IN2014KN00962A - - Google Patents

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Publication number
IN2014KN00962A
IN2014KN00962A IN962KON2014A IN2014KN00962A IN 2014KN00962 A IN2014KN00962 A IN 2014KN00962A IN 962KON2014 A IN962KON2014 A IN 962KON2014A IN 2014KN00962 A IN2014KN00962 A IN 2014KN00962A
Authority
IN
India
Prior art keywords
phosphate
type
met
peaks
powder
Prior art date
Application number
Inventor
Gunnar Bühler
Christian Graf
Andreas Jazdanian
Kilian Schwarz
Michael Rapphahn
Original Assignee
Chem Fab Budenheim Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Fab Budenheim Kg filed Critical Chem Fab Budenheim Kg
Publication of IN2014KN00962A publication Critical patent/IN2014KN00962A/en

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/37—Phosphates of heavy metals
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/37—Phosphates of heavy metals
    • C01B25/377—Phosphates of heavy metals of manganese
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C01P2002/54—Solid solutions containing elements as dopants one element only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/40—Particle morphology extending in three dimensions prism-like
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Abstract

3422xy3422Monometallic phosphate containing manganese (Mn) of the type Mn(PO) · 3 HO or mixed metallic phosphate of the type (Mn Met)(PO) · 3 HO wherein x + y = 1 and Met represents one or multiple metals selected from Fe Co Ni Sc Ti V Cr Cu Zn Be Mg Ca Sr Ba AI Zr Hf Re Ru La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb and Lu characterised in that the phosphate in the powder x ray diffraction diagram has peaks at 10.96 ± 0.05 12.78 ± 0.17 14.96 ± 0.13 17.34 ± 0.15 18.98 ± 0.18 21.75 ± 0.21 22.07 ± 0.11 22.97 ± 0.10 25.93 ± 0.25 26.95 ± 0.30 27.56 ± 0.10 29.19 ± 0.12 29.84 ± 0.21 30.27 ± 0.12 34.86 ± 0.21 35.00 ± 0.20 35.33 ± 0.30 35.58 ± 0.10 35.73 ± 0.12 42.79 ± 0.45 43.37 ± 0.45 44.70 ± 0.15 and 44.93 ± 0.20 degree two Theta based on CuKa radiation.
IN962KON2014 2011-12-21 2012-12-21 IN2014KN00962A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE201110056816 DE102011056816A1 (en) 2011-12-21 2011-12-21 Manganese-containing metal phosphates and process for their preparation
PCT/EP2012/076669 WO2013093014A1 (en) 2011-12-21 2012-12-21 Metal phosphate containing manganese and method for its production

Publications (1)

Publication Number Publication Date
IN2014KN00962A true IN2014KN00962A (en) 2015-10-09

Family

ID=47471837

Family Applications (1)

Application Number Title Priority Date Filing Date
IN962KON2014 IN2014KN00962A (en) 2011-12-21 2012-12-21

Country Status (13)

