GB787300A - Substituted 1, 2, 3, 4-tetrahydronaphthalenes - Google Patents
Substituted 1, 2, 3, 4-tetrahydronaphthalenesInfo
- Publication number
- GB787300A GB787300A GB171/56A GB17156A GB787300A GB 787300 A GB787300 A GB 787300A GB 171/56 A GB171/56 A GB 171/56A GB 17156 A GB17156 A GB 17156A GB 787300 A GB787300 A GB 787300A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ethyl
- tetrahydronaphthalene
- tetramethyl
- tolyl
- acetyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000005329 tetralinyl group Chemical class C1(CCCC2=CC=CC=C12)* 0.000 title 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- XTWHZKTXSJZYLK-UHFFFAOYSA-N 1-(5-ethyl-3,5,8,8-tetramethyl-6,7-dihydronaphthalen-2-yl)ethanone Chemical compound CC(=O)C1=C(C)C=C2C(CC)(C)CCC(C)(C)C2=C1 XTWHZKTXSJZYLK-UHFFFAOYSA-N 0.000 abstract 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 abstract 2
- QHPWUKFONYNREE-UHFFFAOYSA-N 3,6-dimethyl-6-(4-methylphenyl)heptan-3-ol Chemical compound CC(CC)(CCC(C)(C1=CC=C(C=C1)C)C)O QHPWUKFONYNREE-UHFFFAOYSA-N 0.000 abstract 1
- HMJHOYFMNZAJFP-UHFFFAOYSA-N 4-ethyl-1,1,4,6-tetramethyl-2,3-dihydronaphthalene Chemical compound C1=C(C)C=C2C(CC)(C)CCC(C)(C)C2=C1 HMJHOYFMNZAJFP-UHFFFAOYSA-N 0.000 abstract 1
- KCOMWVWZVIVQFP-UHFFFAOYSA-N 5-methyl-5-(4-methylphenyl)hexan-2-one Chemical compound CC(CCC(C)=O)(C)C1=CC=C(C=C1)C KCOMWVWZVIVQFP-UHFFFAOYSA-N 0.000 abstract 1
- VBCIOOKAKHGVMI-UHFFFAOYSA-N 5-methylhex-5-en-2-one Chemical compound CC(=C)CCC(C)=O VBCIOOKAKHGVMI-UHFFFAOYSA-N 0.000 abstract 1
- 238000005727 Friedel-Crafts reaction Methods 0.000 abstract 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 229910010062 TiCl3 Inorganic materials 0.000 abstract 1
- 230000000397 acetylating effect Effects 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- VMPVEPPRYRXYNP-UHFFFAOYSA-I antimony(5+);pentachloride Chemical compound Cl[Sb](Cl)(Cl)(Cl)Cl VMPVEPPRYRXYNP-UHFFFAOYSA-I 0.000 abstract 1
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 abstract 1
- FRIJBUGBVQZNTB-UHFFFAOYSA-M magnesium;ethane;bromide Chemical compound [Mg+2].[Br-].[CH2-]C FRIJBUGBVQZNTB-UHFFFAOYSA-M 0.000 abstract 1
- 235000011007 phosphoric acid Nutrition 0.000 abstract 1
- 239000000344 soap Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 abstract 1
- 239000011592 zinc chloride Substances 0.000 abstract 1
- 235000005074 zinc chloride Nutrition 0.000 abstract 1
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
- C11B9/0053—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms both rings being six-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention comprises 7-acetyl-1,1,4,6-tetramethyl - 4 - ethyl - 1,2,3,4 - tetrahydronaphthalene and its preparation by reacting toluene with methallyl acetone in presence of a Friedel-Crafts catalyst to form 5-methyl-5-p-tolyl-2-hexanone, reacting this with ethyl magnesium bromide to form 3,6-dimethyl-6-p-tolyl-3-heptanol, cyclizing the latter in presence of an acidic type of catalyst such as HF, H2SO4, H3PO4, BF3, P2O5, AlCl3, FeCl3, SbCl5, ZnCl2 or TiCl3 to form 1,1,4,6-tetramethyl-4-ethyl-1,2,3,4-tetrahydronaphthalene and acetylating the latter. An example is given.ALSO:Soaps contain the musk-like compound 7-acetyl - 1,1,4,6 - tetramethyl - 4 - ethyl - 1,2,3,4-tetrahydronaphthalene.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US787300XA | 1955-02-23 | 1955-02-23 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB787300A true GB787300A (en) | 1957-12-04 |
Family
ID=22145877
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB171/56A Expired GB787300A (en) | 1955-02-23 | 1956-01-03 | Substituted 1, 2, 3, 4-tetrahydronaphthalenes |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB787300A (en) |
-
1956
- 1956-01-03 GB GB171/56A patent/GB787300A/en not_active Expired
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