlを2.5cm×2.5cmのリント布に含浸させたものを投与部位に貼付し、24時間閉塞貼付を行い、3,24、48時間後にそれぞれ刺激反応の観察を行いDraize法の判定基準に従って判定する。評価基準は以下の通りである。
一次刺激率が、
◎:0.0未満
○:0.0〜2.0未満
×:2.0以上
環境性(BOD、COD)の評価:界面活性剤あるいは溶剤0.1%水溶液についてJISK0102に準じて行った。
The performance evaluation test methods performed in the examples and comparative examples are as follows.
Evaluation of detergency: White obtained by mixing 10 parts of silicon grease (HIVAC-G manufactured by Shin-Etsu Chemical Co., Ltd.) with 1 part of carbon black (Tokai Carbon SEAST / KH N-339) into 5 cm square 0.1 g of artificial skin (soft semery 1003 color: 1) and 0.5 g of a cleaning solution (abrasive-containing cleaning agent, etc.) are dropped on the artificial skin, then 5 times 5 times 5 times 5 times Rinse with fingers and rinse with tap water. The degree of carbon black remaining on the artificial skin is determined by the L value of the color difference meter. The evaluation criteria are as follows.
×: 45 or less ○: 46-60
◎: 61 or more Evaluation of skin irritation: Administer 10% aqueous solution, 0.5ml impregnated with 2.5cm x 2.5cm lint cloth to healthy skin part where hair of Japanese white rabbit was depilated Affixed to the site, occluded for 24 hours, and observed for stimulation reaction after 3, 24 and 48 hours, respectively, and determined according to the criteria for the Draize method. The evaluation criteria are as follows.
Primary stimulation rate is
◎: Less than 0.0 ○: 0.0 to less than 2.0 ×: 2.0 or more Evaluation of environmental properties (BOD, COD): A surfactant or 0.1% aqueous solution of a solvent was measured according to JISK0102.
[実施例1]
GUR4150:4%とXL−60:12%と精製水とカーボポール941と25%水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し、全体を100%とする。これの性能評価試験結果を表1に示す。
[実施例2]
サンファイン:8%とXL−60:12%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[実施例3]
セオラス:8%とXL−60:12%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[実施例4]
GUR2122:4%とXL−60:12%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[Example 1]
GUR4150: 4%, XL-60: 12%, purified water, carbopol 941, and 25% sodium hydroxide were added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) Is 100%. The performance evaluation test results are shown in Table 1.
[Example 2]
Sun Fine: 8%, XL-60: 12%, purified water, Carbopol 941 and 25% W / W sodium hydroxide added to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) Adjust to 100% overall. The performance evaluation test results are shown in Table 1.
[Example 3]
Theolas: 8%, XL-60: 12%, purified water, carbopol 941, and 25% W / W sodium hydroxide added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) The total is 100%. The performance evaluation test results are shown in Table 1.
[Example 4]
GUR2122: 4%, XL-60: 12%, purified water, carbopol 941, and 25% W / W sodium hydroxide are added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) The total is 100%. The performance evaluation test results are shown in Table 1.
[比較例1]
GUR4150:4%とLP−70:12%と精製水とカーボポール941と25%水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm 2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[比較例2]
サンファイン:8%とLP−70:12%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[比較例3]
EN2:16%とBL−9EX:20%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[比較例4]
セオラス:90%とLP−70:10%とを混合攪拌し錠剤に成型する。これの性能評価試験結果を表1に示す。
[Comparative Example 1]
GUR4150: 4%, LP-70: 12%, purified water, carbopol 941 and 25% sodium hydroxide are added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) Is 100%. The performance evaluation test results are shown in Table 1.
[Comparative Example 2]
Sunfine: 8%, LP-70: 12%, purified water, carbopol 941, and 25% W / W sodium hydroxide added to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) Adjust to 100% overall. The performance evaluation test results are shown in Table 1.
[Comparative Example 3]
EN2: 16%, BL-9EX: 20%, purified water, carbopol 941, and 25% W / W sodium hydroxide added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes) The total is 100%. The performance evaluation test results are shown in Table 1.
[Comparative Example 4]
Theolus: 90% and LP-70: 10% are mixed and stirred to form tablets. The performance evaluation test results are shown in Table 1.