Country Link
US (1) US9350020B2 (en)
EP (1) EP2794472A1 (en)
JP (1) JP6097306B2 (en)
KR (1) KR20140110892A (en)
CN (1) CN104039693B (en)
BR (1) BR112014012066A8 (en)
CA (1) CA2851432A1 (en)
DE (1) DE102011056816A1 (en)
IN (1) IN2014KN00962A (en)
MY (1) MY185281A (en)
RU (1) RU2616063C2 (en)
TW (1) TWI576312B (en)
WO (1) WO2013093014A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102011056812A1 (en) * 2011-12-21 2013-06-27 Chemische Fabrik Budenheim Kg Metal phosphates and process for their preparation
DE102014100026A1 (en) * 2014-01-02 2015-07-02 Chemische Fabrik Budenheim Kg Mixed-metallic crystalline orthophosphates for the time-controlled release of trace elements in rhizodermal and epidermal areas of plants
DE102014118907A1 (en) * 2014-12-17 2016-06-23 Chemische Fabrik Budenheim Kg For the preparation of cathodes for Li-ion batteries suitable phosphate compounds
CN105226245B (en) * 2015-08-27 2018-03-09 青海泰丰先行锂能科技有限公司 A kind of anode material for lithium-ion batteries and preparation method thereof
US10173897B2 (en) 2016-05-10 2019-01-08 Guiqing Huang Method of synthesizing phosphate salt of high purity
CN106085429A (en) * 2016-07-11 2016-11-09 河北大学 Wide range LED fluorescent powder of a series of Color tunable and preparation method thereof
CN106058219B (en) * 2016-08-11 2018-05-22 湖南瑞翔新材料股份有限公司 Compound coating agent, high voltage cobalt acid lithium and preparation method thereof
CN107032314B (en) * 2016-11-26 2018-07-17 华东理工大学 A kind of preparation method of manganese phosphate nanocages
TWI739098B (en) * 2018-06-25 2021-09-11 國立清華大學 Metal (ii) phosphate powders, lithium metal phosphate powders for li-ion battery, and methods for manufacturing the same
CN112340720B (en) * 2019-08-06 2023-05-16 湖南师范大学 Zinc ion battery positive electrode material based on doped zinc-manganese phosphate structure and synthesis method thereof
CN113428850B (en) * 2021-06-23 2023-09-01 青岛科技大学 Method for preparing three-shell layer hydrogen phosphate hollow nano cage material by layer-by-layer assembly method at room temperature
CN115124010B (en) * 2022-07-15 2023-05-30 湖北万润新能源科技股份有限公司 Manganese (II) phosphate nanosheet, lithium manganese iron phosphate positive electrode material and preparation method thereof

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SU539831A1 (en) * 1973-12-21 1976-12-25 Белорусский технологический институт им.С.М.Кирова Method of producing manganese orthophosphate trihydrate
SU676549A1 (en) * 1974-02-18 1979-07-30 Белорусский технологический институт им.С.М.Кирова Method of producing manganese orthophosphate trihydrate
US5910382A (en) 1996-04-23 1999-06-08 Board Of Regents, University Of Texas Systems Cathode materials for secondary (rechargeable) lithium batteries
JP4749551B2 (en) 1999-04-06 2011-08-17 ソニー株式会社 Positive electrode active material and non-aqueous electrolyte secondary battery
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EP1261050A1 (en) * 2001-05-23 2002-11-27 n.v. Umicore s.a. Lithium transition-metal phosphate powder for rechargeable batteries
JP4103487B2 (en) * 2002-07-29 2008-06-18 ソニー株式会社 Method for producing positive electrode active material and method for producing non-aqueous electrolyte battery
UA70214A (en) * 2003-12-30 2004-09-15 Univ Nat Agrarian Medium phosphates of mangane-cobalt trihydrates and a method for obtaining the same
US20070160752A1 (en) * 2006-01-09 2007-07-12 Conocophillips Company Process of making carbon-coated lithium metal phosphate powders
DE102009001204A1 (en) * 2009-02-26 2010-09-02 Chemische Fabrik Budenheim Kg Production of iron orthophosphate
JP5429980B2 (en) * 2009-11-05 2014-02-26 テイカ株式会社 Method for producing carbon-olivine-type manganese iron phosphate lithium composite and positive electrode material for lithium ion battery
EP2355214B1 (en) * 2010-01-28 2013-12-25 Prayon Lithium accumulators based on lithiated iron phosphate and carbon
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CN102205955A (en) * 2011-03-25 2011-10-05 江苏国泰锂宝新材料有限公司 Preparation method for battery anode material LiMPO4

Also Published As

Publication number Publication date
RU2014129527A (en) 2016-02-10
JP2015502911A (en) 2015-01-29
CN104039693A (en) 2014-09-10
BR112014012066A2 (en) 2017-06-13
JP6097306B2 (en) 2017-03-15
US20150108412A1 (en) 2015-04-23
EP2794472A1 (en) 2014-10-29
KR20140110892A (en) 2014-09-17
DE102011056816A1 (en) 2013-08-01
BR112014012066A8 (en) 2017-06-20
CN104039693B (en) 2017-03-01
MY185281A (en) 2021-04-30
WO2013093014A1 (en) 2013-06-27
TW201343542A (en) 2013-11-01
US9350020B2 (en) 2016-05-24
TWI576312B (en) 2017-04-01
CA2851432A1 (en) 2013-06-27
RU2616063C2 (en) 2017-04-12

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