GB435113A - The manufacture of organic disulphides - Google Patents
The manufacture of organic disulphidesInfo
- Publication number
- GB435113A GB435113A GB8098/34A GB809834A GB435113A GB 435113 A GB435113 A GB 435113A GB 8098/34 A GB8098/34 A GB 8098/34A GB 809834 A GB809834 A GB 809834A GB 435113 A GB435113 A GB 435113A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- sodium chlorate
- sodium
- hydrochloric acid
- chlorate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B45/00—Formation or introduction of functional groups containing sulfur
- C07B45/06—Formation or introduction of functional groups containing sulfur of mercapto or sulfide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Organic disulphides are obtained by subjecting organic compounds which contain sulphhydryl groups to the action of chloric acid or its salts, with or without a compound having the property of reducing chloric acid to a lower stage of oxidation, and with or without osmium tetroxide as catalyst. Aqueous or organic solvents may be employed. According to examples, ethylmercaptan, benzylmercaptan, p-thiocresol, and thiosalicylic acid, are converted into the corresponding disulphides with the use of hydrochloric acid and sodium chlorate in aqueous or benzene solution; thiosalicylic acid is treated with sodium chlorate and sodium nitrite in alkaline solution, to give dithiosalicylic acid; and mercaptobenzothiazole is treated with sodium chlorate in presence of osmium tetroxide to give dibenzothiazyldisulphide, which may also be obtained by oxidation of mercaptobenzothiazole with mixed nitric acid, sulphuric acid and sodium chlorate, with hydrochloric acid and sodium chlorate, with hydrochloric acid, sodium chlorate and sodium nitrite, with sodium chlorate and oxalic acid, and with hydrochloric acid, sodium chlorate and sodium bisulphite.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE435113X | 1933-03-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB435113A true GB435113A (en) | 1935-09-16 |
Family
ID=6506732
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB8098/34A Expired GB435113A (en) | 1933-03-21 | 1934-03-14 | The manufacture of organic disulphides |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB435113A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2656392A (en) * | 1948-12-13 | 1953-10-20 | Phillips Petroleum Co | Process for the manufacture of dialkyl sulfides |
-
1934
- 1934-03-14 GB GB8098/34A patent/GB435113A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2656392A (en) * | 1948-12-13 | 1953-10-20 | Phillips Petroleum Co | Process for the manufacture of dialkyl sulfides |
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