[実施例5]
EN2:16%とソフタノール90:20%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を
表1に示す。
[実施例6]
EN2:4%とソフタノール90:5%と精製水とカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計 NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[実施例7]
セオラス:90%とXL−60:10%とを混合攪拌し錠剤に成型する。これの性能評価試験結果を表1に示す。
[実施例8]
GUR2122:4%とXL−60:12%及びXL−80:4%と精製水をカーボポール941と25%W/W水酸化ナトリウムを添加して3500〜4500cps(B型粘度計NO.4 60rpm2分間)になるように調整し全体を100%とする。これの性能評価試験結果を表1に示す。
[Example 5]
EN2: 16%, Softanol 90: 20%, Purified water, Carbopol 941 and 25% W / W sodium hydroxide are added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes). The whole is 100%. The performance evaluation test results are shown in Table 1.
[Example 6]
EN2: 4%, Softanol 90: 5%, purified water, Carbopol 941, and 25% W / W sodium hydroxide were added to adjust to 3500-4500 cps (B-type viscometer NO.4 60 rpm for 2 minutes). The whole is 100%. The performance evaluation test results are shown in Table 1.
[Example 7]
Theolus: 90% and XL-60: 10% are mixed and stirred to form a tablet. The performance evaluation test results are shown in Table 1.
[Example 8]
GUR2122: 4%, XL-60: 12% and XL-80: 4%, purified water was added to Carbopol 941 and 25% W / W sodium hydroxide, and 3500-4500 cps (B-type viscometer NO.4 60 rpm2 Minutes) to make the whole 100%. The performance evaluation test results are shown in Table 1.
[比較例5]
トリエチレングリコールモノブチルエーテル(一般品)単独の性能評価試験結果を表2に示す。
[比較例6]
トリプロピレングリコールモノメチルエーテル(日本乳化剤株式会社製:MFTG)単独の性能評価試験結果を表2に示す。
[比較例7]
3−メトキシー3−メチルブチルアセテート(株式会社クラレ製:ソルフィットアセテート)単独の性能評価試験結果を表2に示す。
[比較例8]
ブチルグリシジルエーテル(日本油脂株式会社製:エビオールB)単独の性能評価試験結果を表2に示す。
[比較例9]
エチレングリコールモノメチルエーテル(一般品)単独の性能評価試験結果を表2に示す。
[比較例10]
CC−90単独の性能評価試験結果を表2に示す。
[実施例9]
XL−60単独の性能評価試験結果を表2に示す。
[実施例10]
ソフタノール90単独の性能評価試験結果を表2に示す。
[Comparative Example 5]
Table 2 shows the performance evaluation test results of triethylene glycol monobutyl ether (general product) alone.
[Comparative Example 6]
Table 2 shows the performance evaluation test results of tripropylene glycol monomethyl ether (manufactured by Nippon Emulsifier Co., Ltd .: MFTG) alone.
[Comparative Example 7]
Table 2 shows the performance evaluation test results of 3-methoxy-3-methylbutyl acetate (manufactured by Kuraray Co., Ltd .: Solfit Acetate) alone.
[Comparative Example 8]
Table 2 shows the performance evaluation test results of butyl glycidyl ether (Nippon Yushi Co., Ltd .: Eviol B) alone.
[Comparative Example 9]
Table 2 shows the results of performance evaluation tests for ethylene glycol monomethyl ether (general product) alone.
[Comparative Example 10]
The performance evaluation test results of CC-90 alone are shown in Table 2.
[Example 9]
Table 2 shows the performance evaluation test results of XL-60 alone.
[Example 10]
Table 2 shows the results of the performance evaluation test for Softanol 90 alone.
本発明は、切削油や粘度の高いグリース類、人体に付着した皮脂、土汚れ、カーボンブラック等の頑固な汚れを除去する研磨剤含有洗浄剤として最適である。 The present invention is optimal as an abrasive-containing cleaning agent that removes stubborn dirt such as cutting oil, high-viscosity grease, sebum adhering to the human body, soil dirt, and carbon black.
Claims (5)
The abrasive-containing cleaning agent according to any one of claims 1 to 4, which is used for cleaning fingers.
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JP2010150403A (en) * | 2008-12-25 | 2010-07-08 | Kao Corp | Method for manufacturing detergent composition for hard surface |
JP2013536281A (en) * | 2010-08-17 | 2013-09-19 | ザ プロクター アンド ギャンブル カンパニー | Method for hand-washing dishes with persistent foam |
EP2625236A4 (en) * | 2010-10-07 | 2014-05-14 | Basf Se | Aqueous polishing composition and process for chemically mechanically polishing substrates having patterned or unpatterned low-k dielectric layers |
WO2021199723A1 (en) * | 2020-03-31 | 2021-10-07 | 株式会社フジミインコーポレーテッド | Polishing composition |
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WO2021199723A1 (en) * | 2020-03-31 | 2021-10-07 | 株式会社フジミインコーポレーテッド | Polishing composition |
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