GB649445A - Manufacture of hydrazine derivatives and triazole derivatives - Google Patents
Manufacture of hydrazine derivatives and triazole derivativesInfo
- Publication number
- GB649445A GB649445A GB472148A GB472148A GB649445A GB 649445 A GB649445 A GB 649445A GB 472148 A GB472148 A GB 472148A GB 472148 A GB472148 A GB 472148A GB 649445 A GB649445 A GB 649445A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrazine
- derivatives
- amino
- triazole
- semicarbazide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
- C07D249/10—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D249/14—Nitrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A process for the manufacture of hydrazine derivatives and triazole derivatives comprises reacting hydrazine or its derivatives having the -NH.NH- structure with carbon monoxide at a pressure above 100 atmospheres and a temperature above 30 DEG C. Semicarbazide and cyclic compounds such as 4 - amino - 1,2,4-triazol-3-one and 4-aminotriazole may be produced. Derivatives of hydrazine may be used as starting materials including hydrazine hydrate semicarbazide, carbohydrazide and hydrazine dicarbonamide. The reaction may be carried out under anhydrous conditions or with water or other liquid media present. The process may be operated continuously. In examples by heating under pressure with carbon monoxide (1) 4-amino-1,2,4-triazol-3-one and (2) 4-amino-1,2,4-triazole are prepared from aqueous hydrazine hydrate; 4-amino-1,2,4-triazol-3-one is prepared from an aqueous solution containing semicarbazide and hydrazine hydrate; (4) semicarbazide from hydrazine hydrate and (5) 4-amino-1,2,4-triazole from aqueous hydrazine hydrate and hydrazine dicarbonamide. Specification 583,172, [Group III], is referred to.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB472148A GB649445A (en) | 1948-02-18 | 1948-02-18 | Manufacture of hydrazine derivatives and triazole derivatives |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB472148A GB649445A (en) | 1948-02-18 | 1948-02-18 | Manufacture of hydrazine derivatives and triazole derivatives |
Publications (1)
Publication Number | Publication Date |
---|---|
GB649445A true GB649445A (en) | 1951-01-24 |
Family
ID=9782536
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB472148A Expired GB649445A (en) | 1948-02-18 | 1948-02-18 | Manufacture of hydrazine derivatives and triazole derivatives |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB649445A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113480486A (en) * | 2021-07-30 | 2021-10-08 | 赣南师范大学 | 3-amido-1, 2,4-triazole derivative and preparation method and application thereof |
-
1948
- 1948-02-18 GB GB472148A patent/GB649445A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113480486A (en) * | 2021-07-30 | 2021-10-08 | 赣南师范大学 | 3-amido-1, 2,4-triazole derivative and preparation method and application thereof |
CN113480486B (en) * | 2021-07-30 | 2022-05-24 | 赣南师范大学 | 3-amido-1, 2,4-triazole derivative and preparation method and application thereof |
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